Studies on external peak broadening in open-tubular liquid chromatography systems using the exponentially modified Gaussian model

1985 ◽  
Vol 20 (6) ◽  
pp. 357-363 ◽  
Author(s):  
W. M. A. Niessen ◽  
H. P. M. van Vliet ◽  
H. Poppe
Keyword(s):  
Liquid Chromatography ◽  
Gaussian Model ◽  
Peak Broadening ◽  
Open Tubular Liquid Chromatography ◽  
Modified Gaussian Model ◽  
Exponentially Modified Gaussian

Peak Broadening in Open-Tubular Liquid Chromatography with Electroosmotic Flow

1985 ◽  
Vol 57 (2) ◽  
pp. 559-561 ◽  
Author(s):  
Michel. Martin ◽  
Georges. Guiochon ◽  
Yvonne. Walbroehi ◽  
James W. Jorgenson
Keyword(s):  
Liquid Chromatography ◽  
Electroosmotic Flow ◽  
Peak Broadening ◽  
Open Tubular Liquid Chromatography

Approaches to estimate the time and height at the peak maximum in liquid chromatography based on a modified Gaussian model

2011 ◽  
Vol 1218 (10) ◽  
pp. 1385-1392 ◽  
Author(s):  
J.J. Baeza-Baeza ◽  
J.R. Torres-Lapasió ◽  
M.C. García-Álvarez-Coque
Keyword(s):  
Liquid Chromatography ◽  
Gaussian Model ◽  
Peak Maximum ◽  
Modified Gaussian Model

Liquid Chromatographic Analysis System for Cyclopiazonic Acid in Peanuts

1984 ◽  
Vol 67 (4) ◽  
pp. 728-731 ◽  
Author(s):  
John A Lansden
Keyword(s):  
Limit Of Detection ◽  
Gaussian Model ◽  
Cyclopiazonic Acid ◽  
Detector Response ◽  
Chromatographic Procedure ◽  
Liquid Chromatographic Analysis ◽  
Modified Gaussian Model ◽  
Analysis System ◽  
Liquid Chromatographic ◽  
Exponentially Modified Gaussian

Abstract A liquid chromatographic procedure has been developed for analysis of cyclopiazonic acid in peanuts. The chromatographic system specifies a C18 or C8 column loaded with 4-dodecyldiethylenetriamine and an aqueous mobile phase containing 4-dodecyldiethylenetriamine, zinc acetate, ammonium acetate, 2-propanol, and acetonitrile. Cyclopiazonic acid was extracted from peanuts with methanol-chloroform (20 + 80), partitioned into aqueous sodium bicarbonate, acidified, and back-extracted into dichloromethane. The limit of detection (280 nm UV) was approximately 4 ng and detector response was linear to at least 1 μg pure cyclopiazonic acid. The recovery of cyclopiazonic acid from peanuts spiked at 68.9, 210, and 955 μ/kg was 85.9% (12.86% CV), 72.9% (6.43% CV), and 81.4% (0.40% CV), respectively. Calculation of the chromatographic peak parameters based on the exponentially modified Gaussian model indicated that the C18 column produced less peak skewing than did the C8 column.

Fabrication of columns for open-tubular liquid chromatography using photopolymerization of acrylates

1990 ◽  
Vol 516 (2) ◽  
pp. 301-312 ◽  
Author(s):  
S. Eguchi ◽  
J.G. Kloosterboer ◽  
C.P.G. Zegers ◽  
P.J. Schoenmakers ◽  
P.P.H. Tock ◽  
...  
Keyword(s):  
Liquid Chromatography ◽  
Open Tubular Liquid Chromatography

Recent progress in open tubular liquid chromatography

1997 ◽  
Vol 16 (6) ◽  
pp. 332-342 ◽  
Author(s):  
Remco Swart ◽  
Johan C Kraak ◽  
Hans Poppe
Keyword(s):  
Liquid Chromatography ◽  
Recent Progress ◽  
Open Tubular Liquid Chromatography
Sign in / Sign up

Export Citation Format

Share Document