Quantitative high-resolution gas chromatographic determination of stereoisomeric composition of chiral volatile compounds in the picogram range by ec-detection

1995 ◽  
Vol 21 (7) ◽  
pp. 987-994 ◽  
Author(s):  
Ann-Britt Wassgren ◽  
Gunnar Bergström
1962 ◽  
Vol 16 ◽  
pp. 1289-1290 ◽  
Author(s):  
Roger Bonnichsen ◽  
Maire Linturi ◽  
Anne-Marie Olson ◽  
T. Briggs ◽  
G. A. D. Haslewood ◽  
...  

1995 ◽  
Vol 41 (1-2) ◽  
pp. 29-33 ◽  
Author(s):  
G. Lercker ◽  
N. Frega ◽  
F. Bocci ◽  
M. T. Rodriguez-Estrada

1971 ◽  
Vol 17 (2) ◽  
pp. 82-85 ◽  
Author(s):  
Naresh C Jain

Abstract An extremely simple, rapid method is described for simultaneously determining methanol, ethanol, acetone, isopropanol, and low-boiling hydrocarbons associated with glue sniffing. Less than 1 µl of blood, mixed with an internal standard, is injected directly into a low-cost gas chromatograph equipped with a flame-ionization detector. No extraction, distillation, and (or) sample preparation is required, and the method is sensitive to less than 10 µg of alcohol per ml.


1986 ◽  
Vol 69 (4) ◽  
pp. 714-720
Author(s):  
Alan M Rothman ◽  
◽  
A Ausari ◽  
O O Bennett ◽  
E J Blusiewicz ◽  
...  

Abstract A liquid chromatographic (LC) method was used to determine p,p'- and o,p'-isomers of dicofol AI (active ingredient) in Kelthane® EC and MF formulations. Samples are dissolved in methanol and AI components and impurities are separated on a high resolution C8 column in series with a short C18 guard column, with a methanol-water-acetic acid mobile phase. Cleaned samples are directly injected into the LC system and are monitored at 254 nm. Twelve collaborators submitted results on 5 samples. Using 95% confidence criteria, the average total standard deviation of the total AI across all samples was 2.82%. The method has been adopted official first action.


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