Study of the thermal properties of derivatives of sulfonamides

1983 ◽  
Vol 26 (1) ◽  
pp. 145-150 ◽  
Author(s):  
J. Ciba ◽  
J. Sycz ◽  
J. Trzcionka
2012 ◽  
Author(s):  
Elmars Zarins ◽  
Karina Siltane ◽  
Elina Misina ◽  
Valdis Kokars ◽  
Kristine Lazdovica ◽  
...  

Author(s):  
Ghazi Mahmoud Hasso Jawish, Rushdi Madwar, Francois Kara Bet Ghazi Mahmoud Hasso Jawish, Rushdi Madwar, Francois Kara Bet

In this research, two ether derivatives of phenolic azo dyes were synthesized via Williamson's reaction according to the SN2 mechanism. The prepared compounds were radically polymerized using (AIBN) as an initiator and their structures were identified by FT-IR and 1H-NMR. Furthermore, thermal properties of these polymers was made by (DSC). Bandgap energy have been calculated to indicate the ability of these polymers as optical semiconductors, it was 2.8ev, 2.4ev for P(AO2) and P(AON1) respectively. Beside the determination of refractive index, kinematic viscosity, density, and degree of Turbidity.


Polymers ◽  
2020 ◽  
Vol 12 (11) ◽  
pp. 2447
Author(s):  
Katarzyna Wilpiszewska ◽  
Adrian Krzysztof Antosik ◽  
Beata Schmidt ◽  
Jolanta Janik ◽  
Joanna Rokicka

The carboxymethylated derivatives of starch (CMS) and cellulose (CMC) were used for film preparation. The infrared spectroscopy revealed that crosslinking via ester bridges with citric acid occurred between the two polysaccharide derivatives. The effect of polysaccharide derivatives ratio on physicochemical properties of prepared films was evaluated. Generally, the values of tested parameters (moisture absorption, surface roughness, and mechanical and thermal properties) were between the values noted for neat CMS or CMC-based films. However, the physicochemical properties of the system with equal CMS/CMC weight ratio diverged from this trend, i.e., the highest tensile strength, the highest Young’s modulus (ca. 3.4 MPa and ca. 4.9 MPa, respectively), with simultaneously the lowest moisture absorption (18.5% after 72 h) have been noted. Such systems could potentially find application in agriculture or pharmacy.


2007 ◽  
Vol 48 (5) ◽  
pp. 889-898 ◽  
Author(s):  
N. B. Morozova ◽  
P. A. Stabnikov ◽  
I. A. Baidina ◽  
P. P. Semyannikov ◽  
S. V. Trubin ◽  
...  

1998 ◽  
Vol 129 (5) ◽  
pp. 473-480
Author(s):  
B. Kowalczyk ◽  
W. Baran ◽  
K. Chaczatrian

2007 ◽  
Vol 43 (4) ◽  
pp. 392-397 ◽  
Author(s):  
S. N. Mikhnevich ◽  
P. A. Shcheglov ◽  
D. V. Drobot

2013 ◽  
Vol 65 (9-10) ◽  
pp. 762-772 ◽  
Author(s):  
Abraham Olasupo Oladebeye ◽  
Aladesanmi Augustine Oshodi ◽  
Isiaka Adekunle Amoo ◽  
Alias Abd Karim

Author(s):  
M.M. Ghoneim ◽  
N.A. El-Ghamaz ◽  
A.Z. El-Sonbati ◽  
M.A. Diab ◽  
A.A. El-Bindary ◽  
...  

2018 ◽  
Vol 15 (30) ◽  
pp. 193-200
Author(s):  
E. A. GULIYEVA ◽  
G. Z. SULEIMANOV

This paper describes the data on synthesis of bis(cyclopentadienyl)vanadium(III) of pentacarbonyl rhenium bistetrahydrofuranate complex with the reaction between dicyclopentadienylvanadium (III) chloride and rhenium sodiumpentacarbonyl in tetrahydrofurane (THF). Formed in this case the target product was separated from reaction mixture by extracting with hot hexane. Their reactionary ability in relation to protonic and aprotonic acids Lewis had been inverstigated. It is revealed, that at interaction of the above mentioned complexes with HCl there is a splitting Re-V bond with formation (C5H5)2VCl and HRe(CO)5; (C5H5)2VCl and HRe(CO)4PPh3 respectively. At interaction with HgCl2 also occurs having break V-Re bond and it turn out (C5H5)2VCl and (OC)5ReHgCl; (C5H5)2VCl and PPh3(OC)4ReHgCl. The interection of these complexes with ligands of various dentate is investigated. A monodentate liqand-triphenil phosphine (PPh3) substitutes one of carbonyl-groups in Re(CO)5) – fragment. Bidentate ligand- acetylacetone (acac) easily push out from coordination sphere vanadium more donor ligand cyclopentadienyl. The composition and structure of the complexes were characterized by the data of NMR, IR, EPR-spectroscopy and thermal analysis.


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