Refractory compound based on low modulus water glass for ramming linings of arc melting furnaces

Refractories ◽  
1982 ◽  
Vol 23 (1-2) ◽  
pp. 66-67
Author(s):  
V. M. Soifer ◽  
O. B. Grishchenko ◽  
V. S. Kozlova ◽  
N. I. Mosolova ◽  
V. N. Abakumova
Keyword(s):  
Water Glass ◽  
Refractory Compound ◽  
Arc Melting ◽  
Low Modulus

Manufacturing of Biomedical Ti-Based Alloys with High Oxygen Content and Various Amount of Beta-Stabilizing Elements

2018 ◽  
Vol 941 ◽  
pp. 2471-2476
Author(s):  
Josef Stráský ◽  
Dalibor Preisler ◽  
Kristína Bartha ◽  
Miloš Janeček
Keyword(s):  
Elastic Modulus ◽  
High Strength ◽  
Beta Phase ◽  
Vacuum Arc ◽  
High Oxygen Content ◽  
Arc Melting ◽  
Vacuum Arc Melting ◽  
Low Modulus ◽  
The Stability ◽  
Effect Of Oxygen

High strength and low elastic modulus are key properties of biomedical Ti-based alloys. Body centred cubic beta phase shows lowest elastic modulus, especially if the stability of the beta phase is low due to the ‘proximity’ to martensitic β to α’’ transformation. It was previously shown that Ti-35Nb-6Ta-7Zr alloy contains biotolerant elements only and exhibits low modulus. By enriching this alloy by 0.7 wt. % of oxygen the strength is significantly enhanced, but elastic modulus increases as well. This fact can be attributed to apparent beta stabilizing effect of oxygen with respect to martensitic β to α’’ transformation. In the present study, six different alloys with reduced niobium and/or tantalum content were prepared by vacuum arc melting. Their microstructure in beta solution treated condition was studied by scanning electron microscopy including energy dispersive spectroscopy and mechanical properties were evaluated by microhardness measurements.

scholarly journals Development of Zirconium-Based Alloys with Low Elastic Modulus for Dental Implant Materials

2019 ◽  
Vol 9 (24) ◽  
pp. 5281
Author(s):  
Minsuk Kim ◽  
Seongbin An ◽  
Chaeeul Huh ◽  
Chungseok Kim
Keyword(s):  
Elastic Modulus ◽  
Stress Shielding ◽  
Melting Process ◽  
Shielding Effect ◽  
X Ray Diffraction ◽  
Two Phase ◽  
Arc Melting ◽  
Pure Zirconium ◽  
Low Modulus ◽  
The Difference

The stress-shielding effect is a phenomenon in which the mutual coupling between bones and bio-materials of the human body is loosened due to the difference in elastic modulus, and bone absorption occurs due to the difference in density, which causes a shortening of the life of the material. The purpose of this study is to develop a zirconium-based alloy with low modulus and to prevent the stress-shielding effect. Zr–7Cu–xSn (x = 1, 5, 10, 15 mass%) alloys were prepared by an arc-melting process of pure zirconium, oxygen-free copper, and tin, respectively. The Zr–7Cu–xSn alloy has two phase α-Zr and Zr2Cu intermetallic compounds. Microstructure characterization was analyzed by microscopy and X-ray diffraction. Corrosion tests of zirconium-based alloys were conducted through polarization tests, and zirconium-based alloys had better corrosion characteristics than other metal bio-materials. In general, the elastic modulus value (14–25 GPa) of the zirconium-based alloy is very similar to the elastic modulus value (15–30 GPa) of the human bone. Consequently, the zirconium-based alloy is likely to be used as a bio-material that negates the effect of stress shielding on human bones.

Microanalytical Identification of a New Zr-Nb-Fe Phase

1990 ◽  
Vol 48 (2) ◽  
pp. 132-133
Author(s):  
O.T. Woo ◽  
G.J.C. Carpenter
Keyword(s):  
Trace Elements ◽  
Cold Rolling ◽  
Proportionality Factor ◽  
Tube Material ◽  
X Ray ◽  
Metal Foils ◽  
Arc Melting ◽  
Intermetallic Particles ◽  
Intermetallic Precipitates ◽  
Cold Worked

To study the influence of trace elements on the corrosion and hydrogen ingress in Zr-2.5 Nb pressure tube material, buttons of this alloy containing up to 0.83 at% Fe were made by arc-melting. The buttons were then annealed at 973 K for three days, furnace cooled, followed by ≈80% cold-rolling. The microstructure of cold-worked Zr-2.5 at% Nb-0.83 at% Fe (Fig. 1) contained both β-Zr and intermetallic precipitates in the α-Zr grains. The particles were 0.1 to 0.7 μm in size, with shapes ranging from spherical to ellipsoidal and often contained faults. β-Zr appeared either roughly spherical or as irregular elongated patches, often extending to several micrometres.The composition of the intermetallic particles seen in Fig. 1 was determined using Van Cappellen’s extrapolation technique for energy dispersive X-ray analysis of thin metal foils. The method was employed to avoid corrections for absorption and fluorescence via the Cliff-Lorimer equation: CA/CB = kAB · IA/IB, where CA and CB are the concentrations by weight of the elements A and B, and IA and IB are the X-ray intensities; kAB is a proportionality factor.

Formation process of periodic non-conservative antiphase boundary structure in L-Pd5Ce

1990 ◽  
Vol 48 (4) ◽  
pp. 162-163
Author(s):  
Masaru Itakura ◽  
Noriyuki Kuwano ◽  
Kensuke Oki
Keyword(s):  
Formation Process ◽  
Domain Size ◽  
Antiphase Boundary ◽  
Boundary Structure ◽  
Temperature Phase ◽  
Arc Melting ◽  
Iced Water ◽  
Antiphase Domains ◽  
Low Temperature Phase ◽  
Degree Of Order

The low temperature phase of Pd5Ce (L-Pd5Ce) has a one-dimensional long period superstructure (1D-LPS) derived from Ll2. The periodic antiphase boundaries (APBs) are parallel to (110) planes and have a shift vector of 1/2[110]. Hereafter, the indices are referred to the basic lattices of Ll2 As insertion of the APB causes a change in composition, such an APB is called “non-conservative”. Then, a domain size M depends upon the Ce concentration in the alloy. It was found that M increases also with temperature. The temperature dependency of M is attributed to a change of the degree of order within the antiphase domains. In this work, morphology of the non-conservative APBs is observed to clarify the formation process of the 1D-LPS.The alloy of Pd-16.7 at%Ce was prepared by arc melting in argon atmosphere. Disc specimens made from the alloy ingot were first held at 985 K for 260 ks and quenched in iced water to obtain the state of M=∞ or Ll2, followed by annealing for various lengths of time. The annealing temperature was 873 K where the equilibrium value for M is about 3 in unit of (110) lattice spacing of Ll2. Observation was carried out using microscopes JEM-2000FX, JEM-4000EX (HVEM Lab., Kyushu Univ.) and JEM-2000EX (Dept. of Mater. Sci. Tech., Kyushu Univ.).

Morphology of Σ3{/70.53°} grain boundaries in a C15 intermetallic compound

1994 ◽  
Vol 52 ◽  
pp. 684-685
Author(s):  
Fuming Chu ◽  
D. P. Pope ◽  
D. S. Zhou ◽  
T. E. Mitchell
Keyword(s):  
Grain Boundary ◽  
Grain Boundaries ◽  
Crystallographic Analysis ◽  
Laves Phase ◽  
Second Phase ◽  
Bright Field Image ◽  
Boundary Edge ◽  
Arc Melting ◽  
Fcc Lattice ◽  
Diffraction Patterns

A C15 Laves phase, HfV2+Nb, shows promising mechanical properties and here we describe the structure of its grain boundaries. The C15 Laves phase has a fcc lattice with a=7.4Å. An alloy of composition Hf14V64Nb22 (including a C15 matrix and a second phase of V-rich bcc solution) was made by arc-melting. The alloy was homogenized at 1200°C for 120h. Preliminary study concentrated on Σ3{<110>/70.53°} grain boundaries in the C15 phase using Philips 400T and CM 30 microscopes.The most-commonly observed morphology of Σ3{<110>/70.53°} grain boundaries in the C15 phase is a faceted boundary. A bright field image (BFI) of the faceted boundary and the corresponding diffraction patterns with the grain boundary edge-on are shown in Fig. 1(a). From the diffraction patterns using a <110> zone axis for both grains, it is obvious that this is a Σ3{<110>/70.53°} grain boundary. Crystallographic analysis shows that the Σ3{<110>/70.53°} grain boundaries selectively facet with the following relationships between the two grains: {111}1//{111}2, {112}1//{112}2, {111}1//{115}2, and {001}1//{221}2.

Influence of low-modulus inclusions of BN on the Y-TZP ceramic properties

2019 ◽  
pp. 49-56
Author(s):  
Buyakov A. S. ◽  
◽  
Mirovoy Yu. A. ◽  
Buyakova S. P. ◽  
◽  
...  
Keyword(s):  
Low Modulus

scholarly journals Sodium Metasilicate Cemented Analogue Material and Its Mechanical Properties

2016 ◽  
Vol 2016 ◽  
pp. 1-17 ◽  
Author(s):  
Songlin Yue ◽  
Yanyu Qiu ◽  
Pengxian Fan ◽  
Pin Zhang ◽  
Ning Zhang
Keyword(s):  
Complex Geometry ◽  
Sodium Metasilicate ◽  
Raw Material ◽  
Fine Aggregate ◽  
Regression Equations ◽  
Deformation And Failure ◽  
Orthogonal Experiments ◽  
Low Modulus ◽  
New Type ◽  
The Relationship

Analogue material with appropriate properties is of great importance to the reliability of geomechanical model test, which is one of the mostly used approaches in field of geotechnical research. In this paper, a new type of analogue material is developed, which is composed of coarse aggregate (quartz sand and/or barite sand), fine aggregate (barite powder), and cementitious material (anhydrous sodium silicate). The components of each raw material are the key influencing factors, which significantly affect the physical and mechanical parameters of analogue materials. In order to establish the relationship between parameters and factors, the material properties including density, Young’s modulus, uniaxial compressive strength, and tensile strength were investigated by a series of orthogonal experiments with hundreds of samples. By orthogonal regression analysis, the regression equations of each parameter were obtained based on experimental data, which can predict the properties of the developed analogue materials according to proportions. The experiments and applications indicate that sodium metasilicate cemented analogue material is a type of low-strength and low-modulus material with designable density, which is insensitive to humidity and temperature and satisfies mechanical scaling criteria for weak rock or soft geological materials. Moreover, the developed material can be easily cast into structures with complex geometry shapes and simulate the deformation and failure processes of prototype rocks.

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