Modified spectrophotometric method for the determination of traces of boron using quinalizarin in a sulfuric-acetic acid medium

1971 ◽  
Vol 59 (4) ◽  
pp. 577-581 ◽  
Author(s):  
H. K. L. Gupta ◽  
D. F. Boltz
The Analyst ◽  
1976 ◽  
Vol 101 (1208) ◽  
pp. 867
Author(s):  
J. P. Sharma ◽  
V. K. S. Shukla ◽  
A. K. Dubey

2019 ◽  
Vol 8 (5) ◽  
pp. 185-186
Author(s):  
Lokanatha Rai KM ◽  
Prakruthi Aiyappa K ◽  
Harshitha BL ◽  
Chaitra Shivani KS

2010 ◽  
Vol 7 (4) ◽  
pp. 1426-1434
Author(s):  
B. K. Jayanna ◽  
G. Nagendrappa ◽  
Ninge Gowda

A novel, simple, sensitive spectrophotometric method is proposed for the determination of cobalt(II). Chloromine-T with iodine in acetic acid produces iodine monochloride, which oxidizes promethazine hydrochloride and diphenylamine to absorbing cations. Those would associate later with cobalt complex to form an ion pair, [Ph+] [CoCl4]-and [Dh2+] [CoCl4]-2in acid medium. These appear to provide exceptional color stability to the systems. The results compare favorably with those of reported method. The conditions required for the determination of cobalt(II) are described and related analytical parameters are also calculated.


1970 ◽  
Vol 50 (2) ◽  
pp. 354-357 ◽  
Author(s):  
J.A. Pérez-Bustamante ◽  
D.Alvarez Jiménez ◽  
F. Burriel-Martí

1964 ◽  
Vol 47 (4) ◽  
pp. 754-755
Author(s):  
William S Hardesty

Abstract The method of Barakat and co-workers for determination of vitamin C in colored products has been modified for potentiometric use. The procedure is simple and rapid: An aliquot of sample containing 1—3 nig of ascorbic acid is titrated in a 3% acetic acid medium in the presence of KI with previously standardized 0.01% N-bromosuccinimide. The potentiometric titration uses two Pt electrodes with a polarizing current. Results were compared with the USP XVI method and the AOAC 2,6-dichlorophenol indophenol method. Recoveries, obtained from seven commercial products, four of which were vitamin C-enriched, ranged from 96 to 101%. The method also works well on drug mixtures containing ascorbic acid. It is recommended that the method be studied collaboratively.


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