Qualitative determination of glyoxylic acid by paper chromatography

1959 ◽  
Vol 8 (7) ◽  
pp. 1290-1291
Author(s):  
A. M. Pakhomov ◽  
V. M. Prostyakova ◽  
V. I. Ivanov
Keyword(s):  
Paper Chromatography ◽  
Glyoxylic Acid ◽  
Qualitative Determination

scholarly journals Citrus limon L Burmf leaves from North Eastern India : A source of Amino acids

2019 ◽  
Vol 9 (4-A) ◽  
pp. 269-270
Author(s):  
Elija Khatiwora
Keyword(s):  
Amino Acids ◽  
Paper Chromatography ◽  
Citrus Limon ◽  
Chromatographic Technique ◽  
Eastern India ◽  
Mobile Phases ◽  
North Eastern ◽  
North Eastern India ◽  
Qualitative Determination

Identification of amino acids from air shade dried powered material of Citrus limon L Burmf (Assam lemon) leaves was carried out in this experiment. Paper chromatographic technique was used for the qualitative determination of amino acids with different mobile phases. Specific amino acids were detected in specific mobile phases. The obtained amino acids were identified by comparing with standard amino acids. Total nine amino acids were detected from of Citrus limon L Burmf leaves. Two mobile phases were found suitable for detection of amino acids present in the leaves of citrus limon L Burmf. Keyword: Citrus limon, Paper chromatography, Amino acids.

A SIMPLE QUALITATIVE DETERMINATION OF JOSEPHSON TUNNEL JUNCTION PARAMETERS NEAR THE TRANSITION TEMPERATURE

1978 ◽  
Vol 39 (C6) ◽  
pp. C6-1232-C6-1233 ◽  
Author(s):  
N. F. Pedersen ◽  
J. Mygind ◽  
O. H. Soerensen ◽  
B. Dueholm
Keyword(s):  
Transition Temperature ◽  
Tunnel Junction ◽  
Josephson Tunnel ◽  
Qualitative Determination

INDIREKTE PAPIERCHROMATOGRAPHISCHE METHODE ZUR BESTIMMUNG DER HARNOESTROGENE

1961 ◽  
Vol 38 (4) ◽  
pp. 545-562 ◽  
Author(s):  
L. Kecskés ◽  
F. Mutschler ◽  
I. Glós ◽  
E. Thán ◽  
I. Farkas ◽  
...  
Keyword(s):  
Pregnant Women ◽  
Granulosa Cell ◽  
Iron Content ◽  
List Type ◽  
Granulosa Cell Tumour ◽  
Hydrolysis Of ◽  
Phenol Fraction ◽  
Qualitative Determination

ABSTRACT 1. An indirect paperchromatographic method is described for separating urinary oestrogens; this consists of the following steps: acidic hydrolysis, extraction with ether, dissociation of phenol-fractions with partition between the solvents. Previous purification of phenol fraction with the aid of paperchromatography. The elution of oestrogen containing fractions is followed by acetylation. Oestrogen acetate is isolated by re-chromatography. The chromatogram was developed after hydrolysis of the oestrogens 'in situ' on the paper. The quantity of oestrogens was determined indirectly, by means of an iron-reaction, after the elution of the iron content of the oestrogen spot, which was developed by the Jellinek-reaction. 2. The method described above is satisfactory for determining urinary oestrogen, 17β-oestradiol and oestriol, but could include 16-epioestriol and other oestrogenic metabolites. 3. The sensitivity of the method is 1.3–1.6 μg/24 hours. 4. The quantitative and qualitative determination of urinary oestrogens with the above mentioned method was performed in 50 pregnant and 9 non pregnant women, and also in 2 patients with granulosa cell tumour.

Development of a New Method for Determination of the Oil Content from Microalgae Lipid Fraction

2017 ◽  
Vol 68 (4) ◽  
pp. 671-674
Author(s):  
Ana Maria Galan ◽  
Ioan Calinescu ◽  
Elena Radu ◽  
Elena Emilia Oprescu ◽  
Gabriel Vasilievici ◽  
...  
Keyword(s):  
Sunflower Oil ◽  
Oil Content ◽  
Lipid Fraction ◽  
New Method ◽  
Ms Analysis ◽  
Qualitative Determination ◽  
Tga Analysis

The purpose of this study was to develop a method for rapid quantitative and qualitative determination of the oil from microalgae lipid fraction obtained from Nannochloris sp biomass. The lipid fraction was first refluxed with 4% KOH in MeOH (60, 90, 120 min), followed by reaction with 20% BF3 in MeOH, using different times of reflux (90,120, 150 min) for each time of reflux with 4% KOH in MeOH. The FAME samples were analyzed by GC-MS analysis. 120 min reflux with 4% KOH in MeOH, 90 min with 20% BF3 in MeOH and a ratio lipid fraction: 4% KOH in MeOH: 20% BF3 in MeOH=1:20:27, were required to obtain the higher percent of oil in the microalgae lipid fraction. The relevance of the method developed was proved by TGA analysis and by transesterification of a sunflower oil sample in the same conditions.

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