Second seminar on methods of obtaining and the physico-chemical properties op refractory carbides and heat-resistant materials made from them

1967 ◽  
Vol 6 (9) ◽  
pp. 767-768
Author(s):  
G. N. Makarenko ◽  
V. B. Fedorus
Keyword(s):  
Chemical Properties ◽  
Heat Resistant ◽  
Physico Chemical

scholarly journals USING MELT HIGH-TEMPERATURE TREATMENT FOR PROCESSING FOUNDRY WASTES OF HEAT-RESISTANT ALLOY

2019 ◽  
Vol 62 (3) ◽  
pp. 222-227
Author(s):  
A. G. Тyagunov ◽  
Е. Е. Baryshev ◽  
G. V. Tyagunov ◽  
Т. K. Кostina ◽  
K. Yu. Shmakova
Keyword(s):  
High Temperature ◽  
Crystallization Process ◽  
Chemical Properties ◽  
High Temperature Treatment ◽  
Critical Temperatures ◽  
Heat Resistant ◽  
Technical Requirements ◽  
Melt Treatment ◽  
Physico Chemical ◽  
Temperature Dependences

At present time, metallurgical wastes are used in metallurgical alloys production more and more. The volume accumulation and increase of return age effect on charge pollution by undesirable elements and nonmetallic inclusions. As a result, structure and properties of the casting inevitably get worse. This circumstance must influence on polytherm’s character of physical properties of the melt, necessary temperature and time parameters of the heat-resistant alloy’s melting accordingly. We have researched the temperature dependences of electrical resistance and kinematic viscosity of liquid heat-resistant composites based оn Ni – Nb – Cr – Mo systems. The critical temperatures were determined for the EP902 alloy. Heating up to these temperatures leads to irreversible changes in direction of the melt improving. Interaction was found between the amount of foundry waste and features of temperature dependences of the melt physico-chemical properties. An increase in the amount of foundry waste using in remelting results in the critical temperatures increasing. Influence of the melt conditions on crystallization process and on the structure of hard metal has been studied. The process of alloy EР902 solidification was researched by differential thermal analysis method. It has shown that the crystallization process starts with extraction of solid solution on the base of γ-phases and ends with forming of the eutectic based on the Ni3Nb intermetallic compound. Heating of the melt over the critical temperature leads to an increase of supercooling and does not effect on the eutectic temperature. The processing mode of the high temperature melt treatment was proposed based on the research results of physico-chemical properties of the liquid metal and process of the melt crystallization. It allows obtaining the highest quality of casting of heat-resistant EР902 alloy, which contains significant amount of foundry waste in the charge. The mechanical tests were implemented for experimental samples melted out by the optimal mode of high-temperature melt treatment (HTTM). Application of HTTM for the melts, contained 50 % of foundry waste in charge, allows obtaining the level of strength and plastic properties exceeding the technical requirements, stabilizing and combining it from melt to melt.

scholarly journals Reuse of Heat Resistant Glass Cullet in Cement Composites Subjected to Thermal Load

Materials ◽  
2020 ◽  
Vol 13 (19) ◽  
pp. 4434
Author(s):  
Aleksandra Powęzka ◽  
Jacek Szulej ◽  
Paweł Ogrodnik
Keyword(s):  
Compressive Strength ◽  
Chemical Properties ◽  
Cement Composite ◽  
Cement Composites ◽  
Thermal And Mechanical Properties ◽  
Glass Cullet ◽  
X Ray ◽  
Average Value ◽  
Heat Resistant ◽  
Physico Chemical

The article describes the possibility of using waste glass cullet as an alternative aggregate for the production of cement composites. Three concrete mixes based on Portland cement CEM I 42.5 R with different contents of recyclate were designed. Borosilicate glass cullet was introduced into the batch by reducing the content of natural aggregate by 0%, 2.5% and 7.5%. Apparent density, water absorption and compressive strength at elevated temperature were measured. The temperature distribution, in cubic samples, was followed by thermocouples. The elements were heated in a special furnace at the temperatures of 200 °C, 400 °C, 600 °C and 800 °C. The composite topography and phase composition were observed using X-ray energy scattering electron microscopy. The results show that the appropriate modification of the cement composite with 2.5% heat-resistant glass cullet improves both the thermal and mechanical properties. Compressive strength reaches an average value of 48.6 MPa after 28 days. The increase in temperature weakens the structure of the composite. It was found that the obtained cement composite has good physico–chemical properties. The research results are presented in the article.

scholarly journals PENGARUH VARIASI KONSENTRASI AMILUM JANTUNG PISANG BATU SEBAGAI BAHAN PENGIKAT TERHADAP SIFAT FISIK TABLET ASAM ASETIL SALISILAT

2021 ◽  
Vol 4 (2) ◽  
pp. 28-36
Author(s):  
Alex Sinaga ◽  
Adelya I Manalu
Keyword(s):  
Salicylic Acid ◽  
Active Substance ◽  
Resistant Starch ◽  
Dosage Form ◽  
Chemical Properties ◽  
Flow Time ◽  
Acetyl Salicylic Acid ◽  
Heat Resistant ◽  
Physico Chemical ◽  
Tablet Dosage

Tablet dosage form is one of the most widely used pharmaceutical. Acetyl salicylic acid is an anti inflammatory medicine, active substance not heat resistant. Starch as a binder of materials in the manufacture of tablets are hydrophilic because amylopectin starch can absorb most of the water. This study aims to determine the variation of the concentration of starch banana heart of stone as the material of binder on physico-chemical properties acid tablets acetyl salicylic meet the requirements of the Indonesian Pharmacopoeia. Based on the explanation above, the research conducted to make four concentration of the starch of banana, i.e. FI (5%), FII (10%), FIII (12.5%) and FIV (15%). From the results evaluation obtained include : flow time, steep angle, indication index, uniformity of weight, hardness, fragility and crumbling time of tablets, all formulas have been qualified by Pharmacopoeia Indonesia. Formulation IV after investigation had better tablet quality.

Decoration of specific sites on freeze-fractured membranes

1978 ◽  
Vol 36 (2) ◽  
pp. 140-141
Author(s):  
H. Gross ◽  
H. Moor
Keyword(s):  
Pure Water ◽  
Freeze Fracture ◽  
Chemical Properties ◽  
Surface Forces ◽  
Sulfate Pentahydrate ◽  
Copper Sulfate Pentahydrate ◽  
Physico Chemical ◽  
Water Of Hydration ◽  
Small Container ◽  
Binding Forces

Fracturing under ultrahigh vacuum (UHV, p ≤ 10-9 Torr) produces membrane fracture faces devoid of contamination. Such clean surfaces are a prerequisite foe studies of interactions between condensing molecules is possible and surface forces are unequally distributed, the condensate will accumulate at places with high binding forces; crystallites will arise which may be useful a probes for surface sites with specific physico-chemical properties. Specific “decoration” with crystallites can be achieved nby exposing membrane fracture faces to water vopour. A device was developed which enables the production of pure water vapour and the controlled variation of its partial pressure in an UHV freeze-fracture apparatus (Fig.1a). Under vaccum (≤ 10-3 Torr), small container filled with copper-sulfate-pentahydrate is heated with a heating coil, with the temperature controlled by means of a thermocouple. The water of hydration thereby released enters a storage vessel.

Physico-Chemical Properties of Recombinant Desulphatohirudin

1990 ◽  
Vol 63 (03) ◽  
pp. 499-504 ◽  
Author(s):  
A Electricwala ◽  
L Irons ◽  
R Wait ◽  
R J G Carr ◽  
R J Ling ◽  
...  
Keyword(s):  
Molecular Weight ◽  
Gel Filtration ◽  
Chemical Properties ◽  
Alpha Helix ◽  
Apparent Molecular Weight ◽  
Correlation Spectroscopy ◽  
Nmr Studies ◽  
Recombinant Hirudin ◽  
Physico Chemical ◽  
Recombinant Molecule

SummaryPhysico-chemical properties of recombinant desulphatohirudin expressed in yeast (CIBA GEIGY code No. CGP 39393) were reinvestigated. As previously reported for natural hirudin, the recombinant molecule exhibited abnormal behaviour by gel filtration with an apparent molecular weight greater than that based on the primary structure. However, molecular weight estimation by SDS gel electrophoresis, FAB-mass spectrometry and Photon Correlation Spectroscopy were in agreement with the theoretical molecular weight, with little suggestion of dimer or aggregate formation. Circular dichroism studies of the recombinant molecule show similar spectra at different pH values but are markedly different from that reported by Konno et al. (13) for a natural hirudin-variant. Our CD studies indicate the presence of about 60% beta sheet and the absence of alpha helix in the secondary structure of recombinant hirudin, in agreement with the conformation determined by NMR studies (17)

Physico-chemical properties of the rare-earth metals, scandium, and yttrium

1963 ◽  
Vol 79 (2) ◽  
pp. 263-293 ◽  
Author(s):  
E.M. Savitskii ◽  
V.F. Terekhova ◽  
O.P. Naumkin
Keyword(s):  
Rare Earth ◽  
Rare Earth Metals ◽  
Chemical Properties ◽  
Physico Chemical ◽  
The Rare Earth

Physico chemical properties and gas adsorption separation characteristics of Itaya zeolite and its modified products.

1990 ◽  
Vol 39 (442) ◽  
pp. 996-1000 ◽  
Author(s):  
Ayao TAKASAKA ◽  
Hideyuki NEMOTO ◽  
Hirohiko KONO ◽  
Yoshihiro MATSUDA
Keyword(s):  
Gas Adsorption ◽  
Chemical Properties ◽  
Physico Chemical

Development of Ketchup from Sudanese Red karkade (Hibiscus sabdariffa L.) byproduct

Food Biology ◽  
1970 ◽  
pp. 19-23
Author(s):  
Nawal Abdel-Gayoum Abdel-Rahman
Keyword(s):  
Sensory Quality ◽  
Chemical Properties ◽  
Storage Period ◽  
Gum Arabic ◽  
Raw Material ◽  
Soluble Solids ◽  
Hibiscus Sabdariffa ◽  
Overall Acceptability ◽  
Physico Chemical ◽  
Tomato Ketchup

The aim of this study is to use of karkede (Hibiscus sabdariffa L.) byproduct as raw material to make ketchup instead of tomato. Ketchup is making of various pulps, but the best type made from tomatoes. Roselle having adequate amounts of macro and micro elements, and it is rich in source of anthocyanine. The ketchup made from pulped of waste of soaked karkede, and homogenized with starch, salt, sugar, ginger (Zingiber officinale), kusbara (Coriandrum sativum) and gum Arabic. Then processed and filled in glass bottles and stored at two different temperatures, ambient and refrigeration. The total solids, total soluble solids, pH, ash, total titratable acidity and vitamin C of ketchup were determined. As well as, total sugars, reducing sugars, colour density, and sodium chloride percentage were evaluated. The sensory quality of developed product was determined immediately and after processing, which included colour, taste, odour, consistency and overall acceptability. The suitability during storage included microbial growth, physico-chemical properties and sensory quality. The karkede ketchup was found free of contaminants throughout storage period at both storage temperatures. Physico-chemical properties were found to be significantly differences at p?0.05 level during storage. There were no differences between karkade ketchup and market tomato ketchup concerning odour, taste, odour, consistency and overall acceptability. These results are encouraging for use of roselle cycle as a raw material to make acceptable karkade ketchup.

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