Synthesis, crystal structure and x-ray diffraction study of cuprous pivaloylisopropenylacetonate

1993 ◽  
Vol 33 (5) ◽  
pp. 743-746 ◽  
Author(s):  
I. A. Baidina ◽  
S. A. Gromilov ◽  
P. A. Stabnikov ◽  
S. A. Prokhorova ◽  
N. A. Bliznyuk ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Diffraction Study ◽  
X Ray Diffraction ◽  
X Ray

Powder X-ray diffraction study of disilver(1+) pentacyanonitrosylferrate(2−)

1999 ◽  
Vol 14 (3) ◽  
pp. 219-221 ◽  
Author(s):  
V. Venegas ◽  
A. Gómez ◽  
E. Reguera
Keyword(s):  
Crystal Structure ◽  
Thermogravimetric Analysis ◽  
Diffraction Study ◽  
Powder Diffraction ◽  
Lattice Parameters ◽  
X Ray Diffraction ◽  
Density Measurements ◽  
X Ray

The crystal structure of disilver(1+) pentacyanonitrosylferrate(2−) was studied by X-ray powder diffraction. IR and Mössbauer spectroscopies, thermogravimetric analysis and density measurements were also carried out. This compound is monoclinic, and its lattice parameters are: a=10.986(3) Å, b=6.4080(10) Å, c=7.4545(19) Å, α=δ=90°, β=102.54°(2).

Synthesis and Crystal Structure of the Triple-decker Complex [(η5-C5Me5)- Ru(μ,η5-1,3-C3B2Me5)RhCl- (Ph2PCH2)2]

2009 ◽  
Vol 64 (1) ◽  
pp. 141-144 ◽  
Author(s):  
Yong Nie ◽  
Thomas Oeser ◽  
Walter Siebert
Keyword(s):  
Crystal Structure ◽  
Single Crystal ◽  
Diffraction Study ◽  
X Ray Diffraction ◽  
Synthesis And Crystal Structure ◽  
X Ray

The dimer [(η5-C5Me5)Ru(C3B2Me5)RhCl]2 (2) reacts with 1,2-bis(diphenylphosphino)ethane (dppe) to give the triple-decker complex [(η5-C5Me5)Ru(C3B2Me5)Rh- (dppe)Cl] (3). Its constitution follows from NMR and MS data, and a single-crystal X-ray diffraction study.

scholarly journals Crystal structure and high temperature X-ray diffraction study of thermoelectric chimney-ladder FeGe (γ ≈ 1.52)

2020 ◽  
Vol 846 ◽  
pp. 155696
Author(s):  
Sylvain Le Tonquesse ◽  
Christopher Hassam ◽  
Yuichi Michiue ◽  
Yoshitaka Matsushita ◽  
Mathieu Pasturel ◽  
...  
Keyword(s):  
Crystal Structure ◽  
High Temperature ◽  
Diffraction Study ◽  
X Ray Diffraction ◽  
X Ray

NEUTRON DIFFRACTION STUDY ON (Bi−Pb)2Sr2Ca2Cu3O10

1990 ◽  
Vol 04 (12) ◽  
pp. 791-794 ◽  
Author(s):  
YANG JI-LIAN ◽  
YE CHUN-TANG ◽  
ZHANG BAI-SHENG ◽  
LI JI-ZHOU ◽  
KANG JIAN ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Neutron Diffraction ◽  
Diffraction Study ◽  
Single Phase ◽  
Polycrystalline Sample ◽  
Neutron Diffraction Study ◽  
Structure Study ◽  
X Ray Diffraction ◽  
Space Group ◽  
X Ray

The polycrystalline sample of (Bi–Pb)2Sr2Ca2Cu3O10 with Tc=107 K was prepared. The X-ray diffraction proved that the sample is single phase. The crystal structure study on the sample has been carried out by neutron diffraction. The result shows that its structure is tetragonal body-centre structure with space group of I4/mmm, containing a few oxygen atoms at 4e site in Bi–Pb layers.

Neutron and X-Ray Diffraction Study of the Crystal Structure of CsTiSi2O6.5

1997 ◽  
Vol 130 (1) ◽  
pp. 97-102 ◽  
Author(s):  
M.L. Balmer ◽  
Q. Huang ◽  
W. Wong-Ng ◽  
R.S. Roth ◽  
A. Santoro
Keyword(s):  
Crystal Structure ◽  
Diffraction Study ◽  
X Ray Diffraction ◽  
X Ray

Molecular conformation of di-o-anisylcarbinol: an X-ray diffraction study

1983 ◽  
Vol 61 (9) ◽  
pp. 2001-2005 ◽  
Author(s):  
C. Faerman ◽  
H. Negri ◽  
G. Punte ◽  
A. A. Vitale ◽  
N. S. Nudelman
Keyword(s):  
Crystal Structure ◽  
Single Crystal ◽  
Diffraction Study ◽  
Molecular Conformation ◽  
Direct Methods ◽  
X Ray Diffraction ◽  
X Ray ◽  
Triclinic System ◽  
Phenyl Rings ◽  
R Factors

Di-o-anisylcarbinol crystallizes in the triclinic system, space group [Formula: see text] with a = 7.50 (4), b = 10.89 (4), c = 7.98 (3) Å, α = 101.9 (1), β = 94.1 (1), γ = 94.6 (1)°, Z = 2, V = 633.11 Å3, Dc = 1.28 mg m−3, Dm = 1.26 (1) mg m−3, CuKα radiation, λ = 1.54178 Å, μ(CuKα) = 0.633 mm−1, F(000) = 260. The structure has been determined by direct methods using single crystal X-ray data and refined by least-squares to the final R factors R = 5.89% and Rw = 5.35%. The molecule has a twist-skewed conformation with the phenyl rings on nearly orthogonal planes. The crystal structure shows a hydrogen-bonded dimer and a peculiar arrangement of the methoxy and phenyl groups.

Röntgenstrukturbestimmung von AlCl3-Pyridin-Addukten: Der strukturelle Aufbau im trans-Dichlorotetrakis(pyridin)aluminium(III)- Tetrachloroaluminat(III) und im Trichlorotris(pyridin)aluminium(III) / X-ray Diffraction Study of AICl3-Pyridine Adducts: The Crystal Structure of trans-Dichlorotetrakis(pyridine)aluminium(III)tetrachloroaluminat(III) and of Trichlorotris(pyridine)aluminium(III)

1982 ◽  
Vol 37 (10) ◽  
pp. 1312-1315 ◽  
Author(s):  
Peter Pullmann ◽  
Karl Hensen ◽  
Jan W. Bats
Keyword(s):  
Crystal Structure ◽  
Least Squares ◽  
Diffraction Study ◽  
X Ray Diffraction ◽  
Full Matrix ◽  
X Ray ◽  
The Mean

Abstract Crystals of [Al(C5H5N)4Cl2][AlCl4] are orthorhombic, Pna21, Z = 4, a = 18.522(7), b = 15.141(5), c = 9.593(3) Å, V = 2690(2) Å3 , Dc = 1.440 g/cm3 . The structure has been solved from 5968 diffractometer measured intensities and refined by full-matrix least squares to Rw(F) = 0.032. The crystal structure shows the complex to be trans-dichloro-tetrakis(pyridine)aluminium(III) tetrachloroaluminat(III). The mean trans Al-Cl-and trans Al-N-distances in the octahedron are 2.279(3) and 2.070(4) Å, respectively. Crystals of Al(C5H5N)3Cl3 are monoclinic, P21/c, Z = 4, a = 7.261(2), b = 29.961(4), c = 8.624(1) Å, β = 98.12(2)°, V -1857(1) Å3 , DC = 1.326 g/cm3 . The structure has been solved from 4707 diffractometer measured intensities and refined to Rw(F) = 0.028. The crystal structure shows octahedral complexes AlCl3·3 (C5H5N) with trans geometry. The Al-N-distance trans to chlorine (2.096(2) Å) is significantly longer than the two other Al-N-distances (mean 2.072(2) Å).

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