Study of metastable superconducting detector response to irradiation using SQUID-readout

1993 ◽  
Vol 93 (3-4) ◽  
pp. 467-472
Author(s):  
TA Girard ◽  
J. M. Tavares ◽  
M. Godinho ◽  
R. P. Henriques ◽  
G. Bonfait ◽  
...  
Keyword(s):  
Detector Response ◽  
Superconducting Detector ◽  
Squid Readout

Flame ionization detector response to coeluting hydrocarbons and carbon disulphide and its application to the determination of the sum of C6-C11 alkanes and cycloalkanes in air

1983 ◽  
Vol 48 (3) ◽  
pp. 722-734
Author(s):  
Martin Koval
Keyword(s):  
Carbon Disulphide ◽  
Internal Standard ◽  
Calibration Procedure ◽  
Detector Response ◽  
Column Temperature ◽  
Flame Ionization ◽  
Other Substances ◽  
Flame Ionisation Detector ◽  
Ionisation Detector

The flame ionisation detector response to C6-C11 aliphatic hydrocarbon solutions in carbon disulphide in the concentration range between 1.3-9.5 mg ml-1 retained lineary despite the excess of solvent entering the detector simultaneously with the analyte. Pure carbon disulphide exhibited a small positive detector response which did not interfere in calibration procedure and which, under certain GC conditions, inverted to negative values. This response was not proportional to the injected volume and was strongly influenced by the column temperature and/or bleed. On the basis of these findings, a method compatible with the widely used charcoal tube carbon disulphide desorption procedure was developed and evaluated. It consists of static desorption of the sum of aliphatic alkanes and cycloalkanes from the activated charcoal after which an internal standard is added to the supernatant eluate. The resulting carbon disulphide solution is analysed on a highly polar stationary phase 1,2,3-tris(2-cyanoethoxy)propane where the solvent and the analyte coelute in a single peak, the height of which is practically proportional to the sum of alkanes and cycloalkanes present. This also makes determinations of other substances present in the sample more simple. The field test of the proposed method yielded values comparable in precision and accuracy with a control infrared spectrophotometric method.

Screening and quantification of hypnotic sedatives in serum by capillary gas chromatography with a nitrogen-phosphorus detector, and confirmation by capillary gas chromatography-mass spectrometry.

1986 ◽  
Vol 32 (2) ◽  
pp. 325-328 ◽  
Author(s):  
V A Soo ◽  
R J Bergert ◽  
D G Deutsch
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Capillary Gas Chromatography ◽  
Gas Chromatography Mass Spectrometry ◽  
Detector Response ◽  
Capillary Gc ◽  
Chromatography Mass Spectrometry ◽  
Nitrogen Phosphorus Detector ◽  
Sedative Drugs ◽  
Nitrogen Phosphorus

Abstract We describe a quantitative screen for hypnotic-sedative drugs in which we use capillary gas chromatography with a nitrogen-phosphorus detector (GC/NPD) as the primary method and capillary gas chromatography-mass spectrometry (GC-MS) for confirmation. GC retention times of the acid-extracted underivatized drugs were stable (CVs less than 1%), and the detector response varied linearly over a 20-fold concentration range with a mean correlation coefficient for 11 drugs of 0.989. The limits of detection were satisfactory (0.5 mg/L in a 0.5-mL serum sample and 1-microL injection volume), as were precision (average CV 5.2% within day, 6.4% between day). The complementary use of capillary GC-MS not only unambiguously confirms presumptive peaks identified by GC, but also prevents reports of false positives and identifies compounds not included in the quantitative GC screen that may be listed in the GC-MS library.

Detector response and calibration of the cosmic-ray detector of the Sileye-3/Alteino experiment

2006 ◽  
Vol 37 (9) ◽  
pp. 1691-1696 ◽  
Author(s):  
M. Casolino ◽  
V. Bidoli ◽  
M. Minori ◽  
L. Narici ◽  
M.P. De Pascale ◽  
...  
Keyword(s):  
Cosmic Ray ◽  
Detector Response

scholarly journals New Results on Radioactive Mixture Identification and Relative Count Contribution Estimation

Sensors ◽  
2021 ◽  
Vol 21 (12) ◽  
pp. 4155
Author(s):  
Bulent Ayhan ◽  
Chiman Kwan
Keyword(s):  
Deep Learning ◽  
Noise Source ◽  
Simulated Data ◽  
Nuclear Material ◽  
Machine Learning Algorithms ◽  
Detector Response ◽  
Nuclear Materials ◽  
Ratio Estimation ◽  
Analysis Software ◽  
Detector Distance

Detecting nuclear materials in mixtures is challenging due to low concentration, environmental factors, sensor noise, source-detector distance variations, and others. This paper presents new results on nuclear material identification and relative count contribution (also known as mixing ratio) estimation for mixtures of materials in which there are multiple isotopes present. Conventional and deep-learning-based machine learning algorithms were compared. Realistic simulated data using Gamma Detector Response and Analysis Software (GADRAS) were used in our comparative studies. It was observed that a deep learning approach is highly promising.

scholarly journals SiLiF Neutron Counters to Monitor Nuclear Materials in the MICADO Project

Sensors ◽  
2021 ◽  
Vol 21 (8) ◽  
pp. 2630
Author(s):  
Luigi Cosentino ◽  
Quentin Ducasse ◽  
Martina Giuffrida ◽  
Sergio Lo Meo ◽  
Fabio Longhitano ◽  
...  
Keyword(s):  
Radioactive Waste ◽  
Detector Response ◽  
Nuclear Materials ◽  
Spent Fuel ◽  
Neutron Detectors ◽  
Intermediate Level Radioactive Waste ◽  
Eu Project ◽  
Interim Storage ◽  
Waste Drums

In the framework of the MICADO (Measurement and Instrumentation for Cleaning And Decommissioning Operations) European Union (EU) project, aimed at the full digitization of low- and intermediate-level radioactive waste management, a set of 32 solid state thermal neutron detectors named SiLiF has been built and characterized. MICADO encompasses a complete active and passive characterization of the radwaste drums with neutrons and gamma rays, followed by a longer-term monitoring phase. The SiLiF detectors are suitable for the monitoring of nuclear materials and can be used around radioactive waste drums possibly containing small quantities of actinides, as well as around spent fuel casks in interim storage or during transportation. Suitable polyethylene moderators can be exploited to better shape the detector response to the expected neutron spectrum, according to Monte Carlo simulations that were performed. These detectors were extensively tested with an AmBe neutron source, and the results show a quite uniform and reproducible behavior.

Superconducting Detector Magnet for BabyIAXO

2021 ◽  
Vol 31 (5) ◽  
pp. 1-5
Author(s):  
Nikolay Bykovskiy ◽  
Alexey Dudarev ◽  
Helder Pais Da Silva ◽  
Patricia Borges de Sousa ◽  
Matthias Mentink ◽  
...  
Keyword(s):  
Superconducting Detector

scholarly journals Simultaneous Determination of Human Serum Albumin and Low-Molecular-Weight Thiols after Derivatization with Monobromobimane

Molecules ◽  
2021 ◽  
Vol 26 (11) ◽  
pp. 3321
Author(s):  
Katarzyna Kurpet ◽  
Rafał Głowacki ◽  
Grażyna Chwatko
Keyword(s):  
Molecular Weight ◽  
Human Serum Albumin ◽  
Serum Albumin ◽  
Human Serum ◽  
Simultaneous Determination ◽  
Reversed Phase ◽  
Fluorescence Labeling ◽  
Detector Response ◽  
Low Molecular Weight

Biothiols are extremely powerful antioxidants that protect cells against the effects of oxidative stress. They are also considered relevant disease biomarkers, specifically risk factors for cardiovascular disease. In this paper, a new procedure for the simultaneous determination of human serum albumin and low-molecular-weight thiols in plasma is described. The method is based on the pre-column derivatization of analytes with a thiol-specific fluorescence labeling reagent, monobromobimane, followed by separation and quantification through reversed-phase high-performance liquid chromatography with fluorescence detection (excitation, 378 nm; emission, 492 nm). Prior to the derivatization step, the oxidized thiols are converted to their reduced forms by reductive cleavage with sodium borohydride. Linearity in the detector response for total thiols was observed in the following ranges: 1.76–30.0 mg mL−1 for human serum albumin, 0.29–5.0 nmol mL−1 for α-lipoic acid, 1.16–35 nmol mL−1 for glutathione, 9.83–450.0 nmol mL−1 for cysteine, 0.55–40.0 nmol mL−1 for homocysteine, 0.34–50.0 nmol mL−1 for N-acetyl-L-cysteine, and 1.45–45.0 nmol mL−1 for cysteinylglycine. Recovery values of 85.16–119.48% were recorded for all the analytes. The developed method is sensitive, repeatable, and linear within the expected ranges of total thiols. The devised procedure can be applied to plasma samples to monitor biochemical processes in various pathophysiological states.

Space to Air High-Altitude Region Adjoint Neutron Transport

2021 ◽  
pp. 154851292110316
Author(s):  
Zachary W LaMere ◽  
Darren E Holland ◽  
Whitman T Dailey ◽  
John W McClory
Keyword(s):  
Energy Spectrum ◽  
High Altitude ◽  
Neutron Energy ◽  
Neutron Transport ◽  
Energy Sources ◽  
Source Spectrum ◽  
Detector Response ◽  
Neutron Energy Spectrum ◽  
True Source ◽  
Adjoint Transport

Neutrons from an atmospheric nuclear explosion can be detected by sensors in orbit. Current tools for characterizing the neutron energy spectrum assume a known source and use forward transport to recreate the detector response. In realistic scenarios the true source is unknown, making this an inefficient, iterative approach. In contrast, the adjoint approach directly solves for the source spectrum, enabling source reconstruction. The time–energy fluence at the satellite and adjoint transport equation allow a Monte Carlo method to characterize the neutron source’s energy spectrum directly in a new model: the Space to High-Altitude Region Adjoint (SAHARA) model. A new adjoint source event estimator was developed in SAHARA to find feasible solutions to the neutron transport problem given the constraints of the adjoint environment. This work explores SAHARA’s development and performance for mono-energetic and continuous neutron energy sources. In general, the identified spectra were shifted towards energies approximately 5% lower than the true source spectra, but SAHARA was able to capture the correct spectral shapes. Continuous energy sources, including real-world sources Fat Man and Little Boy, resulted in identifiable spectra that could have been produced by the same distribution as the true sources as demonstrated by two-dimensional (2D) Kolmogorov–Smirnov tests.

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