Consecutive determination of nitrogen, phosphorus and calcium in animal feeds on a single channel flow injection analyzer with a common analytical manifold

1982 ◽  
Vol 311 (1) ◽  
pp. 23-26 ◽  
Author(s):  
W. D. Basson
2000 ◽  
Vol 83 (6) ◽  
pp. 1293-1298 ◽  
Author(s):  
Jing-Fu Liu ◽  
Gui-Bin Jiang ◽  
Ying-Di Feng

Abstract A rapid and simple procedure was developed for the determination of copper, iron, manganese, and zinc in animal feeds using an identical flow injection spectrophotometric manifold but different chromogenic reagents and different detection wavelengths. Bis(cyclohexanone)oxalydihydrazone, formaldoxime, 1,10-phenanthroline, and xylenol orange were adopted as chromogenic reagents for Cu, Mn, Fe, and Zn, respectively. Detection conditions such as manifold parameters, buffer pH, reagent concentration, temperature, and acidity of sample solution were optimized. Analytical characteristics of the method and interference of metal ions commonly present in feeds were studied. By changing the reagents and detection wavelengths, which can be done quickly, the proposed low cost flow injection system can determine Cu, Fe, Mn, or Zn in the range of 0.5–10 mg/L with a sampling throughput of 120/h.


1989 ◽  
Vol 11 (2) ◽  
pp. 87-88 ◽  
Author(s):  
Sveinbjörn Gizurarson

The applicability of a single-channel flow-injection system with immobilized enzyme coil (Technicon) and UV detection to the determination of glucose is described. The method was used for a pure glucose solution and for serum. The detection limit was 0.10 mM, the rate of determination was 20-40 per hour and the precision was satisfactory. The system is very simple and practical when many analysis are to be determined periodically.


The Analyst ◽  
1977 ◽  
Vol 102 (1219) ◽  
pp. 714 ◽  
Author(s):  
E. H. Hansen ◽  
F. J. Krug ◽  
Animesh K. Ghose ◽  
J. Růžička

1990 ◽  
Vol 73 (3) ◽  
pp. 389-393
Author(s):  
R Martinez-Avila ◽  
V Carbonell ◽  
M De la guardia ◽  
A Salvador

Abstract The direct introduction of slurries in flow Injection-flame atomic absorption spectroscopy has been studied using a single-channel manifold. The influence of flow Injection parameters on the sensitivity and accuracy of this procedure has been established. A method has been developed for the determination of copper, manganese, and lead In sewage sludge where batch digestion of the samples In a microwave oven is carried out before dilution. Both sensitivity and limit of detection of the flow Injection analysis procedure are adequate for the analysis of actual samples (the limit of detection was 0.06, 0.05, and 0.3 ppm for copper, manganese, and lead, respectively). The accuracy of the proposed method, determined from the analysis of 2 reference samples from the European Community Bureau, is better than that obtained by the continuous aspiration of the samples.


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