Masking effect of potassium iodide on the interferences in the atomic-absorption spectrophotometric determination of antimony utilizing stibine generation by sodium borohydride tablet reduction

1981 ◽  
Vol 305 (1) ◽  
pp. 11-14 ◽  
Author(s):  
Manabu Yamamoto ◽  
Tadashi Shohji ◽  
Takahiro Kumamaru ◽  
Yuroku Yamamoto
Keyword(s):  
Atomic Absorption ◽  
Spectrophotometric Determination ◽  
Potassium Iodide ◽  
Sodium Borohydride ◽  
Masking Effect

Comparison of Methods for Determining Biuret in Urea

1979 ◽  
Vol 62 (1) ◽  
pp. 153-159
Author(s):  
Luis F Corominas ◽  
Victor M Boy ◽  
Manuel Guijosa
Keyword(s):  
Atomic Absorption ◽  
Spectrophotometric Determination ◽  
Atomic Absorption Spectrophotometry ◽  
International Organization ◽  
Comparison Of Methods ◽  
Definite Advantage ◽  
Absorption Spectrophotometry ◽  
Alternative Procedures ◽  
Aoac Method

Abstract The official first action AOAC method for the spectrophotometric determination of biuret in urea, 2.072—2.074, was compared with official first action AOAC method 2.C01-2.C03 (atomic absorption spectrophotometry), 2 simplified versions of 2.072-2.074, and modified versions of 2 alternative procedures of the International Organization for Standardization. Three synthetic urea samples (0.3, 1.4, and 3.0% biuret) and 1 commercial urea sample (1.0% biuret) were analyzed. The methods proved to be equivalent and none showed a definite advantage over 2.072-2.074. The purification of biuret and the interference by ammonia are also discussed.

Extraction-atomic-absorption spectrophotometric determination of antimony by generation of its hydride in non-aqueous media

The Analyst ◽  
1984 ◽  
Vol 109 (2) ◽  
pp. 123-125 ◽  
Author(s):  
José Aznárez ◽  
Francisco Palacios ◽  
Maria S. Ortega ◽  
Juan Carlos Vidal
Keyword(s):  
Atomic Absorption ◽  
Spectrophotometric Determination ◽  
Aqueous Media
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