Preparation and optical properties of Bi2S3 microcrystallite doped glass and thin film by the sol-gel process

1994 ◽  
Vol 3 (3) ◽  
pp. 235-239 ◽  
Author(s):  
Ye Hui ◽  
He Dijie ◽  
Jiang Zhonghong ◽  
Ding Yong
2012 ◽  
Vol 581-582 ◽  
pp. 514-518
Author(s):  
Hong Zhu ◽  
Zhi Jun Guo ◽  
Wein Duo Yang ◽  
Wein Feng Chang

This study investigated the structure, microstructure and optical properties of the highly-oriented lead barium titanate (Pb1-xBaxTiO3, PBT) thin films prepared on MgO (100) substrate by a nonaqueous sol-gel process. The film precursor was synthesized by the modified sol-gel processing from lead acetate, barium acetate, and titanium isopropoxide, acetylacetone as chelating agent, and ethylene glycol as solvent. This stable precursor was formed by acetylacetone chelating with titanium isopropoxide and then mixing the solution of the acetates. The spin-coating technique was used to deposit the PBT films on MgO (100) substrate with different barium contents and various spin-coating numbers, respectively. X-ray diffraction was employed to study the crystal structure of the thin film and field emission scanning electron microscopy was used to characterize the microstructure of the films. Optical properties of the thin films were investigated by Ultraviolet-visible spectrophotometer. All films exhibited a (100) preferred orientation, especially the PB0.5T (3-coating layers) thin film. In the optical properties, the adsorption wavelength shifted to the ultraviolet region with increasing barium.


1999 ◽  
Vol 606 ◽  
Author(s):  
Keishi Nishio ◽  
Jirawat Thongrueng ◽  
Yuichi Watanabe ◽  
Toshio Tsuchiya

AbstructWe succeeded in the preparation of strontium-barium niobate (Sr0.3Ba0.7Nb2O6 : SBN30)that have a tetragonal tungsten bronze type structure thin films on SrTiO3 (100), STO, or La doped SrTiO3 (100), LSTO, single crystal substrates by a spin coating process. LSTO substrate can be used for electrode. A homogeneous coating solution was prepared with Sr and Ba acetates and Nb(OEt)5 as raw materials, and acetic acid and diethylene glycol monomethyl ether as solvents. The coating thin films were sintered at temperature from 700 to 1000°C for 10 min in air. It was confirmed that the thin films on STO substrate sintered above 700°C were in the epitaxial growth because the 16 diffraction spots were observed on the pole figure using (121) reflection. The <130> and <310> direction of the thin film on STO were oriented with the c-axis in parallel to the substrate surface. However, the diffraction spots of thin film on LSTO substrate sintered at 700°C were corresponds to the expected pattern for (110).


2011 ◽  
Vol 509 (30) ◽  
pp. 7854-7860 ◽  
Author(s):  
A. Esmaielzadeh Kandjani ◽  
M. Farzalipour Tabriz ◽  
O. Mohammad Moradi ◽  
H.R. Rezaeian Mehr ◽  
S. Ahmadi Kandjani ◽  
...  

1991 ◽  
Vol 74 (1) ◽  
pp. 238-240 ◽  
Author(s):  
Masayuki Nogami ◽  
Yi-Qing Zhu ◽  
Yoshihide Tohyama ◽  
Katsumi Nagasaka ◽  
Takashi Tokizaki ◽  
...  

2014 ◽  
Vol 989-994 ◽  
pp. 656-659
Author(s):  
Ping Cao ◽  
Yue Bai

Al co-doped ZnCoO thin film has been prepared by a sol-gel method. The structural and optical properties of the sample were investigated. X-ray diffraction and UV absorption spectroscopy analyses indicate that Al3+ and Co2+ substitute for Zn2+ without changing the wurtzite structure. With the Al doping, the visible emission increased and the UV emission decreased, which is attributed to the increase of O vacancies and Zn interstitials.


1999 ◽  
Author(s):  
Qing Xiang ◽  
Yan Zhou ◽  
Yee Loy Lam ◽  
Boon Siew Ooi ◽  
Yuen Chuen Chan ◽  
...  

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