Application of a fast X-ray diffraction method for studies of high temperature corrosion of steel surfaces

1991 ◽  
Vol 341 (5-6) ◽  
pp. 436-438 ◽  
Author(s):  
V. Kolarik ◽  
M. Juez-Lorenzo ◽  
W. Engel ◽  
N. Eisenreich
Keyword(s):  
High Temperature ◽  
Diffraction Method ◽  
High Temperature Corrosion ◽  
X Ray Diffraction ◽  
X Ray ◽  
Steel Surfaces ◽  
Corrosion Of Steel

High Temperature Corrosion Kinetics using a Fast X-Ray Diffraction Method

1991 ◽  
Vol 79-82 ◽  
pp. 617-622
Author(s):  
Vladislav Kolarik ◽  
Maria Juez-Lorenzo ◽  
N. Eisenreich ◽  
W. Engel
Keyword(s):  
High Temperature ◽  
Diffraction Method ◽  
High Temperature Corrosion ◽  
X Ray Diffraction ◽  
X Ray ◽  
Corrosion Kinetics

scholarly journals In-situ study of high temperature corrosion kinetics of iron using a fast X-ray diffraction method

1993 ◽  
Vol 03 (C9) ◽  
pp. C9-461-C9-467 ◽  
Author(s):  
M. Juez-Lorenzo ◽  
V. Kolarik ◽  
N. Eisenreich ◽  
W. Engel ◽  
A. J. Criado
Keyword(s):  
High Temperature ◽  
Diffraction Method ◽  
High Temperature Corrosion ◽  
X Ray Diffraction ◽  
X Ray ◽  
In Situ Study ◽  
Corrosion Kinetics ◽  
Kinetics Of

scholarly journals High temperature corrosion kinetics by a fast X-ray diffraction method applied to nickel

1993 ◽  
Vol 03 (C9) ◽  
pp. C9-447-C9-452 ◽  
Author(s):  
V. Kolarik ◽  
M. Juez-Lorenzo ◽  
N. Eisenreich ◽  
W. Engel
Keyword(s):  
High Temperature ◽  
Diffraction Method ◽  
High Temperature Corrosion ◽  
X Ray Diffraction ◽  
X Ray ◽  
Corrosion Kinetics

High temperature corrosion behaviour of aluminised FC 25 cast iron using pack cementation

2019 ◽  
Vol 66 (2) ◽  
pp. 236-241 ◽  
Author(s):  
Somrerk Chandra-Ambhorn ◽  
Neramit Krasaelom ◽  
Tummaporn Thublaor ◽  
Sirichai Leelachao
Keyword(s):  
Cast Iron ◽  
High Temperature ◽  
Corrosion Behaviour ◽  
Mass Gain ◽  
High Temperature Corrosion ◽  
Pack Cementation ◽  
X Ray Diffraction ◽  
Content Type ◽  
X Ray ◽  
Seat Insert

Purpose This study aims to apply the pack cementation to develop the Fe-Al layers on the surface of FC 25 cast iron in order to increase the high-temperature corrosion resistance of the alloy. Design/methodology/approach Pack cementation was applied on the surface of FC 25 cast iron at 1,050°C. The bare and aluminised alloys were subjected to the oxidation test in 20 per cent O2-N2 at 850 °C. Scanning electron microscopy equipped with energy-dispersive X-ray spectroscopy and X-ray diffraction (XRD) were used for characterisation. Findings The layers of pack cementation consisted of Fe2Al5, FeAl2 and FeAl, and solid solution alloyed with Al. The oxidation kinetics of the bare cast iron was parabolic. Mass gain of the aluminised cast iron was significantly decreased compared with that of the bare cast iron. This was because of the protective alumina formation on the aluminised alloy surface. Al in the Fe–Al layer also tended to be homogenised during oxidation. Originality/value Even though the aluminising of alloys was extensively studied, the application of that process to the FC 25 cast iron grade was originally developed in this work. The significantly reduced mass gain of the aluminised FC 25 cast iron makes the studied alloy be promising for the use as a valve seat insert in an agricultural single-cylinder four-stroke engine, which might be run by using a relatively cheaper fuel, i.e. LPG, but as a consequence requires the higher oxidation resistance of the engine parts.

INVESTIGATION ON HIGH-TEMPERATURE CORROSION BEHAVIOR OF INCONEL 600 UNDER SO2-BEARING GAS AT 650°C

2019 ◽  
Vol 27 (06) ◽  
pp. 1950155
Author(s):  
KWANG-HU JUNG ◽  
SEONG-JONG KIM
Keyword(s):  
Electron Microscope ◽  
Weight Gain ◽  
High Temperature ◽  
Scanning Electron Microscope ◽  
High Temperature Corrosion ◽  
X Ray Diffraction ◽  
Oxide Structure ◽  
X Ray ◽  
Inconel 600 ◽  
Scanning Electron

The corrosion characteristics of Inconel 600 were investigated at 650∘C in air and 76%[Formula: see text]%[Formula: see text]%[Formula: see text]%SO2 gas environment up to 500[Formula: see text]h. Specimens exposed to each condition were characterized by weight gain, scanning electron microscope, energy dispersive X-ray spectroscopy and X-ray diffraction. The oxide structure consisting of the thin Cr2O3 layer and Cr2O3 nodules was observed, which increased the weight gain of specimens. In the SO2-bearing gas, it showed a bigger weight gain due to the coarsening of Cr2O3 nodules. Therefore, it was suggested that the sulfur-accelerated coarsening of Cr2O3 nodules at the high temperature.

Assessment of Fatigue Life for High-Temperature Pipeline Welds Using X-Ray Diffraction Technique

2007 ◽  
Vol 353-358 ◽  
pp. 130-133
Author(s):  
Keun Bong Yoo ◽  
Jae Hoon Kim
Keyword(s):  
High Temperature ◽  
Fatigue Life ◽  
Fatigue Damage ◽  
Power Plants ◽  
Low Cycle Fatigue ◽  
Diffraction Method ◽  
Life Assessment ◽  
Fatigue Properties ◽  
X Ray Diffraction ◽  
X Ray

The objective of this study is to examine the feasibility of the X-ray diffraction method for the fatigue life assessment of high-temperature steel pipes used for main steam pipelines, re-heater pipelines and headers etc. in power plants. In this study, X-ray diffraction tests were performed on the specimens simulated for low cycle fatigue damage, in order to estimate fatigue properties at the various stages of fatigue life. As a result of X-ray diffraction tests, it was confirmed that the full width at the half maximum (FWHM) decreased with an increase in the fatigue life ratio, and that the FWHM and the residual stress due to fatigue damage were algebraically linearly related to the fatigue life ratio. From this relationship, a direct assessment of the remaining fatigue life was feasible.

Polymorphic transformations and thermal expansion of some modifications in Ag1.5Cu0.5Se and Ag0.4Cu1.6Se

2019 ◽  
Vol 33 (23) ◽  
pp. 1950271 ◽  
Author(s):  
Y. I. Aliyev ◽  
Y. G. Asadov ◽  
A. O. Dashdemirov ◽  
R. D. Aliyeva ◽  
T. G. Naghiyev ◽  
...  
Keyword(s):  
Thermal Expansion ◽  
High Temperature ◽  
Temperature Dependence ◽  
Single Crystals ◽  
Diffraction Method ◽  
Lattice Parameters ◽  
X Ray Diffraction ◽  
Polymorphic Transformations ◽  
X Ray

The Ag[Formula: see text]Cu[Formula: see text]Se and Ag[Formula: see text]Cu[Formula: see text]Se compounds have been synthesized and grown as single crystals. High-temperature X-ray diffraction method was used to study polymorphic transformations. It is shown that the Ag[Formula: see text]Cu[Formula: see text]Se crystals of high-temperature FCC modification are decomposed into Ag2Se and AgCuSe when the temperature decreases below T = 488 K and Ag[Formula: see text]Cu[Formula: see text]Se is decomposed into Cu2Se and AgCuSe when the temperature decreases below T = 540 K. Transformations in both compounds are reversible. Crystalline parameters are obtained and the temperature dependence of the lattice parameters for each phase is built.

High-Temperature Corrosion of Copper Induced by TeO2

CORROSION ◽  
10.5006/3295 ◽  
2020 ◽  
Vol 76 (2) ◽  
pp. 210-216
Author(s):  
Anton Klimashin
Keyword(s):  
High Temperature ◽  
Phase Distribution ◽  
Copper Ion ◽  
High Temperature Corrosion ◽  
Corrosion Layer ◽  
Corrosion Process ◽  
Ion Conductivity ◽  
X Ray Diffraction ◽  
X Ray ◽  
Oxide Melt

It was found that copper is susceptible to the accelerated high-temperature corrosion induced by TeO2 at 650°C in air, which occurs at a constant rate. The calculated corrosion rate constant is 4.5 × 10−4 kg·m−2·s−1 and does not depend on the specific mass of tellurium oxide. Based on the results of the analysis of the microstructure (scanning electron microscopy/energy dispersive x-ray spectroscopy) and the phase composition (x-ray diffraction) of two formed corrosion layers, the phase distribution in the corrosion product has been ascertained. It was shown that during the corrosion process at 650°С, the inner corrosion layer containing Cu2O and Cu2Te and the outer corrosion layer mainly containing CuTe2O5 and Cu2O were formed. The inner layer provides a high copper ion conductivity due to Cu2Te, while the outer layer possesses a high oxygen ion conductivity due to the oxide melt. The mechanism of the overall corrosion process has been proposed.

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