Facile Synthesis and Crystal Structure of 1,1,1,3-Tetranitro-3-azabutane

2008 ◽  
Vol 634 (8) ◽  
pp. 1244-1246 ◽  
Author(s):  
Thomas M. Klapötke ◽  
Burkhard Krumm ◽  
Matthias Scherr ◽  
Gunnar Spieß ◽  
F. Xaver Steemann
Keyword(s):  
Crystal Structure ◽  
Facile Synthesis ◽  
Synthesis And Crystal Structure

scholarly journals Microwave-Assisted Facile Synthesis and Crystal Structure of cis-9,10,11,15-Tetrahydro-9,10[3′,4′]-furanoanthracene-12,14-dione.

ChemInform ◽  
2006 ◽  
Vol 37 (34) ◽  
Author(s):  
Weerachai Phutdhawong ◽  
Duang Buddhasukh ◽  
Stephen G. Pyne ◽  
Apinpus Rujiwatra ◽  
Chaveng Pakawatchai
Keyword(s):  
Crystal Structure ◽  
Facile Synthesis ◽  
Synthesis And Crystal Structure ◽  
Microwave Assisted

Facile Synthesis and Crystal Structure of [(PhSO2 N)2 WVI Cl2 (CH3CN)2] - the Oxidative Imination of W(CO)6 by N,N-Dichlorophenylsulphonamide

1985 ◽  
Vol 40 (6) ◽  
pp. 736-739 ◽  
Author(s):  
Herbert W. Roesky ◽  
Jörg Sundermeyer, ◽  
Jürgen Schimkowiak ◽  
Peter G. Jones ◽  
Mathias Noltemeyer ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Good Yield ◽  
Polymeric Complex ◽  
Facile Synthesis ◽  
Triclinic Space Group ◽  
Synthesis And Crystal Structure ◽  
Tungsten Hexacarbonyl ◽  
Space Group

AbstractThe reaction of N,N-dichlorophenylsulphonamide with tungsten hexacarbonyl in refluxing CCl4 leads in good yield to the yellow polymeric complex [(PhSO2N)2WCl2]x, which may be converted to the octahedral nitrene complex [(PhSO2N)2WCl2(CH3CN)2] by recrystallisation from aceto­nitrile. Crystals of the acetonitrile complex are triclinic, space group P 1̅, a = 820.7(2), b = 1128.8(3), c = 1286.9(3) pm, α = 89.25(3), β = 89.54(3). γ = 72.67(2)°, Z = 2, R = 0.027 for 2527 unique observed reflections.

BODIPY trimer with 1,3,5-triazine core: Facile synthesis and crystal structure

2021 ◽  
pp. A-H
Author(s):  
Chunhua Huang ◽  
Bin Shen ◽  
Kaili Wang ◽  
Xiaofei Sun
Keyword(s):  
Crystal Structure ◽  
Fluorescence Spectroscopy ◽  
Hirshfeld Surface ◽  
Spectroscopic Methods ◽  
X Ray Diffraction ◽  
Facile Synthesis ◽  
Synthesis And Crystal Structure ◽  
X Ray ◽  
Design And Synthesis ◽  
H Nmr

Trimerization reaction of 8-(4[Formula: see text]-cyanophenyl)-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (CN-BODIPY) led to the isolation of a new triazine-based BODIPY trimer 2,4,6-tris(8[Formula: see text]-phenyl-1[Formula: see text],3[Formula: see text],5[Formula: see text],7[Formula: see text]-tetramethyl-4[Formula: see text],4[Formula: see text]-difluoro-4[Formula: see text]-bora-3a[Formula: see text],4a[Formula: see text]-diaza-s-indacene)-1,3,5-triazine (1). This BODIPY trimer 1 have been characterized by a series of spectroscopic methods including MALDI-TOF mass, 1H NMR, electronic absorption, IR and fluorescence spectroscopy. In particular, the single crystals of 1 have be obtained by slow diffusion of methanol into the solution of this compound in CHCl3. The BODIPY trimer structure of 1 with a triazine core has been directly revealed on the basis of single crystal X-ray diffraction analysis with the intermolecular interactions investigated by Hirshfeld surface analysis. This work will be helpful for the design and synthesis of new multiple BODIPY derivatives with various application.

Facile synthesis and crystal structure of 1,5-dimethyl-6-thioxo-1,3,5-triazinane-2,4-dione

2015 ◽  
Vol 56 (4) ◽  
pp. 806-810 ◽  
Author(s):  
N. Shajari ◽  
A. R. Kazemizadeh ◽  
A. Ramazani ◽  
S. W. Joo ◽  
K. Ślepokura ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Facile Synthesis ◽  
Synthesis And Crystal Structure

scholarly journals Microwave‐Assisted Facile Synthesis and Crystal Structure of cis‐9,10,11,15‐Tetrahydro‐9,10[3′,4′]‐furanoanthracene‐12,14‐dione

2006 ◽  
Vol 36 (7) ◽  
pp. 881-883 ◽  
Author(s):  
Weerachai Phutdhawong ◽  
Duang Buddhasukh ◽  
Stephen G. Pyne ◽  
Apinpus Rujiwatra ◽  
Chaveng Pakawatchai
Keyword(s):  
Crystal Structure ◽  
Facile Synthesis ◽  
Synthesis And Crystal Structure ◽  
Microwave Assisted

Synthesis and crystal structure of [MnL(μ-Cl)MnCl3]·H2O L=N, N'-bis(2'-pyridine)methyl-1,10-phenanthroline-2,9-dimethanamine

2002 ◽  
Vol 2002 (3) ◽  
pp. 120-121
Author(s):  
Tian Fu Liu ◽  
Hua Kuan Lin ◽  
Shou Rong Zhu ◽  
Zhong Ming Wang ◽  
Hong Gen Wang ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Synthesis And Crystal Structure
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