Microwave‐Assisted Efficient One‐Pot Multi‐Component Synthesis of Octahydroquinazolinone Derivatives Catalyzed by Cu@Ag Core‐Shell Nanoparticle

2019 ◽  
Vol 4 (19) ◽  
pp. 5696-5706 ◽  
Author(s):  
Lipeeka Rout ◽  
Aniket Kumar ◽  
Pradyumna K Chand ◽  
L Satish K Achary ◽  
Priyabrat Dash
Keyword(s):  
Core Shell ◽  
One Pot ◽  
Microwave Assisted ◽  
Octahydroquinazolinone Derivatives

One-pot microwave assisted approach for synthesis of CdSe/CdS core-shell quantum dots (QDs) and investigating optical properties

2016 ◽  
Vol 30 (07) ◽  
pp. 1650074 ◽  
Author(s):  
M. Molaei ◽  
F. Salari Bardsiri ◽  
A. R. Bahador ◽  
M. Karimipour
Keyword(s):  
Core Shell ◽  
Heat Sensitivity ◽  
X Ray Diffraction ◽  
Cdse Qds ◽  
One Pot ◽  
X Ray ◽  
Microwave Assisted ◽  
Transmission Electron ◽  
Core Shell Structure ◽  
Microwave Assisted Method

In this work, CdSe QDs were synthesized using a microwave assisted method and chemical reaction between NaHSe, CdSO4 at the presence of TGA as capping molecule. Thereafter without CdSe extraction, CdS shell was grown subsequently around CdSe cores by a reaction based on the heat sensitivity of Na2S2O3 dissociation. Synthesized QDs were characterized by means of X-ray diffraction spectroscopy (XRD), Fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM), UV–Vis and photoluminescence (PL) spectroscopy. All of these analyzes confirmed formation of CdSe QDs and successfully growth of CdS shell on surface of CdSe to forming CdSe/CdS core-shell structure.

scholarly journals CdSe-ZnO Core–Shell Quantum Dots for Protein Detection: A Potential Sensing Platform

2021 ◽  
Vol 1 (1) ◽  
pp. 3-13
Author(s):  
Erin A. Jenrette ◽  
Monique J. Farrell ◽  
Jasmin A. Flowers ◽  
Aswini K. Pradhan
Keyword(s):  
Quantum Dots ◽  
Metal Oxide ◽  
Protein Detection ◽  
Oxide Shell ◽  
Core Shell ◽  
One Pot ◽  
Microwave Assisted ◽  
Shell Nanostructures ◽  
Sensing Platform ◽  
User Friendly

A highly sensitive biosensing platform comprised of CdSe-ZnO core–shell nanostructures for targeted applications in protein detection is demonstrated. This innovative technique uses a microwave-assisted thermal decomposition method to produce a rapid, less hazardous, and user-friendly procedure to synthesize a semiconductor core surrounded by nanometer-thick metal oxide shells. The benefit of using a metal oxide shell includes mitigating the toxicity of the CdSe core, thus increasing its biocompatibility and minimizing its photochemical corrosion and oxidation. We present a simple one-pot microwave-assisted protocol for the formation of CdSe-ZnO core–shell quantum dots (QDs). These QDs optimize the recognition limit of bovine serum albumin (BSA) protein through a spectral signal at a considerably low concentration (2.5 × 10−6 M), thus demonstrating its potential to become a highly effective surface-plasmon-enhanced Raman spectroscopy (SERS)-like sensing platform. We report a QD material that can mimic a strong SERS-like behavior due to charge transfer affecting the local electric field.

scholarly journals One pot microwave synthesis of highly stable AuPd@Pd supported core–shell nanoparticles

2018 ◽  
Vol 208 ◽  
pp. 409-425 ◽  
Author(s):  
Alexander G. R. Howe ◽  
Peter J. Miedziak ◽  
David J. Morgan ◽  
Qian He ◽  
Peter Strasser ◽  
...  
Keyword(s):  
Microwave Synthesis ◽  
Core Shell ◽  
Shell Nanoparticles ◽  
One Pot ◽  
Microwave Assisted ◽  
Core Shell Nanoparticles

A series of 1 wt% supported Au, Pd and AuPd nanoalloy catalysts were prepared via microwave assisted reduction of PdCl2 and HAuCl4 in a facile, one pot process.

Microwave-assisted one-pot synthesis of pyrimido［4,5-b］quinolines derivatives

2013 ◽  
Vol 30 (6) ◽  
pp. 636-642
Author(s):  
Xueli Zhang ◽  
Zhilan Lin ◽  
Huiling Hu ◽  
Jiaxin He ◽  
Yuan Gao
Keyword(s):  
One Pot ◽  
Microwave Assisted ◽  
One Pot Synthesis
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