Rapid depth profiling of lead zirconate titanate (PZT) thin films by pulsed glow-discharge optical emission spectroscopy

2006 ◽  
Vol 38 (4) ◽  
pp. 757-760 ◽  
Author(s):  
P. Schwaller ◽  
M. Aeberhard ◽  
T. Nelis ◽  
A. Fischer ◽  
R. Thapliyal ◽  
...  
1999 ◽  
Vol 596 ◽  
Author(s):  
K. S Brinkman ◽  
R. W. Schwartz ◽  
R. K Marcus ◽  
A. Anfone

AbstractCompositional depth profiles have been obtained on chemical solution deposited lead zirconate titanate (PZT) thin films using radio-frequency glow discharge atomic emission spectroscopy. The technique is very rapid, requiring less than one minute for complete multi-element depth profiling of films and multilayer substrates. In the present study, the method was employed to obtain compositional profiles of the various metallic (Pb, Zr, Ti, Si) and organic-related (C, H, O) species that are present in the films and underlying device. Preliminary results using this relatively new technique are reported for PZT films deposited by an aqueous acetate process and heat treated at temperatures ranging from 300 and 700°C. The initial results from these investigations suggest that Pb volatilization occurs at temperatures as low as those typically encountered during the pyrolysis step. Significant interdiffusion of the Pb into the underlying Pt electrode at this temperature is also suggested. Effects of modifying ligand on film thickness and organic decomposition behavior were also observed.


2015 ◽  
Vol 1094 ◽  
pp. 181-187
Author(s):  
Yi Liu ◽  
Wei Xuan Lin ◽  
Wei Bing Ye ◽  
Huan Sheng Li ◽  
Jiong Li ◽  
...  

The depth profiles of Ni-coated copper substrates polished by different mesh size sandpapers were measured by the glow discharge optical emission spectroscopy (GDOES) depth profiling technique. The measured depth profiles were well fitted by the MRI-CRAS model developed recently on the basis of the Mixing-Roughness-Information depth (MRI) model and the CRAter-Simulation (CRAS) model, taking into account the pronounced crater effect upon GDOES depth profiling. The crater effect upon depth profiling was characterized quantitatively and the interface roughness values between the coated Ni layer and the Cu substrates were determined and compared with the ones measured by AFM.


2002 ◽  
Vol 373 (7) ◽  
pp. 656-663 ◽  
Author(s):  
Kenneth R. Marcus ◽  
Alwyn B. Anfone ◽  
Wandee Luesaiwong ◽  
Teresa A. Hill ◽  
Dvora Perahia ◽  
...  

2016 ◽  
Vol 31 (11) ◽  
pp. 2207-2212 ◽  
Author(s):  
C. Schubert ◽  
V. Hoffmann ◽  
A. Kümmel ◽  
J. Sinn ◽  
M. Härtel ◽  
...  

This article describes the compositional depth profiling (CDP) of diamond-like carbon (DLC) layers by Glow Discharge-Optical Emission Spectrometry (GD-OES).


2011 ◽  
Vol 520 (5) ◽  
pp. 1660-1667 ◽  
Author(s):  
Marcus Wilke ◽  
Gerd Teichert ◽  
Ryota Gemma ◽  
Astrid Pundt ◽  
Reiner Kirchheim ◽  
...  

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