Mass spectra of methyl esters of brominated fatty acids and their presence in soft drinks and cocktail syrups

2013 ◽  
Vol 27 (9) ◽  
pp. 1083-1089 ◽  
Author(s):  
Paul Bendig ◽  
Lisa Maier ◽  
Katja Lehnert ◽  
Holger Knapp ◽  
Walter Vetter
1970 ◽  
Vol 82 ◽  
pp. 1-42
Author(s):  
K.R Pedersen ◽  
J Lam

Ketilidian sedimentary rocks nearly 2000 m.y. old and only slightly metamorphosed have been shown to contain fossils and organic compounds. Results of work on organic material from a 1-3 m thick coal-graphite layer from the Foselv Formation in the Sortis Group in Grænseland are presented. Aliphatic (straight chain, branched and cyclic) hydrocarbons are dominant in the extract from two coal-graphite samples weighing about 4 kg and 10 kg respectively. Further investigations of these compounds have revealed many saturated straight-chain hydrocarbons, with the n-C15 alkane, the most abundant among the normal alkanes, ranging from C12 to about C21, and various isoalkanes and anteisoalkanes. Saturated cyclic hydrocarbons like alkyl cyclohexanes, and homologous series of alkyl benzenes and alkyl naphthalenes are also present. A series of monoterpenoid compounds is present. Six of them are fairly well characterized by their mass spectra. Fatty acids and methyl esters of fatty acids are present, notably a homologous series of straight-chain fatty acids. Branched acids are also present in minor amounts. The organic compounds further indicate that this Precambrian coal-graphite layer is the result of biological activity.


Author(s):  
Codrean POP ◽  
Levente BARA ◽  
Elena HORJ ◽  
Andreea IORDACHE ◽  
Cornel LASLO ◽  
...  

The aim of this work was to establish the extraction procedure, the derivatization method, the separation temperature program, the identification and quantitation of the free fatty acids from meat. A gas chromatography - mass spectrometric (GC/MS) technique was used. The fatty acids were obtained by grounding meat, water and sand and then extraction was performed by mixing chloroform:methanol (2:1) during 30 seconds, at room temperature. The fatty acids were derivatized to obtain methyl esters. A Trace DSQ ThermoFinnigan quadrupole mass spectrometer coupled with a Trace GC was used. Fatty acids were separated on a Rtx-5MS capillary column, 30m x 0.25mm, 0.25µm film thickness, using a suitable temperature program. The identification of fatty acids was obtained by comparison of fatty acids methyl esters (FAME) mass spectra with the mass spectra of FAME kits and of NIST library. Concentrations of fatty acids were calculated by using a proper internal standard.


2019 ◽  
Vol 56 (4) ◽  
pp. 279-286 ◽  
Author(s):  
Tomasz Wasilewski ◽  
Yong-Qiang Sun ◽  
Wiesław Hreczuch ◽  
Artur Seweryn ◽  
Tomasz Bujak

2003 ◽  
Vol 783 (2) ◽  
pp. 443-451 ◽  
Author(s):  
M.M. Keinänen ◽  
L.K. Korhonen ◽  
P.J. Martikainen ◽  
T. Vartiainen ◽  
I.T. Miettinen ◽  
...  

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