Electrospray tandem mass spectrometry of new porphyrin amino acid conjugates

2005 ◽  
Vol 19 (18) ◽  
pp. 2569-2580 ◽  
Author(s):  
V. Vaz Serra ◽  
M. R. M. Domingues ◽  
M. A. F. Faustino ◽  
P. Domingues ◽  
J. P. C. Tomé ◽  
...  
2017 ◽  
Vol 10 (1) ◽  
pp. 100-109
Author(s):  
Hongxia Li ◽  
Natasha Trzaskalski ◽  
R.J. Neil Emery

Objective:A simple and fast high performance liquid chromatography-electrospray tandem mass spectrometry (LC-ESI-MS/MS) method has been developed for the analysis of brassinosteroids (BRs) in plants without derivatization.Materials:The BRs (including castasterone, 24-epicastasterone, brassinolide and 24-epibrassinolide) have been extracted with ice cold 80% aqueous methanol solution.Method:Five different purification strategies have been tested for the purification and enrichment of BRs.Conclusion:This analytical method was sensitive, reliable, rapid and applicable to trace analysis in complex plant samples.


2015 ◽  
Vol 7 (18) ◽  
pp. 7574-7581 ◽  
Author(s):  
Magdalena M. Dziągwa-Becker ◽  
Jose M. Marin Ramos ◽  
Jakub K. Topolski ◽  
Wiesław A. Oleszek

Free amino acid determination in plants by LC-MS/MS.


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