Development of X-ray diffractometer for in-situ observation of thin-film crystal growth equipped with focusing monochromator

2010 ◽  
Vol 8 (2) ◽  
pp. 294-296 ◽  
Author(s):  
Hiroshi Tameoka ◽  
Tatsuya Kawase ◽  
Masao Tabuchi ◽  
Yoshikazu Takeda
Keyword(s):  
Thin Film ◽  
Crystal Growth ◽  
In Situ Observation ◽  
X Ray

Crystal growth of β′-Gd2(MoO4)3 and in situ observation of its domain structure by the microscope and the synchrotron X-ray topography

2001 ◽  
Vol 233 (4) ◽  
pp. 717-722 ◽  
Author(s):  
Qingxi Yuan ◽  
Chunhua Zhao ◽  
Weiping Luo ◽  
Xiaofeng Yin ◽  
Jun Xu ◽  
...  
Keyword(s):  
Crystal Growth ◽  
Domain Structure ◽  
In Situ Observation ◽  
X Ray

In-situ Observation of SiC Bulk Single Crystal Growth by X-Ray Topography

2000 ◽  
Vol 338-342 ◽  
pp. 457-460 ◽  
Author(s):  
Tomohisa Kato ◽  
Naoki Oyanagi ◽  
Hirotaka Yamaguchi ◽  
Yukio Takano ◽  
Shin Ichi Nishizawa ◽  
...  
Keyword(s):  
Crystal Growth ◽  
Single Crystal ◽  
Single Crystal Growth ◽  
In Situ Observation ◽  
Bulk Single Crystal ◽  
X Ray

SiC Single Crystal Growth Rate Measurement by In-Situ Observation using the Transmission X-Ray Technique

2000 ◽  
Vol 338-342 ◽  
pp. 75-78 ◽  
Author(s):  
Naoki Oyanagi ◽  
Shin Ichi Nishizawa ◽  
Tomohisa Kato ◽  
Hirotaka Yamaguchi ◽  
Kazuo Arai
Keyword(s):  
Growth Rate ◽  
Crystal Growth ◽  
Single Crystal ◽  
Single Crystal Growth ◽  
Crystal Growth Rate ◽  
In Situ Observation ◽  
Rate Measurement ◽  
X Ray ◽  
Growth Rate Measurement

scholarly journals In-situ Observation of 2-Dimensional X-ray Diffraction of Organic Thin-film Growth by Synchrotron Radiation

Hyomen Kagaku ◽  
2014 ◽  
Vol 35 (4) ◽  
pp. 190-195 ◽  
Author(s):  
Noriyuki YOSHIMOTO ◽  
Takeshi WATANABE ◽  
Tomoyuki KOGANEZAWA ◽  
Mamoru KIKUCHI ◽  
Ichiro HIROSAWA
Keyword(s):  
Thin Film ◽  
Synchrotron Radiation ◽  
Film Growth ◽  
Thin Film Growth ◽  
In Situ Observation ◽  
Organic Thin Film ◽  
X Ray Diffraction ◽  
X Ray

Single Crystal Growth of High-Pressure Phases of Ice and Salt Hydrate Far Below the Original Melting Point by Mixing Alcohol: Crystal Structure Determination of Magnesium Chloride Heptahydrate

2020 ◽  
Author(s):  
Keishiro Yamashita ◽  
Kazuki Komatsu ◽  
Hiroyuki Kagi
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
Crystal Growth ◽  
Single Crystal ◽  
Room Temperature ◽  
Growth Technique ◽  
Salt Hydrate ◽  
X Ray

An crystal-growth technique for single crystal x-ray structure analysis of high-pressure forms of hydrogen-bonded crystals is proposed. We used alcohol mixture (methanol: ethanol = 4:1 in volumetric ratio), which is a widely used pressure transmitting medium, inhibiting the nucleation and growth of unwanted crystals. In this paper, two kinds of single crystals which have not been obtained using a conventional experimental technique were obtained using this technique: ice VI at 1.99 GPa and MgCl<sub>2</sub>·7H<sub>2</sub>O at 2.50 GPa at room temperature. Here we first report the crystal structure of MgCl2·7H2O. This technique simultaneously meets the requirement of hydrostaticity for high-pressure experiments and has feasibility for further in-situ measurements.

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