High-resolution solid-state NMR investigation of the filler-rubber interaction: 2. High-speed [1H] magic-angle spinning NMR spectroscopy in carbon-black-filled polybutadiene

2001 ◽  
Vol 50 (4) ◽  
pp. 387-394 ◽  
Author(s):  
Rachel Mansencal ◽  
Bassel Haidar ◽  
Alain Vidal ◽  
Luc Delmotte ◽  
Jean-Michel Chezeau
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Carbon Black ◽  
Solid State Nmr ◽  
High Speed ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Angle Spinning

High resolution triple resonance micro magic angle spinning NMR spectroscopy of nanoliter sample volumes

2016 ◽  
Vol 18 (6) ◽  
pp. 4902-4910 ◽  
Author(s):  
J. Ole Brauckmann ◽  
J. W. G. (Hans) Janssen ◽  
Arno P. M. Kentgens
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Single Crystals ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Triple Resonance ◽  
Angle Spinning

To be able to study mass-limited samples and small single crystals, a triple resonance micro-magic angle spinning (μMAS) probehead for the application of high-resolution solid-state NMR of nanoliter samples was developed.

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