Optimization of powder injection molding of feedstock based on aluminum oxide and multicomponent water-soluble polymer binder

2011 ◽  
Vol 51 (7) ◽  
pp. 1376-1382 ◽  
Author(s):  
Berenika Hausnerova ◽  
Lucie Marcanikova ◽  
Petr Filip ◽  
Petr Saha
1983 ◽  
Vol 12 (5) ◽  
pp. 625-626 ◽  
Author(s):  
Shoichi Hayashida ◽  
Hirotsugu Sato ◽  
Shungo Sugawara

Polymers ◽  
2019 ◽  
Vol 11 (3) ◽  
pp. 432 ◽  
Author(s):  
Daniel Sanetrnik ◽  
Berenika Hausnerova ◽  
Vladimir Pata

Wall slip in the flow of powder injection molding (PIM) compounds can be the cause of unrealistically low viscosity values, and can lead to a failure of flow simulation approaches. Regardless of its importance, it has been considered only scarcely in the rheological models applied to PIM materials. In this paper, an online extrusion rheometer equipped with rectangular slit dies was used to evaluate the slip velocity of commercial as well as in-house-prepared PIM feedstocks based on metallic and ceramic powders at close-to-processing conditions. The tested slit dies varied in their dimensions and surface roughness. The wall-slip effect was quantified using the Mooney analysis of slip velocities. The smaller gap height (1 mm) supported the wall-slip effect. It was shown that both the binder composition and the powder characteristic affect slip velocity. Slip velocity can be reduced by tailoring a powder particle size distribution towards smaller particle fractions. The thickness of the polymer layer formed at the channel wall is higher for water-soluble feedstocks, while in the case of the catalytic polyacetal feedstocks the effect of surface roughness was manifested through lower viscosity at smooth surfaces.


2016 ◽  
Vol 690 ◽  
pp. 87-91
Author(s):  
Parinya Chakartnarodom ◽  
Nuntaporn Kongkajun ◽  
Nutthita Chuankrerkkul

The purpose of this work is to use the statistical methods including linear regression and statistical hypothesis test to study the dissolution behavior of polyethylene glycol (PEG), a water-soluble binder, during debinding step of the green specimens of mullite formed by powder injection molding (PIM). Two systems of composite binders were investigated including (A) 80 wt% polyethylene glycol (PEG) and 20 wt% polyvinyl butyral (PVB) and (B) 78 wt% PEG, 20 wt% PVB, and 2 wt% steric acid (SA)The lab-scale plunger type PIM machine was used to prepare the green specimens consisting of mullite powder and the composite binder. The possible solid loadings of the green specimens that could be prepared by this machine were 50, 52, and 54 vol% mullite (50, 48, and 46 vol% binder). The debinding was done by soaking the green specimens in the warm water at 40 or 60 oC to remove PEG. At level of significance 0.05 for statistical analysis, the dissolution behavior of PEG can be fitted with Avarami equation. In addition, from the Avarami equation obtained from each experimental condition, the dissolution rate of PEG was independent of the parameters used in this study including solid loading in the green specimens, water temperatures for debinding, and composite binder systems.


2005 ◽  
Vol 40 (5) ◽  
pp. 1105-1109 ◽  
Author(s):  
Minseok Song ◽  
Min Soo Park ◽  
Jin Kon Kim ◽  
Il Bum Cho ◽  
Kyung Ho Kim ◽  
...  

Author(s):  
Alexander Muranov ◽  
Alexey Semenov ◽  
Anatoly Kutsbakh ◽  
Boris Semenov

The article discusses one of the modern areas of powder metallurgy – the technology of manufacturing shaped parts by the powder injection molding (PIM). For the powder-polymer mixture (feedstock) with a wax-polypropylene binder of the solvent-thermal type of removal by isobaric volume dilatometry, the dependence of PVT state parameters was studied. For each component of the polymer binder, the dependence of pressure on the temperature of phase transition was obtained. As a result of mathematical processing and analysis of PVT data for the feedstock of the studied type, a technological window of parameters has been determined that allows injection molding of «green parts» with minimal volume shrinkage. The results of a comparative analysis of the compaction of feedstock with a polymer binder catalytic and solution-thermal type of removal are presented.


2021 ◽  
Author(s):  
Aranee Pleng Teepakakorn ◽  
Makoto Ogawa

Water-induced self-healing materials were prepared by the hybridization of a water-soluble polymer, poly(vinyl alcohol), with a smectite clay by mixing in an aqueous media and subsequent casting. Without using chemical...


2020 ◽  
Author(s):  
Elena Glazkova ◽  
Nikolay Rodkevich ◽  
Nikita Toropkov ◽  
Aleksandr Pervikov ◽  
Marat Lerner

Sign in / Sign up

Export Citation Format

Share Document