Exploring the effect of electron beam irradiation on the properties of some EPDM-flax fiber composites

2017 ◽  
Vol 40 (1) ◽  
pp. 315-327 ◽  
Author(s):  
Maria Daniela Stelescu ◽  
Anton Airinei ◽  
Elena Manaila ◽  
Nicusor Fifere ◽  
Gabriela Craciun ◽  
...  
Polymers ◽  
2021 ◽  
Vol 13 (15) ◽  
pp. 2555
Author(s):  
Anton Airinei ◽  
Mihai Asandulesa ◽  
Maria Daniela Stelescu ◽  
Niţǎ Tudorachi ◽  
Nicusor Fifere ◽  
...  

This paper deals with the dielectric and sorption properties of some flax fiber-reinforced ethylene-propylene-diene monomer (EPDM) composites containing different fiber loadings as well as their behavior after exposure to different doses of electron beam irradiation. Three relaxation processes were evinced, a weak relaxation β at sub-Tg temperatures and two α-type relaxations above the Tg. The EPDM/flax composites exhibited higher values of dielectric constant, dielectric loss and conductivity as compared to a pristine EPDM sample. Using thermogravimetric analysis (TG) coupled with Fourier transform infrared spectroscopy (FTIR) and mass spectrometry (MS) (TG/FTIR/MS system), the degradation products can be identified. The water uptake increased as the flax fiber level increased in composites. The water uptake tests of irradiated composites showed that the highest water content was obtained for a flax fiber level of 20 phr.


2010 ◽  
Vol 15 (2) ◽  
pp. 380-385 ◽  
Author(s):  
Patrícia Y. Inamura ◽  
Kleber Shimazaki ◽  
Maria Aparecida Colombo ◽  
Ricardo de Rosa ◽  
Esperidiana Augusta Barretos de Moura ◽  
...  

2019 ◽  
Vol 33 (26) ◽  
pp. 1950305 ◽  
Author(s):  
Subhashree Patra ◽  
Kamal Lochan Mohanta ◽  
Chhatrapati Parida

This investigation aims to analyze the effects of electron beam irradiation on the morphological and mechanical properties of green composites synthesized using natural fibers of luffa cylindrica (LC) and biodegradable polymer poly (lactic) acid. This work aims to transform the low priced, readily available, agricultural waste product LC fiber into a high value product. The major challenge during the fabrication of natural fiber composites is the chemical bonding between hydrophilic LC fiber and hydrophobic poly lactic acid (PLA) matrix. Due to the disagreeing chemical nature of fiber and matrix, they are not compatible. The fibers are exposed to physical treatment, i.e., electron beam irradiation of different doses 0.5, 1.0, 2.0, 4.0 and 10.0 Gy using 6 MeV medical linear accelerator to increase the compatibility of LC fiber with PLA. Before irradiation, LC fibers are modified with calcium salts to explore the use of composite materials in biomedical terrain. When PLA is reinforced with irradiated LC fiber, tensile strength increases by 79.87% and flexural strength increases by 177%. Mechanical parameters generated by flexural and tensile tests of this study can be explored to have various clinical applications like bone implant, replacement of cervical cavities, etc.


Author(s):  
B. L. Armbruster ◽  
B. Kraus ◽  
M. Pan

One goal in electron microscopy of biological specimens is to improve the quality of data to equal the resolution capabilities of modem transmission electron microscopes. Radiation damage and beam- induced movement caused by charging of the sample, low image contrast at high resolution, and sensitivity to external vibration and drift in side entry specimen holders limit the effective resolution one can achieve. Several methods have been developed to address these limitations: cryomethods are widely employed to preserve and stabilize specimens against some of the adverse effects of the vacuum and electron beam irradiation, spot-scan imaging reduces charging and associated beam-induced movement, and energy-filtered imaging removes the “fog” caused by inelastic scattering of electrons which is particularly pronounced in thick specimens.Although most cryoholders can easily achieve a 3.4Å resolution specification, information perpendicular to the goniometer axis may be degraded due to vibration. Absolute drift after mechanical and thermal equilibration as well as drift after movement of a holder may cause loss of resolution in any direction.


Author(s):  
Wei-Chih Wang ◽  
Jian-Shing Luo

Abstract In this paper, we revealed p+/n-well and n+/p-well junction characteristic changes caused by electron beam (EB) irradiation. Most importantly, we found a device contact side junction characteristic is relatively sensitive to EB irradiation than its whole device characteristic; an order of magnitude excess current appears at low forward bias region after 1kV EB acceleration voltage irradiation (Vacc). Furthermore, these changes were well interpreted by our Monte Carlo simulation results, the Shockley-Read Hall (SRH) model and the Generation-Recombination (G-R) center trap theory. In addition, four essential examining items were suggested and proposed for EB irradiation damage origins investigation and evaluation. Finally, by taking advantage of the excess current phenomenon, a scanning electron microscope (SEM) passive voltage contrast (PVC) fault localization application at n-FET region was also demonstrated.


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