scholarly journals Detection of [1,6-13C2]-glucose metabolism in rat brain by in vivo1H-[13C]-NMR spectroscopy

2002 ◽  
Vol 49 (1) ◽  
pp. 37-46 ◽  
Author(s):  
Robin A. de Graaf ◽  
Peter B. Brown ◽  
Graeme F. Mason ◽  
Douglas L. Rothman ◽  
Kevin L. Behar
2011 ◽  
Vol 36 (11) ◽  
pp. 1962-1968 ◽  
Author(s):  
Kathleen Ennis ◽  
Dinesh Kumar Deelchand ◽  
Ivan Tkac ◽  
Pierre-Gilles Henry ◽  
Raghavendra Rao

2004 ◽  
Vol 45 (2-3) ◽  
pp. 297-303 ◽  
Author(s):  
Marı́a A Garcı́a-Espinosa ◽  
Tiago B Rodrigues ◽  
Alejandra Sierra ◽  
Marina Benito ◽  
Carla Fonseca ◽  
...  

2010 ◽  
Vol 112 (1) ◽  
pp. 24-33 ◽  
Author(s):  
Pieter van Eijsden ◽  
Kevin L. Behar ◽  
Graeme F. Mason ◽  
Kees P. J. Braun ◽  
Robin A. de Graaf

2002 ◽  
Vol 82 (4) ◽  
pp. 857-866 ◽  
Author(s):  
Pierre-Gilles Henry ◽  
Vincent Lebon ◽  
Françoise Vaufrey ◽  
Emmanuel Brouillet ◽  
Philippe Hantraye ◽  
...  

Molbank ◽  
10.3390/m1140 ◽  
2020 ◽  
Vol 2020 (2) ◽  
pp. M1140
Author(s):  
Jack Bennett ◽  
Paul Murphy

(2S,3R,6R)-2-[(R)-1-Hydroxyallyl]-4,4-dimethoxy-6-methyltetrahydro-2H-pyran-3-ol was isolated in 18% after treating the glucose derived (5R,6S,7R)-5,6,7-tris[(triethylsilyl)oxy]nona-1,8-dien-4-one with (1S)-(+)-10-camphorsulfonic acid (CSA). The one-pot formation of the title compound involved triethylsilyl (TES) removal, alkene isomerization, intramolecular conjugate addition and ketal formation. The compound was characterized by 1H and 13C NMR spectroscopy, ESI mass spectrometry and IR spectroscopy. NMR spectroscopy was used to establish the product structure, including the conformation of its tetrahydropyran ring.


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