scholarly journals Efficient transfer of DNP‐enhanced 1 H magnetization to half‐integer quadrupolar nuclei in solids at moderate spinning rate

Author(s):  
Hiroki Nagashima ◽  
Julien Trébosc ◽  
Yoshihiro Kon ◽  
Olivier Lafon ◽  
Jean‐Paul Amoureux
Author(s):  
F. Pourpoint ◽  
O. Lafon ◽  
R. Gauvin ◽  
J.-P. Amoureux ◽  
L. Delevoye

1992 ◽  
Vol 47 (5) ◽  
pp. 665-674
Author(s):  
J. P. Amoureux

Abstract This article describes a few aspects of NMR characterization of half-integer quadrupolar nuclei in powder samples which are either static or rotating around one fixed axis (M.A.S. and V.A.S. techniques). The simultaneous occurence of C.S.A. and quadrupole interactions with possible noncoincident tensors is discussed. Two experimental limitations are taken into accout: the sample spinning speed and the RF-amplifier power


1987 ◽  
Vol 71 (1) ◽  
pp. 62-74 ◽  
Author(s):  
A.P.M Kentgens ◽  
J.J.M Lemmens ◽  
F.M.M Geurts ◽  
W.S Veeman

2003 ◽  
Vol 23 (4) ◽  
pp. 213-223 ◽  
Author(s):  
Jean-Paul Amoureux ◽  
Cláudia Morais ◽  
Julien Trebosc ◽  
João Rocha ◽  
Christian Fernandez

2016 ◽  
Vol 18 (36) ◽  
pp. 25284-25295 ◽  
Author(s):  
Aaron J. Rossini ◽  
Michael P. Hanrahan ◽  
Martin Thuo

Fast MAS and proton detection are applied to rapidly acquire wideline solid-state NMR spectra of spin-1/2 and half-integer quadrupolar nuclei.


2015 ◽  
Vol 142 (9) ◽  
pp. 094201 ◽  
Author(s):  
Qiang Wang ◽  
Yixuan Li ◽  
Julien Trébosc ◽  
Olivier Lafon ◽  
Jun Xu ◽  
...  

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