Using hyperbolic secant pulses to assist characterization of chemical shift tensors for half-integer spin quadrupolar nuclei in MAS powder samples

Thomas T. Nakashima; Roshanak Teymoori; Roderick E. Wasylishen

doi:10.1002/mrc.2413

Using hyperbolic secant pulses to assist characterization of chemical shift tensors for half-integer spin quadrupolar nuclei in MAS powder samples

Magnetic Resonance in Chemistry ◽

10.1002/mrc.2413 ◽

2009 ◽

Vol 47 (6) ◽

pp. 465-471 ◽

Cited By ~ 13

Author(s):

Thomas T. Nakashima ◽

Roshanak Teymoori ◽

Roderick E. Wasylishen

Keyword(s):

Chemical Shift ◽

Quadrupolar Nuclei ◽

Chemical Shift Tensors ◽

Integer Spin ◽

Half Integer ◽

Powder Samples

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NMR Characterization of Half-integer Quadrupolar Nuclei in Solids

Zeitschrift für Naturforschung A ◽

10.1515/zna-1992-0505 ◽

1992 ◽

Vol 47 (5) ◽

pp. 665-674

Author(s):

J. P. Amoureux

Keyword(s):

Quadrupolar Nuclei ◽

Rf Amplifier ◽

Quadrupole Interactions ◽

Half Integer ◽

Nmr Characterization ◽

Powder Samples ◽

Fixed Axis ◽

Spinning Speed

Abstract This article describes a few aspects of NMR characterization of half-integer quadrupolar nuclei in powder samples which are either static or rotating around one fixed axis (M.A.S. and V.A.S. techniques). The simultaneous occurence of C.S.A. and quadrupole interactions with possible noncoincident tensors is discussed. Two experimental limitations are taken into accout: the sample spinning speed and the RF-amplifier power

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Phosphorus Chemical Shift Tensors of Phosphido Ligands in Ruthenium Carbonyl Compounds: 31P NMR Spectroscopy of Single-Crystal and Powder Samples and ab Initio Calculations

Journal of the American Chemical Society ◽

10.1021/ja0122041 ◽

2002 ◽

Vol 124 (7) ◽

pp. 1541-1552 ◽

Cited By ~ 26

Author(s):

Klaus Eichele ◽

Roderick E. Wasylishen ◽

John F. Corrigan ◽

Nicholas J. Taylor ◽

Arthur J. Carty ◽

...

Keyword(s):

Nmr Spectroscopy ◽

Chemical Shift ◽

Ab Initio Calculations ◽

Single Crystal ◽

Carbonyl Compounds ◽

31P Nmr ◽

31P Nmr Spectroscopy ◽

Chemical Shift Tensors ◽

Ruthenium Carbonyl ◽

Powder Samples

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An efficient simulation of variable-angle spinning lineshapes for the quadrupolar nuclei with half-integer spin

Journal of Magnetic Resonance (1969) ◽

10.1016/0022-2364(91)90165-p ◽

1991 ◽

Vol 95 (3) ◽

pp. 509-522 ◽

Cited By ~ 8

Author(s):

Zhiwen Zheng ◽

Zhehong Gan ◽

Naresh K Sethi ◽

D.W Alderman ◽

David M Grant

Keyword(s):

Quadrupolar Nuclei ◽

Efficient Simulation ◽

Integer Spin ◽

Half Integer ◽

Variable Angle ◽

Angle Spinning ◽

Variable Angle Spinning

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19F-decoupling of half-integer spin quadrupolar nuclei in solid-state NMR: Application of frequency-swept decoupling methods

Solid State Nuclear Magnetic Resonance ◽

10.1016/j.ssnmr.2011.07.003 ◽

2011 ◽

Vol 40 (2) ◽

pp. 84-87 ◽

Cited By ~ 10

Author(s):

C. Vinod Chandran ◽

Günter Hempel ◽

Thomas Bräuniger

Keyword(s):

Solid State ◽

Solid State Nmr ◽

Quadrupolar Nuclei ◽

Integer Spin ◽

Half Integer

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Sensitivity enhancement of the central-transition signal of half-integer spin quadrupolar nuclei in solid-state NMR: Features of multiple fast amplitude-modulated pulse transfer

Journal of Magnetic Resonance ◽

10.1016/j.jmr.2008.02.020 ◽

2008 ◽

Vol 192 (2) ◽

pp. 230-234 ◽

Cited By ~ 8

Author(s):

Mithun Goswami ◽

P.K. Madhu

Keyword(s):

Solid State ◽

Solid State Nmr ◽

Sensitivity Enhancement ◽

Quadrupolar Nuclei ◽

Integer Spin ◽

Half Integer ◽

Central Transition

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Solid-State13C Chemical Shift Tensors in Terpenes. 3. Structural Characterization of Polymorphous Verbenol

Journal of the American Chemical Society ◽

10.1021/ja9932378 ◽

2000 ◽

Vol 122 (15) ◽

pp. 3708-3714 ◽

Cited By ~ 31

Author(s):

James K. Harper ◽

David M. Grant

Keyword(s):

Chemical Shift ◽

Structural Characterization ◽

Chemical Shift Tensors

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Fast amplitude-modulated pulse trains with frequency sweep (SW-FAM) in static NMR of half-integer spin quadrupolar nuclei

Journal of Magnetic Resonance ◽

10.1016/j.jmr.2006.03.016 ◽

2006 ◽

Vol 181 (1) ◽

pp. 68-78 ◽

Cited By ~ 18

Author(s):

Thomas Bräuniger ◽

Günter Hempel ◽

P.K. Madhu

Keyword(s):

Quadrupolar Nuclei ◽

Frequency Sweep ◽

Pulse Trains ◽

Integer Spin ◽

Half Integer

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Side-band analysis in variable-angle sample-spinning (VASS) NMR for the central transition of quadrupolar nuclei (half-integer spin)

Magnetic Resonance in Chemistry ◽

10.1002/mrc.1260280103 ◽

1990 ◽

Vol 28 (1) ◽

pp. 5-10 ◽

Cited By ~ 21

Author(s):

J. P. Amoureux ◽

C. Fernandez ◽

F. Lefebvre

Keyword(s):

Quadrupolar Nuclei ◽

Side Band ◽

Integer Spin ◽

Half Integer ◽

Central Transition ◽

Variable Angle

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Recent advances in experimental solid state NMR methodology for half-integer spin quadrupolar nuclei

Progress in Nuclear Magnetic Resonance Spectroscopy ◽

10.1016/s0079-6565(98)00028-4 ◽

1999 ◽

Vol 34 (2) ◽

pp. 159-201 ◽

Cited By ~ 263

Author(s):

M Smith

Keyword(s):

Solid State ◽

Solid State Nmr ◽

Quadrupolar Nuclei ◽

Integer Spin ◽

Half Integer ◽

Recent Advances

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Multiple-Quantum Magic-Angle Spinning: High-Resolution Solid-State NMR of Half-Integer Spin Quadrupolar Nuclei

Annual Reports on NMR Spectroscopy - Annual Reports on NMR Spectroscopy Volume 54 ◽

10.1016/s0066-4103(04)54003-6 ◽

2004 ◽

pp. 81-153 ◽

Cited By ~ 41

Author(s):

Amir Goldbourt ◽

P.K. Madhu

Keyword(s):

Solid State ◽

High Resolution ◽

Solid State Nmr ◽

Magic Angle Spinning ◽

Magic Angle ◽

Quadrupolar Nuclei ◽

Multiple Quantum ◽

Integer Spin ◽

Half Integer ◽

Angle Spinning

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