Ultrafast Preparation of AIE-Active Fluorescent Organic Nanoparticles via a “One-Pot” Microwave-Assisted Kabachnik-Fields Reaction

2016 ◽  
Vol 37 (21) ◽  
pp. 1754-1759 ◽  
Author(s):  
Zi Long ◽  
Meiying Liu ◽  
Qing Wan ◽  
Liucheng Mao ◽  
Hongye Huang ◽  
...  
Keyword(s):  
One Pot ◽  
Organic Nanoparticles ◽  
Microwave Assisted ◽  
Fluorescent Organic Nanoparticles

Fabrication of amphiphilic fluorescent nanoparticles with an AIE feature via a one-pot clickable mercaptoacetic acid locking imine reaction: synthesis, self-assembly and bioimaging

2016 ◽  
Vol 7 (27) ◽  
pp. 4559-4566 ◽  
Author(s):  
Qing Wan ◽  
Meiying Liu ◽  
Dazhuang Xu ◽  
Liucheng Mao ◽  
Hongye Huang ◽  
...  
Keyword(s):  
Self Assembly ◽  
Mercaptoacetic Acid ◽  
Fluorescent Nanoparticles ◽  
Reaction Synthesis ◽  
One Pot ◽  
Organic Nanoparticles ◽  
Water Dispersible ◽  
Fluorescent Organic Nanoparticles

Water dispersible and non-toxic AIE active fluorescent organic nanoparticles were fabricatedviaa one-pot clickable mercaptoacetic acid locking imine reaction.

Microwave-assisted one-pot synthesis of pyrimido［4,5-b］quinolines derivatives

2013 ◽  
Vol 30 (6) ◽  
pp. 636-642
Author(s):  
Xueli Zhang ◽  
Zhilan Lin ◽  
Huiling Hu ◽  
Jiaxin He ◽  
Yuan Gao
Keyword(s):  
One Pot ◽  
Microwave Assisted ◽  
One Pot Synthesis

scholarly journals One-Pot Microwave-Assisted Synthesis of Water-Soluble Pyran-2,4,5-triol Glucose Amine Schiff Base Derivative: XRD/HSA Interactions, Crystal Structure, Spectral, Thermal and a DFT/TD-DFT

Crystals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 117
Author(s):  
Yousef Hijji ◽  
Rajeesha Rajan ◽  
Hamdi Ben Yahia ◽  
Said Mansour ◽  
Abdelkader Zarrouk ◽  
...  
Keyword(s):  
Schiff Base ◽  
Molecular Orbital ◽  
Density Functional ◽  
Condensation Reaction ◽  
3D Structure ◽  
Water Soluble ◽  
Microwave Assisted Synthesis ◽  
One Pot ◽  
Microwave Assisted ◽  
Td Dft

The(3R,4R,6R)-3-(((E)-2-hydroxybenzylidene)amino)-6-(hydroxymethyl)tetrahydro-2H-pyran-2,4,5-triol water-soluble Glucose amine Schiff base (GASB-1) product was made available by condensation of 2-hydroxybenzaldehyde with (3R,6R)-3-amino-6-(hydroxymethyl)-tetra-hydro-2H-pyran-2,4,5-triol under mono-mode microwave heating. A one-pot 5-minute microwave-assisted reaction was required to complete the condensation reaction with 90% yield and without having byproducts. The 3D structure of GASB-1 was solved from single crystal X-ray diffraction data and computed by DFT/6-311G(d,p). The Hirshfeld surface analysis (HSA), molecular electronic potential (MEP), Mulliken atomic charge (MAC), and natural population analysis (NPA) were performed. The IR and UV-Vis spectra were matched to their density functional theory (DFT) relatives and the thermal behavior was resolved in an open-room condition via thermogravimetry/Derivative thermogravimetry (TG/DTG) and differential scanning calorimetry (DSC). The highest occupied molecular orbital/lowest unoccupied molecular orbital (HOMO/LUMO), density of state (DOS), and time-dependence TD-DFT computations were correlated to the experimental electron transfer in water and acrylonitrile solvents.

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