Microwave-Assisted Homogeneous Polymerizations in Water-Soluble Ionic Liquids: An Alternative and Green Approach for Polymer Synthesis

2007 ◽  
Vol 28 (4) ◽  
pp. 456-464 ◽  
Author(s):  
Carlos Guerrero-Sanchez ◽  
Matthias Lobert ◽  
Richard Hoogenboom ◽  
Ulrich S. Schubert
Keyword(s):  
Ionic Liquids ◽  
Polymer Synthesis ◽  
Water Soluble ◽  
Microwave Assisted ◽  
Green Approach

A Green Approach for Producing Solvent-free Anisyl Acetate by Enzymecatalyzed Direct Esterification in Sponge-like Ionic Liquids Under Conventional and Microwave Heating

2013 ◽  
Vol 1 (2) ◽  
pp. 145-154 ◽  
Author(s):  
Pedro Lozano ◽  
Juana Bernal ◽  
Almudena Lajarin ◽  
Daniel Romera ◽  
Eduardo Garcia-Verdugo ◽  
...  
Keyword(s):  
Ionic Liquids ◽  
Microwave Heating ◽  
Solvent Free ◽  
Direct Esterification ◽  
Green Approach

scholarly journals One-Pot Microwave-Assisted Synthesis of Water-Soluble Pyran-2,4,5-triol Glucose Amine Schiff Base Derivative: XRD/HSA Interactions, Crystal Structure, Spectral, Thermal and a DFT/TD-DFT

Crystals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 117
Author(s):  
Yousef Hijji ◽  
Rajeesha Rajan ◽  
Hamdi Ben Yahia ◽  
Said Mansour ◽  
Abdelkader Zarrouk ◽  
...  
Keyword(s):  
Schiff Base ◽  
Molecular Orbital ◽  
Density Functional ◽  
Condensation Reaction ◽  
3D Structure ◽  
Water Soluble ◽  
Microwave Assisted Synthesis ◽  
One Pot ◽  
Microwave Assisted ◽  
Td Dft

The(3R,4R,6R)-3-(((E)-2-hydroxybenzylidene)amino)-6-(hydroxymethyl)tetrahydro-2H-pyran-2,4,5-triol water-soluble Glucose amine Schiff base (GASB-1) product was made available by condensation of 2-hydroxybenzaldehyde with (3R,6R)-3-amino-6-(hydroxymethyl)-tetra-hydro-2H-pyran-2,4,5-triol under mono-mode microwave heating. A one-pot 5-minute microwave-assisted reaction was required to complete the condensation reaction with 90% yield and without having byproducts. The 3D structure of GASB-1 was solved from single crystal X-ray diffraction data and computed by DFT/6-311G(d,p). The Hirshfeld surface analysis (HSA), molecular electronic potential (MEP), Mulliken atomic charge (MAC), and natural population analysis (NPA) were performed. The IR and UV-Vis spectra were matched to their density functional theory (DFT) relatives and the thermal behavior was resolved in an open-room condition via thermogravimetry/Derivative thermogravimetry (TG/DTG) and differential scanning calorimetry (DSC). The highest occupied molecular orbital/lowest unoccupied molecular orbital (HOMO/LUMO), density of state (DOS), and time-dependence TD-DFT computations were correlated to the experimental electron transfer in water and acrylonitrile solvents.

Improvement of New Dianionic Ionic Liquids vs Monoanionic in Solubility of Poorly Water-Soluble Drugs

2021 ◽  
Author(s):  
Daniela A.S. Agostinho ◽  
Ana R. Jesus ◽  
Ana B.P. Silva ◽  
José M.S.S. Esperança ◽  
Alexandre Paiva ◽  
...  
Keyword(s):  
Ionic Liquids ◽  
Water Soluble ◽  
Poorly Water Soluble Drugs ◽  
Water Soluble Drugs ◽  
Poorly Water Soluble

scholarly journals Towards macrocyclic ionic liquids: novel ammonium salts based on tetrasubstituted p-tert-butylthiacalix[4]arenes

RSC Advances ◽  
2017 ◽  
Vol 7 (3) ◽  
pp. 1671-1686 ◽  
Author(s):  
Pavel L. Padnya ◽  
Elena A. Andreyko ◽  
Polina A. Gorbatova ◽  
Viktor V. Parfenov ◽  
Ildar Kh. Rizvanov ◽  
...  
Keyword(s):  
Ionic Liquids ◽  
Water Soluble ◽  
Ammonium Salts ◽  
Ammonium Ionic Liquids

Water-soluble and water-insoluble ammonium ionic liquids based on p-tert-butylthiacalix[4]arenes in cone and 1,3-alternate conformation were synthesized.

Microwave-Assisted Polymer Synthesis: State-of-the-Art and Future Perspectives

2004 ◽  
Vol 25 (20) ◽  
pp. 1739-1764 ◽  
Author(s):  
Frank Wiesbrock ◽  
Richard Hoogenboom ◽  
Ulrich S. Schubert
Keyword(s):  
State Of The Art ◽  
Polymer Synthesis ◽  
Future Perspectives ◽  
Microwave Assisted

Microwave Assisted Synthesis of Schiff Bases: A Green Approach

2012 ◽  
Vol 10 (1) ◽  
Author(s):  
Mousumi Chakraborty ◽  
Sanjay Baweja ◽  
Sunita Bhagat ◽  
TejpalSingh Chundawat
Keyword(s):  
Microwave Irradiation ◽  
Microwave Power ◽  
Mass Spectra ◽  
Molar Ratio ◽  
Microwave Assisted Synthesis ◽  
Schiff’S Bases ◽  
Microwave Assisted ◽  
Green Approach ◽  
Schiff's Bases ◽  
Effects Of Temperature

Abstract In the present study Schiff’s bases are synthesized by the conventional as well as by microwave irradiation. Excellent yield within short reaction time is obtained using microwave irradiation along with other advantages like mild reaction condition, non-hazardous and safer environmental conditions. The effects of temperature, reactant molar ratio, and microwave power variation on yield are observed. Mathematical model has been developed using matlab software to obtain the yield as a function of microwave power. Kinetic study of the reaction has also been attempted. Schiff’s bases structures are confirmed by IR, 1HNMR, Mass Spectra and elemental analysis.

scholarly journals Ionic Liquids as Doping Agents in Microwave Assisted Reactions

10.5772/51659 ◽  
2013 ◽  
Author(s):  
Marcos A. P. Martins ◽  
Jefferson Trindade ◽  
Guilherme S. ◽  
Lilian Buriol ◽  
Clarissa P.
Keyword(s):  
Ionic Liquids ◽  
As Doping ◽  
Microwave Assisted

Water-soluble TRIS-terminated PAMAM dendrimers: microwave-assisted synthesis, characterization and Cu(ii) intradendrimer complexes

RSC Advances ◽  
2015 ◽  
Vol 5 (74) ◽  
pp. 60581-60595 ◽  
Author(s):  
Ali Serol Ertürk ◽  
Mustafa Ulvi Gürbüz ◽  
Metin Tülü ◽  
Abdürrezzak Emin Bozdoğan
Keyword(s):  
Drug Carriers ◽  
Pamam Dendrimers ◽  
Water Soluble ◽  
Microwave Assisted Synthesis ◽  
Potential Drug ◽  
Microwave Assisted

Microwave-assisted synthesis, characterization and Cu(ii) complexes of water-soluble TRIS-terminated PAMAM dendrimers as novel potential drug carriers and templates for nanomaterials.

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