Liquid Chromatography with mass spectrometry analysis of mycotoxins in food samples using silica hydride based stationary phases

2017 ◽  
Vol 40 (9) ◽  
pp. 1953-1959 ◽  
Author(s):  
Joseph J. Pesek ◽  
Maria T. Matyska ◽  
Jessica F. Hoffmann ◽  
Nathalia A. Madruga ◽  
Rosane L. Crizel ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Liquid Chromatography ◽  
Stationary Phases ◽  
Food Samples ◽  
Mass Spectrometry Analysis ◽  
Spectrometry Analysis ◽  
Silica Hydride

Letter: High-Performance Liquid Chromatography/Electrospray Mass Spectrometry Analysis of the Mycotoxin Aurofusarin

2008 ◽  
Vol 14 (5) ◽  
pp. 329-333 ◽  
Author(s):  
Torsten Neuhof ◽  
Robert Köppen ◽  
Matthias Koch ◽  
Irene Nehls
Keyword(s):  
Mass Spectrometry ◽  
High Performance Liquid Chromatography ◽  
Liquid Chromatography ◽  
High Performance ◽  
Multiple Reaction Monitoring ◽  
Food Samples ◽  
Mass Spectrometry Analysis ◽  
Tandem Mass ◽  
Fragmentation Pattern ◽  
Spectrometry Analysis

High-performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) can be used for simultaneous quantification of various mycotoxins in contaminated food samples. Therefore, multi-mycotoxin methods have been developed in the last couple of years. To enlarge these methods for further analytes, we have developed a LC-MS/MS method for the quantification of the mycotoxin aurofusarin. Additionally, further LC-MS n experiments were performed to demonstrate the fragmentation pattern of aurofusarin. Applicable multiple reaction monitoring (MRM) transitions of aurofusarin were found and optimized by parameter variation of the tandem mass spectrometer. The applicability of the developed method was tested by analysis of naturally contaminated wheat.

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