Microwave-assisted extraction versus Soxhlet extraction to determine triterpene acids in olive skins

2017 ◽  
Vol 40 (5) ◽  
pp. 1209-1217 ◽  
Author(s):  
Ignacio Fernandez-Pastor ◽  
Antonia Fernandez-Hernandez ◽  
Sergio Perez-Criado ◽  
Francisco Rivas ◽  
Antonio Martinez ◽  
...  
Keyword(s):  
Soxhlet Extraction ◽  
Microwave Assisted Extraction ◽  
Microwave Assisted ◽  
Triterpene Acids ◽  
Assisted Extraction

scholarly journals Evaluation of Microwave-Assisted Extraction for the Analysis of Polychlorinated Biphenyls and Organochlorine Pesticides in Fish

2008 ◽  
Vol 91 (5) ◽  
pp. 1124-1129 ◽  
Author(s):  
Takamitsu Otake ◽  
Yoshie Aoyagi ◽  
Masahiko Numata ◽  
Takashi Yarita
Keyword(s):  
Polychlorinated Biphenyls ◽  
Organochlorine Pesticides ◽  
Soxhlet Extraction ◽  
Liquid Extraction ◽  
Isotope Dilution Method ◽  
Dilution Method ◽  
Microwave Assisted Extraction ◽  
Extraction Techniques ◽  
Microwave Assisted ◽  
Assisted Extraction

Abstract The efficiency of microwave-assisted extraction (MAE) was evaluated for the analysis of polychlorinated biphenyls (PCBs) and organochlorine pesticides (OCPs) in fish. An isotope dilution method was used for quantification via analysis of the samples by gas chromatography and mass spectrometry. MAE solvent, temperature, and time were optimized, and observed concentrations were compared. The MAE results were also compared to those of other extraction techniques (Soxhlet extraction, pressurized liquid extraction, saponification, and homogenization). Concentrations of PCBs and OCPs obtained by MAE at 120C for 10 min were comparable to those by the other techniques. The results suggest that MAE can be used for the analysis of PCBs and OCPs in fish.

scholarly journals Microwave-Assisted Extraction as an Alternative to Soxhlet, Sonication, and Supercritical Fluid Extraction

1996 ◽  
Vol 79 (1) ◽  
pp. 142-156 ◽  
Author(s):  
Viorica Lopez-A Vila ◽  
Richard Young ◽  
Nataly Teplitsky
Keyword(s):  
Supercritical Fluid Extraction ◽  
Supercritical Fluid ◽  
Soxhlet Extraction ◽  
Standard Reference Materials ◽  
Microwave Assisted Extraction ◽  
Fluid Extraction ◽  
Microwave Assisted ◽  
Spiked Soil ◽  
Assisted Extraction ◽  
Relative Standard

Abstract Microwave-assisted extraction (MAE), Soxhlet, soni cation, and supercritical fluid extraction (SFE) were compared in their ability to extract 95 compounds listed in U.S. Environmental Protection Agency Method 8250. Freshly spiked soil samples and 2 standard reference materials were extracted with hexane-acetone (1 + 1) by MAE and Soxhlet extraction, with methylene chloride-acetone (1 + 1) by sonication extraction, and with supercritical carbondioxide modified with 10% methanol by SFE. Results indicate that MAE is a promising extraction technique. Of 94 compounds for which we are reporting data, 51 compounds gave MAE recoveries of >80%; 33,50-79%; 8,20-49%; and 2, <19%. Soxhlet extraction gave very similar results: 50 recoveries were >80%; 32,50-79%; 8,20-49%; and 4, <19%. Sonica tion recoveries were slightly higher: 63 values were >80%; 25,50-79%; 4,20-49%; and 2, <19%. SFE recoveries were the lowest: 37 values were >80%; 37, 50-79%; 12,20-49%, and 8, <19%. MAE gave the best precision: relative standard deviations (RSDs) were <10% for 90 of 94 compounds. Soxhlet extraction gave the worst precision: only 52 of 94 samples gave RSDs ≤10%. Although MAE looks promising, 15 polar basic compounds extracted at 115°C with hexane acetone for 10 min (1000 W power) gave poor recoveries. Because no technique gave acceptable recoveries for these polar compounds, we investigated their extraction with MAE using acetonitrile at 50° and 115°C. Ten of the 15 compounds were quantitatively recovered (>70%) with acetonitrile at 115°C.

Comparison of microwave-assisted extraction and Soxhlet extraction for phenols in soil samples using experimental designs

The Analyst ◽  
1998 ◽  
Vol 123 (8) ◽  
pp. 1679-1684 ◽  
Author(s):  
A. Egizabal ◽  
O. Zuloaga ◽  
N. Etxebarria ◽  
L. A. Fernández ◽  
J. M. Madariaga
Keyword(s):  
Soxhlet Extraction ◽  
Soil Samples ◽  
Experimental Designs ◽  
Microwave Assisted Extraction ◽  
Microwave Assisted ◽  
Assisted Extraction

A Comparison Study on Microwave-Assisted Extraction of Catalpol from Rehmannia glutinosa Libosch with Conventional Methods

2014 ◽  
Vol 1033-1034 ◽  
pp. 329-336
Author(s):  
Xiu Li Zhang ◽  
Chun Li Li ◽  
Xue Yin ◽  
Xin Yun Su ◽  
De Hong Yu
Keyword(s):  
Soxhlet Extraction ◽  
Ultrasonic Extraction ◽  
Microwave Assisted Extraction ◽  
Rehmannia Glutinosa ◽  
Extraction Technology ◽  
Considerable Saving ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Percentage Extraction ◽  
Rehmannia Glutinosa Libosch

Catalpol, an iridoid glycoside, has been verified to be of neuroprotection and may be a potential agent for the treatment of neurodegenerative disease. The extraction technology of catalpol has been tested in this paper. We used different extraction methods including extraction at room temperature (ERT), heat reflux extraction, Soxhlet extraction, ultrasonic extraction and microwave-assisted extraction (MAE) to evaluat the percentage extraction of catapol fromRehmannia glutinosa Libosch.The extracts were analyzed by high performance liquid chromatography (HPLC). Methanol (100%, v/v) extracted high percentage extraction of catapol compared to ethanol (60%, v/v) which achieved the highest percentage extraction of catapol in different concentration of ethanol. The results showed that the percentage extraction of catalpol fromRehmannia glutinosa Liboschby MAE was more efficient in short time followed by ultrasonic extraction, Soxhlet extraction, heat reflux extraction and ERT methods. MAE has need of 4 min, whereas ultrasonic extraction, Soxhlet extraction, heat reflux extraction and ERT techniques require 70, 140, 180 min and 60 h respectively, to leach higher percentage extraction of catalpol. The time taken by MAE was nearly 18 times less than the ultrasonic extraction, 35 times less than Soxhlet extraction, 45 times less than heat reflux extraction and 900 times less than ERT for the highest percentage extraction of catalpol. The present results showed that the high extraction efficiency and considerable saving of time by MAE were more competent than the conventional extraction techniques.

Microwave-assisted extraction versus Soxhlet extraction in the analysis of 21 organochlorine pesticides in plants

2003 ◽  
Vol 1008 (1) ◽  
pp. 115-122 ◽  
Author(s):  
M Barriada-Pereira ◽  
E Concha-Graña ◽  
M.J González-Castro ◽  
S Muniategui-Lorenzo ◽  
P López-Mahı́a ◽  
...  
Keyword(s):  
Organochlorine Pesticides ◽  
Soxhlet Extraction ◽  
Microwave Assisted Extraction ◽  
Microwave Assisted ◽  
Assisted Extraction

scholarly journals Microwave-assisted extraction of flavonoids from Phyllostachys heterocycla leaves: Optimization, mechanism, and antioxidant activity in vitro

BioResources ◽  
2021 ◽  
Vol 16 (4) ◽  
pp. 8060-8081
Author(s):  
Jie Xu ◽  
Jianjun Wu ◽  
Juan Qi ◽  
Juan Li ◽  
Yongju Liu ◽  
...  
Keyword(s):  
Antioxidant Activities ◽  
Radical Scavenging ◽  
Soxhlet Extraction ◽  
Extraction Yield ◽  
Microwave Assisted Extraction ◽  
Extraction Technology ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Phyllostachys Heterocycla

Flavonoids were extracted from Phyllostachys heterocycla leaves by adopting microwave-assisted extraction technology. Based on the single factor experiment and Plackett-Burman design results, the extraction process of flavonoids was further optimized using the response surface methodology. The optimum conditions were as follows: an ethanol concentration of 78.1%, an extraction time of 24.9 min, and a microwave power of 559 W. Under these conditions, the extraction yield of flavonoids was 4.67%, which was in close proximity to the predicted value (4.70%) and higher than the extraction yield from traditional Soxhlet extraction (3.35%). Moreover, the possible extraction mechanisms of these two extraction methods were further derived to explain why the microwave-assisted extraction of flavonoids was more efficient compared with traditional Soxhlet extraction. Ultimately, the antioxidant activities in vitro of flavonoids from Phyllostachys heterocycla leaves were evaluated via DPPH and ABTS radical scavenging assay. The flavonoids from Phyllostachys heterocycla leaves exhibited excellent antioxidant activities in vitro and Phyllostachys heterocycla leaves could be a new natural source for developing antioxidants. Overall, the findings of this research could provide a theoretical reference for the further comprehensive development and utilization of bamboo resources.

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