Chromatographic determination of biogenic amines in four typical Italian cheeses: correlations with processing and nutritional characteristics through a chemometric approach

2019 ◽  
Vol 99 (11) ◽  
pp. 4963-4968
Author(s):  
Luca Rivoira ◽  
Michele Castiglioni ◽  
Maria Concetta Bruzzoniti
1993 ◽  
Vol 76 (3) ◽  
pp. 575-577 ◽  
Author(s):  
Susanna Eerola ◽  
Riitta Hinkkanen ◽  
Erja Lindfors ◽  
Timo Hirvi

Abstract National Veterinary Institute, Department of Chemistry, SF-00101, Helsinki, Finland A liquid chromatographic method is described for the determination of biogenic amines found in dry sausages: tryptamine, phenylethylamine, putrescine, cadaverine, histamine, serotonin, tyramine, spermidine, and spermine. Amines were extracted with perchloric acid solution and derivatized with dansyl chloride. After derivatization, ammonia was added to remove an interfering peak near cadaverine. Liquid chromatographic separations were performed by using a Spherisorb ODS2 column and an ammonium acetate-acetonitrile gradient elution program. The limits of determination of the individual amines were 1-5 mg/kg. This method is also applicable to detection of amines in other food samples.


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