Rapid method for the simultaneous determination of glucose and fructose using anthrone reagent

1968 ◽  
Vol 19 (10) ◽  
pp. 597-601 ◽  
Author(s):  
J. W. de Bruyn ◽  
H. A. Van Keulen ◽  
J. H. A. Ferguson
Keyword(s):  
Simultaneous Determination ◽  
Rapid Method ◽  
Anthrone Reagent

scholarly journals Determination of Residues of Flumequine and 7-Hydroxyflumequine in Edible Sheep Tissues by Liquid Chromatography with Fluorimetric and Ultraviolet Detection

1998 ◽  
Vol 81 (3) ◽  
pp. 519-527 ◽  
Author(s):  
Jean-michel Delmas ◽  
Anne-marie Chape ◽  
Pascal Sanders
Keyword(s):  
Liquid Chromatography ◽  
Ethyl Acetate ◽  
Simultaneous Determination ◽  
Rapid Method ◽  
Active Metabolite ◽  
Fluorimetric Detection ◽  
Ultraviolet Detection ◽  
Tissue Extracts ◽  
Edible Tissues

abstract A simple, sensitive, and rapid method for simultaneous determination of residues of flumequine and its microbiologically active metabolite 7-hydroxyflumequine in 100 mg sheep edible tissues (muscle, liver, kidney, and fat) by liquid chromatography is reported. After liquid-liquid cleanup with ethyl acetate, tissue extracts were injected onto a Select B column. The 2 compounds were determined by ultraviolet and fluorimetric detection. The method was repeatable and reproducible for flumequine and 7-hydroxyflumequine in muscle, liver, kidney, and fat, with limits of detection below 2 and 3 μg/kg for flumequine and 7-hydroxyflumequine, respectively. Mean recoveries for flumequine were 90 ± 7, 82 ± 7,89 ± 5, and 82 ± 6% in muscle, liver, kidney, and fat, respectively. Mean recoveries for 7-hydroxyflumequine were 91 ± 2, 90 ± 4, 86 ± 3, and 84 ± 4% in muscle, liver, kidney, and fat, respectively.

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