In situ Raman scattering studies of high-pressure stability and transformations in the matrix of a nanostructured glass-ceramic composite

2005 ◽  
Vol 36 (10) ◽  
pp. 938-945 ◽  
Author(s):  
Kristina E. Lipinska-Kalita ◽  
Stephen A. Gramsch ◽  
Patricia E. Kalita ◽  
Russell J. Hemley
2011 ◽  
Vol 134 (23) ◽  
pp. 234503 ◽  
Author(s):  
T. Deschamps ◽  
C. Martinet ◽  
D. de Ligny ◽  
J. L. Bruneel ◽  
B. Champagnon

2017 ◽  
Vol 73 (9-10) ◽  
pp. 381-385 ◽  
Author(s):  
V. A. Rozenenkova ◽  
S. S. Solntsev ◽  
N. A. Mironova ◽  
S. V. Gavrilov

2012 ◽  
Vol 512-515 ◽  
pp. 671-675 ◽  
Author(s):  
Ai Guo Zhou ◽  
Liang Li ◽  
Tai Chao Su ◽  
Shang Sheng Li

Ti3SiC2, a ternary carbide, was proposed at this paper to use as the binder of polycrystalline diamonds to overcome the weaknesses of traditional metal binders and ceramic binders. Ti3SiC2was first reported to be in-situ synthesized under high pressure (4GPa) and at high temperature (1400°C) (HPHT) from the mixtures of Ti, Si and graphite powders or the mixture of Ti, SiC and graphite powders. Ti3SiC2-damond composites were also made at HPHT from the previous mixtures and diamond particles. TiCx, Ti5Si3Cxand TiSi2were main impurities and/or intermediate products of Ti3SiC2samples synthesized at HPHT. Ti3SiC2content increased as synthesized time increased from 10 min to 60 min. For as-synthesized composites, diamond particles were evenly distributed in matrix. The diamond particles are bonded well with the matrix by three types of interface.


2013 ◽  
Vol 45 (3) ◽  
pp. 331-339
Author(s):  
A. Faeghi-Nia

An Apatite-Wollastonite-Phlogopite glass-ceramic composite, was developed by sintering and crystallization of the powdered glass. The non-isothermal and isothermal sintering kinetics were studied for this glass-ceramic. Hot-stage microscopy (HSM) measurements demonstrated that it is possible to sinter and crystallize this glass-ceramic with 80% relative density. The activation energy of sintering was analyzed using previously reported model of sintering and it was obtained Q=193.83 KjmolK-1. Also it was shown that the microstructure of sample is a function of particle size distribution.


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