Differential Thermal Analysis and X-Ray Diffraction Studies of Griseofulvin−Succinic Acid Solid Dispersions

1973 ◽  
Vol 62 (3) ◽  
pp. 498-501 ◽  
Author(s):  
Win Loung Chiou ◽  
Sarfaraz Niazi
Keyword(s):  
Thermal Analysis ◽  
Differential Thermal Analysis ◽  
Succinic Acid ◽  
Solid Dispersions ◽  
X Ray Diffraction ◽  
X Ray

PENINGKATAN LAJU DISOLUSI ACYCLOVIR DENGAN METODE SISTEM DISPERSI PADAT MENGGUNAKAN POLOXAMER 188

2016 ◽  
Vol 5 (1) ◽  
pp. 6
Author(s):  
Budi Setiawan ◽  
Erizal Zaini ◽  
Salman Umar
Keyword(s):  
Electron Microscopy ◽  
Thermal Analysis ◽  
Scanning Electron Microscopy ◽  
Fourier Transform ◽  
Differential Thermal Analysis ◽  
Fourier Transform Infrared ◽  
X Ray Diffraction ◽  
Poloxamer 188 ◽  
X Ray ◽  
Scanning Electron

Sebuah penelitian tentang sistem dispersi padat dari asiklovir dengan poloxamer 188 telah dilakukan formulasi dengan pencampuran secara fisika dengan rasio 1 : 1, 1 : 3, 1 : 5 dan dispersi padat 1 : 1, 1 : 3, 1 : 5 dan penggilingan 1:1 sebagai pembanding. Dispersi padat dibuat menggunakan metode pencairan (fusi), yang digabung dengan poloxamer 188 pada hotplate kemudian asiklovir dimasukkan ke dalam hasil poloxamer 188 lalu di kocok hingga membentuk masa homogen. Semua formula yang terbentuk termasuk asiklovir poloxamer 188 murni dianalisis karakterisasinya dengan Differential Thermal Analysis (DTA), X-ray Diffraction, Scanning Electron Microscopy (SEM), dan Fourier Transform Infrared (FTIR), kemudian pengambilan dilakukan  (penentuan kadar) mengunakan spektrofotometer UV pada panjang gelombang 257,08 nm dan uji laju disolusi dengan aquadest bebas CO2 menggunakan metode dayung. Hasil pengambilan  (penentuan kadar) menunjukkan bahwa semua formula memenuhi persyaratan farmakope Amerika edisi 30 dan farmakope Indonesia edisi 4 yaitu 95-110%. Sedangkan hasil uji laju disolusi untuk campuran fisik 1: 1, dan dispersi padat 1: 1, dan penggilingan 1: 1 menunjukkan peningkatan yang nyata dibandingkan asiklovir murni. Hal ini juga dapat dilihat dari hasil perhitungan statistik  menggunakan analisis varian satu arah  SPSS 17.

scholarly journals The Potential for Natural Stones from Northeastern Brazil to Be Used in Civil Construction

Minerals ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 440
Author(s):  
Fabiana Pereira da Costa ◽  
Jucielle Veras Fernandes ◽  
Luiz Ronaldo Lisboa de Melo ◽  
Alisson Mendes Rodrigues ◽  
Romualdo Rodrigues Menezes ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Thermal Analysis ◽  
Differential Thermal Analysis ◽  
Chemical Resistance ◽  
Mechanical Analysis ◽  
Northeastern Brazil ◽  
X Ray Diffraction ◽  
X Ray ◽  
Chemical Agents ◽  
Natural Stones

Natural stones (limestones, granites, and marble) from mines located in northeastern Brazil were investigated to discover their potential for use in civil construction. The natural stones were characterized by chemical analysis, X-ray diffraction, differential thermal analysis, and optical microscopy. The physical-mechanical properties (apparent density, porosity, water absorption, compressive and flexural strength, impact, and abrasion) and chemical resistance properties were also evaluated. The results of the physical-mechanical analysis indicated that the natural stones investigated have the potential to be used in different environments (interior, exterior), taking into account factors such as people’s circulation and exposure to chemical agents.

The Roman Ceramics of Salobrena (Granada-Spain) and their Raw Materials

1992 ◽  
Vol 267 ◽  
Author(s):  
Ana M De Andres ◽  
Isabel MuÑOZ
Keyword(s):  
Thermal Analysis ◽  
Differential Thermal Analysis ◽  
Raw Materials ◽  
Third Century ◽  
Western Coast ◽  
X Ray Diffraction ◽  
X Ray ◽  
The Third ◽  
Good Number ◽  
Scanning Electron

ABSTRACTNineteen roman ceramic sherds found near Salobreña (Granada, Spain), in the western coast of the Mediterranean Sea, as well as different ceramic clays from the surroundingsare studied. Both clays and ceramic sherds are characterizad by X-ray diffraction and spectrometry, differential thermal analysis, and scanning electron and optical microscopies. A good number of the ceramic pieces, among which some “Terrae Sigillatae”, have a composition similar to that of the local clays and, thus, have been probably manufactured at Salobreña. Only a few of them have a foreign origin. For most of them, the firing temperature was about 800-850 °C, although some have been produced at 900-1000 °C, and some others at 1000-1100 °C. It is concluded that Salobreña appearsto have been an important settlement just in the third century of the Christian era.

scholarly journals Silica-Kaolin Mix Effect on Evaporative Pattern Castings Surface Roughness

2016 ◽  
Vol 16 (3) ◽  
pp. 83-88 ◽  
Author(s):  
B.V. Omidiji ◽  
R.H. Khan ◽  
M.S. Abolarin
Keyword(s):  
Thermal Analysis ◽  
Surface Roughness ◽  
Differential Thermal Analysis ◽  
Ratio Method ◽  
Gating System ◽  
X Ray Diffraction ◽  
Pouring Temperature ◽  
Material Loss ◽  
Refractory Coating ◽  
X Ray

Abstract The influence of the refractory coating which is a mixture of silica flour and kaolin on the surface roughness of the plate castings produced using evaporative patterns had been considered in this work. The kaolin was used as a binder and ratio method was employed to form basis for the factorial design of experiment which led to nine runs of experiments. Methyl alcohol at 99% concentration was used as the carrier for the transfer of the coating to the surface of the patterns. Pouring temperature was observed as a process parameter alongside the mix ratios of the coating. Attempts were made to characterize the refractory coating by using two methods; differential thermal analysis (DTA) and X-ray diffraction. Attempt was also made to characterize the casting material. Gating system design was done for the plate casting to determine the correct proportions of the gating parameters in order to construct the gating system properly to avoid turbulence during pouring of liquid metal. A digital profilometer was used to take the measurements of the surface roughness. It was observed that the mix ratio 90% silica flour-10% kaolin produced the lowest value of the surface roughness of the plate castings and had the lowest material loss in the DTA test. The pouring temperature of 650°C produced best casting.

scholarly journals SOLUBILITY OF GERMANIUM DISELENIDE IN THE Cu3AsSe4

2021 ◽  
Vol 0 (4) ◽  
pp. 67-70
Author(s):  
Z.T. Hasanova ◽  
Keyword(s):  
Thermal Analysis ◽  
Differential Thermal Analysis ◽  
Phase Equilibria ◽  
Solid Solutions ◽  
X Ray Diffraction ◽  
X Ray

Differential thermal analysis and powder X-ray diffraction methods were used for phase equilibria studying in the Cu3AsSe4-GeSe2 system. It was established that wide (up to 30 mol.%) solid solutions based on Cu3AsSe4 are formed. GeSe2-rich alloys consist of various heterogeneous mixtures, including phases outside the T–x plane of this section

The (AgInSe2)1-x(VSe)x system (0 ≤x ≤ 0.5): X-ray diffraction and differential thermal analysis measurements

2005 ◽  
Vol 2 (10) ◽  
pp. 3766-3769 ◽  
Author(s):  
S. Durán ◽  
P. Grima ◽  
M. Muñoz ◽  
M. Quintero ◽  
J. Ruiz ◽  
...  
Keyword(s):  
Thermal Analysis ◽  
Differential Thermal Analysis ◽  
X Ray Diffraction ◽  
X Ray

Purification of Bentonite Clays from Cubati, PB, Brazil, for Diversified Applications

2014 ◽  
Vol 805 ◽  
pp. 486-491
Author(s):  
J.M.R. Figueirêdo ◽  
Juliana Melo Cartaxo ◽  
I.A. Silva ◽  
C.D. Silva ◽  
Gelmires Araújo Neves ◽  
...  
Keyword(s):  
Thermal Analysis ◽  
Differential Thermal Analysis ◽  
Chemical Analysis ◽  
Laser Diffraction ◽  
The State ◽  
X Ray Diffraction ◽  
X Ray ◽  
Granulometric Analysis ◽  
Bentonite Clays

The State of Paraíba, Brazil, retains about 88.5% of all Brazilian bentonite, and much of this production comes from deposits in the District of Boa Vista, PB. Nevertheless, the deposits are almost depleted. Recently, new deposits were found, which will increases the reserves of the State, in the regions of Cubati and Pedra Lavrada, PB. The objective of this work is to characterize and develop purified clays, through sieving and hydrocycloning techniques, from those recently discovered bentonites for several applications. The characterization of the sample was done through granulometric analysis by laser diffraction, X-ray diffraction, chemical analysis by X-ray fluorescence, and thermogravimetric and differential thermal analysis. The results show that the samples are typical of bentonite clays, and that the purification solely by hydrocyclone presents the best results.

Vacuum Carburization of Nanometer Tungsten Powder with Carbon Black

2007 ◽  
Vol 534-536 ◽  
pp. 165-168 ◽  
Author(s):  
Luo Ji ◽  
Lin Tao ◽  
Zhi Meng Guo ◽  
Cheng Chang Jia
Keyword(s):  
Thermal Analysis ◽  
Differential Thermal Analysis ◽  
Surface Area ◽  
Tungsten Powder ◽  
Bet Surface Area ◽  
X Ray Diffraction ◽  
X Ray ◽  
X Ray Scattering ◽  
Vacuum Carburization ◽  
Dta Curves

Vacuum carburization of nanometer tungsten powder was investigated in a simple designed apparatus. An X-Y recorder was used to plot differential thermal analysis (DTA) curves to determine the starting temperature of carburization of four samples with different specific surface area. The product was characterized by X-ray Diffraction (XRD) and small angle X-ray scattering (SAXS). The results show that finer tungsten powder has lower starting temperature of carburization. Tungsten powder, the BET surface area of which is 32.97m2/g, was completely carburized to tungsten carbide at 1050°C, even though the starting temperature was 890°C. The particle was found to grow sharply before carburization.

Solid phase precipitates in (Zr,Th)-OH-(oxalate, malonate) ternary aqueous system

2009 ◽  
Vol 97 (4-5) ◽  
Author(s):  
Taishi Kobayashi ◽  
Takayuki Sasaki ◽  
I. Takagi ◽  
Hirotake Moriyama
Keyword(s):  
Thermal Analysis ◽  
Differential Thermal Analysis ◽  
Solid Phase ◽  
Aqueous System ◽  
Carboxylate Ligand ◽  
X Ray Diffraction ◽  
Large Excess ◽  
X Ray ◽  
Acidic Conditions ◽  
Solid Phases

AbstractThe solubility-limiting solid phases in the ternary aqueous systems of Zr(IV)/OH/oxalate, Zr(IV)/OH/malonate, Th(IV)/OH/oxalate and Th(IV)/OH/malonate were characterized by elemental analysis, X-ray diffraction, thermogravimetric analysis and differential thermal analysis. The ternary solid phase of M(IV)/OH/carboxylate was observed to form, even under acidic conditions, depending on the pH and the concentration of carboxylate ligand. In the presence of a large excess of carboxylic acid, however; the binary M(IV)-carboxylate solid phase formed.

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