Development, validation and application to real samples of a multiresidue LC-MS/MS method for determination of β2-agonists and anabolic steroids in bovine hair

2014 ◽  
Vol 49 (9) ◽  
pp. 936-946 ◽  
Author(s):  
M. Leporati ◽  
M. Bergoglio ◽  
P. Capra ◽  
E. Bozzetta ◽  
M. C. Abete ◽  
...  
Keyword(s):  
Anabolic Steroids ◽  
Real Samples ◽  
Β2 Agonists

scholarly journals Applicability of Cork as Novel Modifiers to Develop Electrochemical Sensor for Caffeine Determination

Materials ◽  
2020 ◽  
Vol 14 (1) ◽  
pp. 37
Author(s):  
Mayra K. S. Monteiro ◽  
Djalma R. Da Silva ◽  
Marco A. Quiroz ◽  
Vítor J. P. Vilar ◽  
Carlos A. Martínez-Huitle ◽  
...  
Keyword(s):  
Electrochemical Sensor ◽  
Linear Response ◽  
High Performance ◽  
Low Cost ◽  
Pharmaceutical Formulations ◽  
Caffeine Concentration ◽  
Real Samples ◽  
Wide Range ◽  
Potential Use

This study aims to investigate the applicability of a hybrid electrochemical sensor composed of cork and graphite (Gr) for detecting caffeine in aqueous solutions. Raw cork (RAC) and regranulated cork (RGC, obtained by thermal treatment of RAC with steam at 380 °C) were tested as modifiers. The results clearly showed that the cork-graphite sensors, GrRAC and GrRGC, exhibited a linear response over a wide range of caffeine concentration (5–1000 µM), with R2 of 0.99 and 0.98, respectively. The limits of detection (LOD), estimated at 2.9 and 6.1 µM for GrRAC and GrRGC, suggest greater sensitivity and reproducibility than the unmodified conventional graphite sensor. The low-cost cork-graphite sensors were successfully applied in the determination of caffeine in soft drinks and pharmaceutical formulations, presenting well-defined current signals when analyzing real samples. When comparing electrochemical determinations and high performance liquid chromatography measurements, no significant differences were observed (mean accuracy 3.0%), highlighting the potential use of these sensors to determine caffeine in different samples.

A “turn-on” small molecule fluorescent sensor for the determination of Al3+ ion in real samples: theoretical calculations, and photophysical and electrochemical properties

2021 ◽  
Vol 45 (39) ◽  
pp. 18400-18411
Author(s):  
Süreyya Oğuz Tümay ◽  
Ahmet Şenocak ◽  
Arif Mermer
Keyword(s):  
Small Molecule ◽  
Fluorescent Sensor ◽  
Theoretical Calculations ◽  
Sample Analysis ◽  
Fluorescence Sensing ◽  
Paper Test ◽  
Real Samples ◽  
Real Sample Analysis ◽  
Turn On

The fluorescence sensing properties of a naphthalene-based acetohydrazide (3) were investigated. A highly selective “turn-on” response was obtained towards Al3+ ions, and this was used for real sample analysis and development of paper test strips.

Design of a novel optical sensor for determination of trace amounts of copper by UV–visible spectrophotometry in real samples

2017 ◽  
Vol 32 (3) ◽  
pp. e4110
Author(s):  
Eslam Pourbasheer ◽  
Somayeh Morsali ◽  
Zhila Azari ◽  
Mohammad Ali Karimi ◽  
Mohammad Reza Ganjali
Keyword(s):  
Optical Sensor ◽  
Real Samples ◽  
Visible Spectrophotometry ◽  
Uv Visible

scholarly journals A novel ratiometric fluorescent probe for the selective determination of HClO based on the ESIPT mechanism and its application in real samples

RSC Advances ◽  
2019 ◽  
Vol 9 (53) ◽  
pp. 30943-30951 ◽  
Author(s):  
Jingrui Li ◽  
Aijun Gong ◽  
Guoqing Shi ◽  
Chengwen Chai
Keyword(s):  
Fluorescent Probe ◽  
Real Samples ◽  
Selective Determination ◽  
Ratiometric Fluorescent Probe

Based on the ESIPT fluorescence mechanism, herein, a novel ratiometric fluorescent probe was designed and synthesized for the detection of HClO.

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