One-Pot Synthesis of New 1,5-Disubstituted Tetrazoles Bearing 2,2-Bis(trimethylsilyl)ethenyl Groups via The Ugi Four-Component Condensation Reaction Catalyzed by MgBr2·2Et2O

2013 ◽  
Vol 51 (1) ◽  
pp. 80-84 ◽  
Author(s):  
Kazem D. Safa ◽  
Tohid Shokri ◽  
Hassan Abbasi ◽  
Reza Teimuri-Mofrad
Author(s):  
Naser Foroughifar ◽  
Akbar Mobinikhaledi ◽  
Mohammad Ali Bodaghi Fard ◽  
Hassan Moghanian ◽  
Sattar Ebrahimi

2006 ◽  
Vol 84 (3) ◽  
pp. 433-437 ◽  
Author(s):  
Kamal K Kapoor ◽  
Bilal A Ganai ◽  
Satish Kumar ◽  
Charanjeet S Andotra

The antimony(III) chloride impregnated on alumina efficiently catalyses a one-pot, three-component condensation reaction among an aldehyde, a β-ketoester, and urea or thiourea to afford the corresponding dihydropyrimidinones in good to excellent yields. The reactions are probed in microwave (MW), ultrasonic, and thermal conditions and the best results are found using MW under solvent-free conditions.Key words: Biginelli dihydropyrimidinones synthesis, SbCl3–Al2O3, MW, sonication, solid supported.


RSC Advances ◽  
2020 ◽  
Vol 10 (20) ◽  
pp. 11808-11815 ◽  
Author(s):  
Suhas G. Patil ◽  
Jagannath S. Jadhav ◽  
Sagar T. Sankpal

A novel Mg3N2-assisted one-pot annulation strategy has been developed via cyclo-condensation reaction of 2-pyridyl ketones with alkyl glyoxylates or aldehydes, allowing the formation of imidazo[1,5-a]pyridines exclusively with an exellent yield.


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