Synthesis and characterization of a noncytotoxic, X-ray opaque polyurethane containing iodinated hydroquinone bis(2-hydroxyethyl) ether as chain extender for biomedical applications

2013 ◽  
Vol 102 (9) ◽  
pp. 3207-3215 ◽  
Author(s):  
S. Kiran ◽  
Roy Joseph
Keyword(s):  
Biomedical Applications ◽  
Chain Extender ◽  
Synthesis And Characterization ◽  
X Ray

Study and Characterization of Powders Nanocomposites Calcium Phosphate/Silica-Gel (SiO2n) Obtained from Attrition Milling: For Biomedical Applications

2008 ◽  
Vol 396-398 ◽  
pp. 615-618
Author(s):  
Rodrigo Brandão ◽  
Fernando Pupio ◽  
Nelson Heriberto A. Camargo ◽  
E. Gemelli
Keyword(s):  
Calcium Phosphate ◽  
Silica Gel ◽  
Biomedical Applications ◽  
Bone Matrix ◽  
Synthesis And Characterization ◽  
X Ray Diffraction ◽  
X Ray ◽  
Attrition Milling ◽  
Bone Calcium

The bioceramics nanostructured have made important characteristics in biomedical applications, especially the calcium phosphate ceramics. The aim of this work is synthesis and characterization of calcium phosphate and nanocomposites powders, the method of dissolution of CaO in liquid medium, precipitation and formation of bone calcium phosphate matrix, and nanocomposites by adding the solution of phosphoric acid (H3PO4). The nanocomposites powders were synthesized using as strengthening silica gel nanometer (20nm) at concentrations of 1%, 2%, 3% and 5% by volume and subjected to heat treatment to 900°C for 2 hours, seeking obtained HA (Hydroxyapatite). Later the bone matrix of calcium phosphate and nanocomposites powders were subjected from process attrition milling for 2 hours, by way of comparison. The studies characterizations were conducted through the technique of X-ray diffraction, scanning electron microscopy (SEM) and dilatometric test.

scholarly journals Synthesis and Characterization of SPIONs for Biomedical applications

2014 ◽  
Vol 70 (a1) ◽  
pp. C743-C743
Author(s):  
Tatiane Britos ◽  
Li Min ◽  
Lilia De Souza Li ◽  
Paula Haddad
Keyword(s):  
Biomedical Applications ◽  
Superparamagnetic Iron Oxide ◽  
Cell Types ◽  
Synthesis And Characterization ◽  
X Ray Diffraction ◽  
X Ray ◽  
Mercaptosuccinic Acid ◽  
Transmission Electron ◽  
Oxidized Iron

This work reports the synthesis and characterization of superparamagnetic iron oxide nanoparticles (SPIONs), with great potential for biomedical applications. SPIONs were prepared through a decomposition of Fe(acac)3 in the presence of 1,2 hexadecanodiol (reducing agent), oleic acid and oleylamine (ligands) in a hot organic solvent. The mercaptosuccinic acid (MSA) and 2,3- dimercaptosuccinic acid (DMSA) were exchanged onto the nanocrystal surface making the particles stable in water. The thiolated nanoparticles (SH-NPs) were characterized by Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), transmission electron microscopy (TEM), and vibrating sample magnetometry (VSM). The as-prepared sample presented an amorphous partially oxidized iron structure. The results showed that the SH-NPs have a mean diameter of 6 nm and display superparamagnetic behavior at room temperature. Preliminary tests of incorporation of these systems were evaluated in Hela cells and stem cells. The results showed that the thiolated nanoparticles have no toxic effects for both cell types with good incorporation after 6 hours of transfection. Magnetic resonance image (MRI) were also carried and showed that the MNPs increase the contrast in systems investigated. Acknowledgements: FAPESP (2011/10125-0), CNPq, CAPES, UNICAMP

Synthesis and Characterization of Ceramic Modified with Niobium for Biomedical Applications

2016 ◽  
Vol 869 ◽  
pp. 884-889
Author(s):  
Nadia Sueli Vieira Capanema ◽  
Alexandra A.P. Mansur ◽  
Herman Sander Mansur
Keyword(s):  
Biomedical Applications ◽  
Room Temperature ◽  
Structural Changes ◽  
Calcium Phosphates ◽  
Synthesis And Characterization ◽  
Body Parts ◽  
New Materials ◽  
X Ray Diffraction ◽  
X Ray

The need for obtaining new materials to replace human body parts that were destroyed or damaged led scientists from different areas of research for developing new biomaterials. Thus, the aim of this work was the synthesis and characterization of niobium-modified apatite bioceramics. Calcium phosphates (CaP) were synthesized with niobium partially replacing calcium sites using aqueous precipitation route at room temperature. The bioceramics, with and without Nb incorporation, were characterized by scanning electron microscopy (SEM) coupled with energy dispersive spectroscopy (EDS) and X-ray diffraction (XRD) as prepared and after heat treatments The results indicated that Nb was incorporated in the apatite structure promoting morphological and structural changes in the ceramic properties.

Synthesis and characterization of TiN / Ti / AISI 410 coatings

2018 ◽  
Vol 2 (1) ◽  
pp. 7
Author(s):  
S Chirino ◽  
Jaime Diaz ◽  
N Monteblanco ◽  
E Valderrama
Keyword(s):  
Synthesis And Characterization ◽  
Photoemission Spectroscopy ◽  
X Ray Diffraction ◽  
X Ray ◽  
Columnar Grains ◽  
Tin Thin Films ◽  
Steel Aisi ◽  
Interacting Surfaces ◽  
Stainless Steel Aisi

The synthesis and characterization of Ti and TiN thin films of different thicknesses was carried out on a martensitic stainless steel AISI 410 substrate used for tool manufacturing. The mechanical parameters between the interacting surfaces such as thickness, adhesion and hardness were measured. By means of the scanning electron microscope (SEM) the superficial morphology of the Ti/TiN interface was observed, finding that the growth was of columnar grains and by means of EDAX the existence of titanium was verified.  Using X-ray diffraction (XRD) it was possible to observe the presence of residual stresses (~ -3.1 GPa) due to the different crystalline phases in the coating. Under X-ray photoemission spectroscopy (XPS) it was possible to observe the molecular chemical composition of the coating surface, being Ti-N, Ti-N-O and Ti-O the predominant ones.

scholarly journals Synthesis and characterization of Fe, Co, and Ni colloids in 2-mercaptoethanol

2020 ◽  
Vol 10 ◽  
pp. 184798042096688
Author(s):  
Galo Cárdenas-Triviño ◽  
Sergio Triviño-Matus
Keyword(s):  
Electron Microscopy ◽  
Electron Diffraction ◽  
Colloidal Dispersions ◽  
Synthesis And Characterization ◽  
X Ray ◽  
Transmission Electron ◽  
Vis Spectroscopy ◽  
Chemical Liquid Deposition ◽  
Liquid Deposition

Metal colloids in 2-mercaptoethanol using nanoparticles (NPs) of iron (Fe), cobalt (Co), and nickel (Ni) were prepared by chemical liquid deposition method. Transmission electron microscopy, electron diffraction, UV-VIS spectroscopy, and scanning electron microscopy with electron dispersive X-ray spectroscopy characterized the resulting colloidal dispersions. The NPs exhibited sizes with ranges from 9.8 nm for Fe, 3.7 nm for Co, and 7.2 nm for Ni. The electron diffraction shows the presence of the metals in its elemental state Fe (0), Co (0), and Ni (0) and also some compounds FeO (OH), CoCo2S4, and NiNi2S4.

scholarly journals Synthesis and Characterization of Clay Polymer Nanocomposites of P(4VP-co-AAm) and Their Application for the Removal of Atrazine

Polymers ◽  
2019 ◽  
Vol 11 (4) ◽  
pp. 721 ◽  
Author(s):  
Jorge A. Ramírez-Gómez ◽  
Javier Illescas ◽  
María del Carmen Díaz-Nava ◽  
Claudia Muro-Urista ◽  
Sonia Martínez-Gallegos ◽  
...  
Keyword(s):  
Polymer Nanocomposites ◽  
Nanocomposite Materials ◽  
Synthesis And Characterization ◽  
Cross Linking ◽  
X Ray Diffraction ◽  
Numerous Species ◽  
X Ray ◽  
Different Types ◽  
Synthesized Materials

Atrazine (ATZ) is an herbicide which is applied to the soil, and its mechanism of action involves the inhibition of photosynthesis. One of its main functions is to control the appearance of weeds in crops, primarily in corn, sorghum, sugar cane, and wheat; however, it is very toxic for numerous species, including humans. Therefore, this work deals with the adsorption of ATZ from aqueous solutions using nanocomposite materials, synthesized with two different types of organo-modified clays. Those were obtained by the free radical polymerization of 4-vinylpyridine (4VP) and acrylamide (AAm) in different stoichiometric ratios, using tetrabutylphosphonium persulfate (TBPPS) as a radical initiator and N,N′-methylenebisacrylamide (BIS) as cross-linking agent. The structural, morphological, and textural characteristics of clays, copolymers, and nanocomposites were determined through different analytical and instrumental techniques, i.e., X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR), and thermogravimetric analysis (TGA). Adsorption kinetics experiments of ATZ were determined with the modified and synthesized materials, and the effect of the ratio between 4VP and AAm moieties on the removal capacities of the obtained nanocomposites was evaluated. Finally, from these sets of experiments, it was demonstrated that the synthesized nanocomposites with higher molar fractions of 4VP obtained the highest removal percentages of ATZ.

scholarly journals Synthesis and characterization of novel protein nanodots as drug delivery carriers with an enhanced biological efficacy of melatonin in breast cancer cells

RSC Advances ◽  
2021 ◽  
Vol 11 (16) ◽  
pp. 9076-9085
Author(s):  
Kanchan Yadav ◽  
Megha Das ◽  
Nurul Hassan ◽  
Archana Mishra ◽  
Jayeeta Lahiri ◽  
...  
Keyword(s):  
Breast Cancer ◽  
Drug Delivery ◽  
Cancer Cells ◽  
Live Cell Imaging ◽  
Biomedical Applications ◽  
Breast Cancer Cells ◽  
Cell Imaging ◽  
Synthesis And Characterization ◽  
Novel Protein

A novel nanodot-using protein has been synthesized for the live cell imaging and drug delivery of melatonin in breast cancer cells. Its unique properties hold potential for various biomedical applications in the field of bioimaging and drug delivery.

scholarly journals High-pressure synthesis and characterization of the non-centrosymmetric scandium borate ScB6O9(OH)3

2020 ◽  
Vol 75 (6-7) ◽  
pp. 597-603
Author(s):  
Birgit Fuchs ◽  
Hubert Huppertz
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Synthesis And Characterization ◽  
X Ray Diffraction ◽  
X Ray ◽  
High Pressure High Temperature ◽  
Structure Solution ◽  
Temperature Experiment ◽  
Pressure Synthesis

AbstractThe non-centrosymmetric scandium borate ScB6O9(OH)3 was obtained through a high-pressure/high-temperature experiment at 6 GPa and 1473 K. Single-crystal X-ray diffraction revealed that the structure is isotypic to InB6O9(OH)3 containing borate triple layers separated by scandium layers. The compound crystallizes in the space group Fdd2 with the lattice parameters a = 38.935(4), b = 4.4136(4), and c = 7.6342(6) Å. Powder X-ray diffraction and vibrational spectroscopy were used to further characterize the compound and verify the proposed structure solution.

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