scholarly journals Factors affecting solid phase microextraction (SPME) to concentrate the odorants of Chinese white salted noodles for GC–MS analysis

2007 ◽  
Vol 22 (4) ◽  
pp. 274-279 ◽  
Author(s):  
Li-Yun Lin ◽  
Chiung-Huei Peng ◽  
Hui-Er Wang ◽  
Tsung-Han Wu ◽  
Cheng-Chang Chen ◽  
...  
Keyword(s):  
Solid Phase Microextraction ◽  
Solid Phase ◽  
Factors Affecting ◽  
Ms Analysis ◽  
Chinese White

Development of an effervescent tablet microextraction method using NiFe2O4-based magnetic nanoparticles for preconcentration/extraction of heavy metals prior to ICP-MS analysis of seafood

2019 ◽  
Vol 34 (3) ◽  
pp. 598-606 ◽  
Author(s):  
Peipei Zhou ◽  
Rongjie Zheng ◽  
Wei Zhang ◽  
Wei Liu ◽  
Yanyan Li ◽  
...  
Keyword(s):  
Heavy Metals ◽  
Magnetic Nanoparticles ◽  
Metal Ions ◽  
Solid Phase Microextraction ◽  
Solid Phase ◽  
Ms Analysis ◽  
Icp Ms ◽  
Effervescent Tablet

A novel magnetic NiFe2O4-based effervescent tablet-assisted dispersive solid-phase microextraction (MNET-DSPM) was developed for extraction of metal ions prior to ICP-MS.

MIL-53(Al)/Fe2O3 nanocomposite for solid-phase microextraction of organophosphorus pesticides followed by GC-MS analysis

2020 ◽  
Vol 187 (12) ◽  
Author(s):  
Soleyman Moinfar ◽  
Ali Khodayari ◽  
Shabnam Sohrabnezhad ◽  
Ali Aghaei ◽  
Lazgin Abdi Jamil
Keyword(s):  
Solid Phase Microextraction ◽  
Solid Phase ◽  
Organophosphorus Pesticides ◽  
Ms Analysis

Headspace solid-phase microextraction (HS-SPME) coupled with gas chromatography-mass spectrometric (GC-MS) analysis of volatile profiles during the stir-frying process of malt

2016 ◽  
Vol 8 (7) ◽  
pp. 1699-1704 ◽  
Author(s):  
Yao Xu ◽  
Xia Zhou ◽  
Dayong Zhang ◽  
Zelun Lan ◽  
Yun Zhang ◽  
...  
Keyword(s):  
Gas Chromatography ◽  
Solid Phase Microextraction ◽  
Solid Phase ◽  
Mass Spectrometric ◽  
Volatile Profile ◽  
Headspace Solid Phase Microextraction ◽  
Frying Process ◽  
Ms Analysis ◽  
Volatile Profiles ◽  
The Relationship

The purpose of this study was to analyze the relationship between volatile profile variations of malt and its stir-fried forms, so as to sum up odor changes in the stir-frying process.

scholarly journals Sampling Dynamics for Volatile Organic Compounds Using Headspace Solid-Phase Microextraction Arrow for Microbiological Samples

Separations ◽  
2018 ◽  
Vol 5 (3) ◽  
pp. 45 ◽  
Author(s):  
Kevin Eckert ◽  
David Carter ◽  
Katelynn Perrault
Keyword(s):  
Volatile Organic Compounds ◽  
Organic Compounds ◽  
Solid Phase Microextraction ◽  
Solid Phase ◽  
Fiber Type ◽  
Gas Chromatography Mass Spectrometry ◽  
Ms Analysis ◽  
Wide Range ◽  
Volatile Organic ◽  
Agricultural Applications

Volatile organic compounds (VOCs) are monitored in numerous fields using several commercially-available sampling options. Sorbent-based sampling techniques, such as solid-phase microextraction (SPME), provide pre-concentration and focusing of VOCs prior to gas chromatography–mass spectrometry (GC–MS) analysis. This study investigated the dynamics of SPME Arrow, which exhibits an increased sorbent phase volume and improved durability compared to traditional SPME fibers. A volatile reference mixture (VRM) and saturated alkanes mix (SAM) were used to investigate optimal parameters for microbiological VOC profiling in combination with GC–MS analysis. Fiber type, extraction time, desorption time, carryover, and reproducibility were characterized, in addition to a comparison with traditional SPME fibers. The developed method was then applied to longitudinal monitoring of Bacillus subtilis cultures, which represents a ubiquitous microbe in medical, forensic, and agricultural applications. The carbon wide range/polydimethylsiloxane (CWR/PDMS) fiber was found to be optimal for the range of expected VOCs in microbiological profiling, and a statistically significant increase in the majority of VOCs monitored was observed. B. subtilis cultures released a total of 25 VOCs of interest, across three different temporal trend categories (produced, consumed, and equilibrated). This work will assist in providing foundational data for the use of SPME Arrow in future microbiological applications.

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