Time to ignition, heat release rate and fire endurance time of wood in cone calorimeter test

2001 ◽  
Vol 25 (4) ◽  
pp. 161-167 ◽  
Author(s):  
Toshiro Harada
Keyword(s):  
Heat Release ◽  
Heat Release Rate ◽  
Release Rate ◽  
Cone Calorimeter ◽  
Endurance Time ◽  
Cone Calorimeter Test ◽  
Time To Ignition ◽  
Fire Endurance

scholarly journals Use of the cone calorimeter to detect seasonal differences in selected combustion characteristics of ornamental vegetation

2005 ◽  
Vol 14 (3) ◽  
pp. 321 ◽  
Author(s):  
David R. Weise ◽  
Robert H. White ◽  
Frank C. Beall ◽  
Matt Etlinger
Keyword(s):  
Moisture Content ◽  
Heat Release ◽  
Heat Release Rate ◽  
Release Rate ◽  
Cone Calorimeter ◽  
Mass Loss Rate ◽  
Combustion Characteristics ◽  
Release Rates ◽  
Intermediate Scale ◽  
Time To Ignition

The flammability of living vegetation is influenced by a variety of factors, including moisture content, physical structure and chemical composition. The relative flammability of ornamental vegetation is of interest to homeowners seeking to make their homes ‘fire safe’. The relative importance of the factors influencing fire behaviour characteristics, such as flammability, is unknown. In the present study, oxygen consumption calorimetry was used to obtain selected combustion characteristics of ornamental vegetation. Peak heat release rate, mass loss rate, time to ignition and effective heat of combustion of 100 × 100-mm samples of foliage and small branches were measured using a bench-scale cone calorimeter. Green and oven-dry samples of 10 species were collected and tested seasonally for a period of 1 year. Similar measurements were made on whole shrubs in an intermediate-scale calorimeter. The range of cone calorimeter peak heat release rates for green and oven-dry samples was 1–176 and 49–331 kW m−2, respectively. Moisture content significantly reduced heat release rates and increased time to ignition. Peak heat release rates for Olea europea and Adenostoma fasciculatum were consistently highest over the year of testing; Aloe sp. consistently had the lowest heat release rate. The correlation of peak heat release rates measured by the cone calorimeter and an intermediate-scale calorimeter was statistically significant yet low (0.51). The use of the cone calorimeter as a tool to establish the relative flammability rating for landscape vegetation requires additional investigation.

scholarly journals Studies on the flammability of polypropylene/ammonium polyphosphate and montmorillonite by using the cone calorimeter test

2018 ◽  
Vol 16 (1) ◽  
pp. 108-115 ◽  
Author(s):  
A.A. Hanna ◽  
M.A. Nour ◽  
E.R. Souaya ◽  
M.A. sherief ◽  
A.S. Abdelmoaty
Keyword(s):  
Heat Release ◽  
Heat Release Rate ◽  
Release Rate ◽  
Cone Calorimeter ◽  
Acid Treatment ◽  
Ammonium Polyphosphate ◽  
Fire Performance ◽  
Cone Calorimeter Test ◽  
Peak Heat Release Rate

AbstractFire performance of polypropylene (PP) containing different percentages of ammonium polyphosphate (APP) with montmorillonite (Mt) or treated montmorillonite (MtT) was carried out by using the cone calorimeter test (CCT). Different samples from ammonium polyphosphate and montmorillonite were mixed with 90% polypropylene. The characterization of the prepared samples indicates that there is incorporation between the components of the samples. Heat release rate (HRR), peak heat release rate (PHRR), average heat release rate (Av-HRR), and time to ignition (TTI) of the samples were obtained from the cone calorimeter test. Also, the fire performance index (FPI) and the fire growth rate (FIGRA) were calculated. The interpretation of the curves and the parameters results from the cone calorimeter test which indicates that the addition of montmorillonite to APP increases its action as a flame retardant for PP. Moreover, the samples contain acid treatment montmorillonite showed an increase in the efficiency of ammonium polyphosphate when used. This result may be due to an increase in the SiO2 content by acid treatment.

Influence of grammage on heat release rate of polypropylene fabrics

2017 ◽  
Vol 36 (1) ◽  
pp. 30-46 ◽  
Author(s):  
Nicolas Hernandez ◽  
Rodolphe Sonnier ◽  
Stéphane Giraud
Keyword(s):  
Heat Flux ◽  
Growth Rate ◽  
Heat Release ◽  
Heat Release Rate ◽  
Release Rate ◽  
Cone Calorimeter ◽  
Heat Fluxes ◽  
Fire Growth ◽  
Time To Ignition ◽  
Moderate Change

The flammability of nine polypropylene fabrics or sheets has been tested using cone calorimeter at various heat fluxes (25, 35, 50, and 75 kW/m2) in order to assess the relevance of this fire test for thermally thin materials. The chosen procedure uses a grid and allows maintaining a constant exposed surface during the test, except for the lightest fabric. The structure of the knitted fabrics has a relatively small influence on the main flammability parameters. On the contrary, the area density of the sample (from 218 to 5729 g/m2) impacts strongly the time to ignition, the peak of heat release rate, and the increase in heat release rate after ignition (fire growth rate). At a fixed heat flux, thicker is the sample, higher are the time to ignition and the peak of heat release rate and lower is the fire growth rate. Moreover, thick samples exhibit the highest sensitivity of peak of heat release rate and the lowest sensitivity of fire growth rate to heat flux. This study emphasizes the fact that a moderate change in weight may have a significant influence on cone calorimeter results, without any significance on real flammability.

Synthesis of a phosphorus–nitrogen-containing flame retardant and its application in epoxy resin

2018 ◽  
Vol 31 (2) ◽  
pp. 186-196 ◽  
Author(s):  
Shuang Yang ◽  
Yefa Hu ◽  
Qiaoxin Zhang
Keyword(s):  
Heat Release ◽  
Flame Retardant ◽  
Epoxy Resin ◽  
Heat Release Rate ◽  
Flame Retardancy ◽  
Release Rate ◽  
Epoxy Resins ◽  
Proton Nuclear Magnetic Resonance ◽  
Scanning Calorimetry ◽  
Cone Calorimeter Test

In this article, a phosphorus–nitrogen-containing flame retardant (DOPO-T) was successfully synthesized by nucleophilic substitution reaction between 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) and cyanuric chloride. The chemical structure of DOPO-T was characterized by Fourier transform infrared spectroscopy, proton nuclear magnetic resonance (NMR) and phosphorous-31 NMR, and elemental analysis. DOPO-T was then blended with diglycidyl ether of bisphenol-A to prepare flame-retardant epoxy resins. Thermal properties, flame retardancy, and combustion behavior of the cured epoxy resins were evaluated by differential scanning calorimetry, thermogravimetric analysis, limited oxygen index (LOI) measurement, UL94 vertical burning test, and cone calorimeter test. The results indicated that the glass transition temperature ( Tg) and temperature at 5% weight loss of epoxy resin (EP)/DOPO-T thermosets were gradually decreased with the increasing content of DOPO-T. DOPO-T catalyzed the decomposition of EP matrix in advance. The flame-retardant performance of EP thermosets was significantly enhanced with the addition of DOPO-T. EP/DOPO-T-0.9 sample had an LOI value of 36.2% and achieved UL94 V-1 rating. In addition, the average of heat release rate, peak of heat release rate, average of effective heat of combustion, and total heat release (THR) of EP/DOPO-T-0.9 sample were decreased by 32%, 48%, 23%, and 31%, respectively, compared with the neat EP sample. Impressively, EP/DOPO-T thermosets acquired excellent flame retardancy under low loading of flame retardant.

A Comparison of the Behaviour of Spruce Wood and Polyolefins during the Test on the Cone Calorimeter

2013 ◽  
Vol 726-731 ◽  
pp. 4280-4287 ◽  
Author(s):  
Jozef Martinka ◽  
Emília Hroncová ◽  
Tomáš Chrebet ◽  
Karol Balog
Keyword(s):  
Heat Flux ◽  
Heat Release ◽  
Heat Release Rate ◽  
Release Rate ◽  
Cone Calorimeter ◽  
Lower Sensitivity ◽  
Average Heat ◽  
Fire Propagation ◽  
Spruce Wood

This article deals with comparison of the behaviour of spruce wood and polyolefins (polyethylene PE and polypropylene PP) during the test on the cone calorimeter. Samples were tested on the cone calorimeter at heat flux of 20 and 40 kW/m2. An evaluation of the behaviour of examined materials was based on the determination of the maximum and the average heat release rate, yield of carbon monoxide (CO), and relative comparison of tendency to fire propagation in a flashover phase. The tendency of materials to fire propagation in the flashover phase was evaluated based on the Pearson ́s correlation, the Spearman ́s correlation and the Kendall ́s correlation coefficient of HRR-CO and CO2-CO. Spruce wood showed better properties in comparison with PE and PP in all evaluated parameters (the maximum and the average heat release rate, the yield of CO, and also the resistance to fire propagation in the flashover phase. Additionally, spruce wood showed significantly lower sensitivity of dependence of the maximum and also the average heat release rate on external heat flux.

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