A new method for preparation of an etched porous joint for capillary electrophoresis and its pore-size evaluation

2009 ◽  
Vol 30 (8) ◽  
pp. 1355-1361 ◽  
Author(s):  
Longhua Guo ◽  
Bin Qiu ◽  
Mingxing Chen ◽  
Guonan Chen
2008 ◽  
Vol 607 ◽  
pp. 39-41
Author(s):  
Jerzy Kansy ◽  
Radosław Zaleski

A new method of analysis of PALS spectra of porous materials is proposed. The model considers both the thermalization process of positronium inside the pores and the pore size distribution. The new model is fitted to spectra of mesoporous silica MCM-41 and MSF. The resulting parameters are compared with parameters obtained from fitting the “conventional” models, i.e. a sum of exponential components with discrete or/and distributed lifetimes.


2018 ◽  
Vol 6 (2) ◽  
pp. 535-547 ◽  
Author(s):  
Chuanjie Fang ◽  
Sungil Jeon ◽  
Saeid Rajabzadeh ◽  
Liang Cheng ◽  
Lifeng Fang ◽  
...  

A new method was used to tailor the surface pore size of PVDF hollow fiber membranes in the TIPS process by the co-extrusion of different solvents at the outer layer of the extruded polymeric solution.


2014 ◽  
Vol 894 ◽  
pp. 3-7 ◽  
Author(s):  
Grzegorz Adamek ◽  
Montasser Dewidar ◽  
Jarosław Jakubowicz

In this work a new method of Ti-void composites (foam, scaffold) preparation is shown. In this process as a space holder particles we have applied a saccharose crystals (table sugar) with size up to 1.3 mm. After Ti and saccharose particles mixing and pressing, a green compacts composed of sugar and Ti grains were produced. Then, the sugar crystals were removed by its dissolution in water, which lead to open spaces (pores) formation in the green compacts. Then the compacts were sintered at 1250 °C. Alternatively, a sugar was evaporated during sintering without water dissolution. The foams were investigated by SEM, XRD and computed tomography. Such prepared void metal composites have porosity of about 72% and average pore size of about 0.7 mm. The pores have cubical shape corresponding to sugar crystals shape. The method is very promising in foams preparation and the made Ti-void composites can be applied for hard tissue implants, for example.


2017 ◽  
Vol 41 (21) ◽  
pp. 12920-12929 ◽  
Author(s):  
Yan Zhang ◽  
Wujuan Chen ◽  
Yi Zhang ◽  
Yating Zhang ◽  
Luqi Zhu ◽  
...  

A new method of capillary electrophoresis was developed for the sensitive determination of glutathione in biological samples.


1977 ◽  
Vol 5 (3) ◽  
pp. 326-328
Author(s):  
N Sato ◽  
A H Fieldsteel

A new method of enumerating Mycobacterium leprae has been developed. Suspensions containing the organisms were filtered through a polycarbonate membrane filter (25-mm diameter, 0.4-micronm pore size, 10-micronm thick; Nucleopore) to concentrate the organisms. The membrane was then mounted on a glass slide and stained with a standard acid-fast stain. Finally, the membrane was treated with a small amount of chloroform to fix it to the slide and make it transparent. This method enabled us to detect M. leprae in quantities as small as 4.98 X 10(2) regardless of the total volume of the original material. Comparison with a standard method for enumerating M. leprae showed that both methods gave similar results when the organisms counted by the standard method were present in sufficient quantity for reproducibility. Because the least number of organisms that can be detected with the standard method is 10(4) ml and because the organisms detected with the new method could be concentrated on the polycarbonate filter from a large amount of infected fluid, a substantial number of suspensions were shown by the new method, but not by the standard method, to contain M. leprae.


2020 ◽  
Vol 1157 ◽  
pp. 122339
Author(s):  
Magdalena Świądro ◽  
Paweł Stelmaszczyk ◽  
Renata Wietecha-Posłuszny ◽  
Dominika Dudek

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