N-Arylcarbonylpseudoprolines as Tunable Chiral Derivatizing Agents for the Determination of the Absolute Configuration of Secondary Alcohols

2011 ◽  
Vol 2011 (16) ◽  
pp. 2920-2923 ◽  
Author(s):  
So-Yeong Han ◽  
Kihang Choi
Keyword(s):  
Absolute Configuration ◽  
Secondary Alcohols ◽  
The Absolute ◽  
Chiral Derivatizing Agents

ChemInform Abstract: Study for the Determination of the Absolute Configuration of Fluoromethylated Secondary Alcohols by the Modified Mosher Method.

ChemInform ◽  
2010 ◽  
Vol 28 (51) ◽  
pp. no-no
Author(s):  
L. XIAO ◽  
T. YAMAZAKI ◽  
T. KITAZUME ◽  
T. YONEZAWA ◽  
Y. SAKAMOTO ◽  
...  
Keyword(s):  
Absolute Configuration ◽  
Secondary Alcohols ◽  
The Absolute

Determination of the absolute configuration of secondary alcohols by modified Horeau's method using HPLC

1989 ◽  
Vol 54 (1) ◽  
pp. 151-159 ◽  
Author(s):  
Aleš Svatoš ◽  
Irena Valterová ◽  
Anna Fábryová ◽  
Jan Vrkoč
Keyword(s):  
Absolute Configuration ◽  
Secondary Alcohols ◽  
Model Compounds ◽  
Defense Substance ◽  
Determination Of Absolute Configuration ◽  
The Absolute

A method for determination of absolute configuration of secondary alcohols, based on a modified Horeau's method, has been developed. The ratio of (1R,2'S)- and (1R,2'R)-N-[1-(1-naphthyl)-ethyl]-2-phenylbutanamides (V and VI, respectively) was determined by HPLC on a straight phase. The method was tested on a series of steroid and terpene model compounds and was used in the determination of absolute configuration of 15-ripperten-3α-ol (XV), the defense substance of Nasutitermes nigriceps termites. The sensibility of the determination is 100 nmol of the alcohol.

A new approach for the determination of the absolute configuration of secondary alcohols by 1H NMR with O-substituted mandelate derivatives

1998 ◽  
Vol 39 (13) ◽  
pp. 1759-1762 ◽  
Author(s):  
Isabelle Chataigner ◽  
Jacques Lebreton ◽  
Didier Durand ◽  
André Guingant ◽  
Jean Villiéras
Keyword(s):  
1H Nmr ◽  
Absolute Configuration ◽  
Secondary Alcohols ◽  
New Approach ◽  
The Absolute

Determination of the absolute configuration of chiral secondary alcohols; new advances using 13C- and 2D-NMR spectroscopy

1993 ◽  
Vol 4 (7) ◽  
pp. 1527-1532 ◽  
Author(s):  
T. Pehk ◽  
E. Lippmaa ◽  
M. Lopp ◽  
A. Paju ◽  
B.C. Borer ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
Absolute Configuration ◽  
2D Nmr ◽  
Secondary Alcohols ◽  
2D Nmr Spectroscopy ◽  
The Absolute

Study for the determination of the absolute configuration of fluoromethylated secondary alcohols by the modified Mosher method

1997 ◽  
Vol 84 (1) ◽  
pp. 19-23 ◽  
Author(s):  
Ling Xiao ◽  
Takashi Yamazaki ◽  
Tomoya Kitazume ◽  
Tetsuo Yonezawa ◽  
Yoshitake Sakamoto ◽  
...  
Keyword(s):  
Absolute Configuration ◽  
Secondary Alcohols ◽  
The Absolute
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