Preparation and Characterization of Cu2SnSe4 Nanoparticles Using a Microwave-Assisted Polyol Method

2004 ◽  
Vol 2004 (9) ◽  
pp. 1859-1864 ◽  
Author(s):  
Haviv Grisaru ◽  
V. G. Pol ◽  
Aharon Gedanken ◽  
Israel Nowik
Keyword(s):  
Polyol Method ◽  
Microwave Assisted

scholarly journals Microwave-assisted synthesis and characterization of some optically active poly(ester-imide) thermoplastic elastomers

e-Polymers ◽  
2009 ◽  
Vol 9 (1) ◽  
Author(s):  
Saeed Zahmatkesh ◽  
Abdol Reza Hajipour
Keyword(s):  
Thermal Analyses ◽  
Specific Rotation ◽  
Thermoplastic Elastomers ◽  
Optically Active ◽  
Microwave Assisted Synthesis ◽  
H Nmr ◽  
Microwave Assisted ◽  
Diacid Chloride ◽  
Elemental Analyses

AbstractPyromellitic dianhydride (1) was reacted with L-leucine (2) to result in [N,N'-(pyromellitoyl)-bis-L-leucine diacid] (3). This compound (3) was converted to N,N'-(pyromellitoyl)-bis-L-leucine diacid chloride (4) by reaction with thionyl chloride. The microwave-assisted polycondensation of this diacid chloride (4) with polyethyleneglycol-diol (PEG-200) and/or three synthetic bisphenols furnish a series of new PEIs and Co-PEIs in a laboratory microwave oven (Milestone). The resulting polymers and copolymers have inherent viscosities in the range of 0.31- 0.53 dl g-1. These polymers are optically active, thermally stable and soluble in polar aprotic solvents such as DMF, DMSO, NMP, DMAc and sulfuric acid. All of the above polymers were fully characterized by IR spectroscopy, 1H NMR spectroscopy, elemental analyses, specific rotation and thermal analyses. Some structural characterizations and physical properties of these optically active PEIs and Co-PEIs are reported.

Microwave-assisted synthesis and characterization of hexagonal Fe3O4 nanoplates

2010 ◽  
Vol 12 (1) ◽  
pp. 99-104 ◽  
Author(s):  
Huifen Zhou ◽  
Ran Yi ◽  
Junhui Li ◽  
Yuan Su ◽  
Xiaohe Liu
Keyword(s):  
Synthesis And Characterization ◽  
Microwave Assisted Synthesis ◽  
Microwave Assisted

Microwave assisted synthesis and solid-state characterization of lithocholyl amides of isomeric aminopyridines

Steroids ◽  
2011 ◽  
Vol 76 (3) ◽  
pp. 261-268 ◽  
Author(s):  
Kari V. Ahonen ◽  
Manu K. Lahtinen ◽  
Arto M. Valkonen ◽  
Martin Dračínský ◽  
Erkki T. Kolehmainen
Keyword(s):  
Solid State ◽  
Microwave Assisted Synthesis ◽  
Microwave Assisted ◽  
Solid State Characterization

Microwave Assisted Hydrothermal Synthesis and Structural Characterization of TiO2 Nanotubes

2015 ◽  
Vol 15 (9) ◽  
pp. 7391-7394 ◽  
Author(s):  
Sung Hun Cho ◽  
Rajesh Adhikari ◽  
Seung Ho Kim ◽  
Tae Ho Kim ◽  
Soo Wohn Lee
Keyword(s):  
Hydrothermal Synthesis ◽  
Structural Characterization ◽  
Tio2 Nanotubes ◽  
Microwave Assisted
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