Triple Resonance Cross-Polarization for More Sensitive 13C MAS NMR Spectroscopy of Deuterated Proteins

ChemPhysChem ◽  
2011 ◽  
Vol 12 (11) ◽  
pp. 2092-2096 ◽  
Author(s):  
Ümit Akbey ◽  
Francesca Camponeschi ◽  
Barth-Jan van Rossum ◽  
Hartmut Oschkinat
Keyword(s):  
Nmr Spectroscopy ◽  
Mas Nmr ◽  
Triple Resonance ◽  
Cross Polarization ◽  
13C Mas Nmr ◽  
Deuterated Proteins

scholarly journals Probing Pore Size and Connectivity in Porous Silicas Using 13C MAS NMR Spectroscopy of Supercritical Methane

2020 ◽  
Vol 124 (21) ◽  
pp. 11536-11543
Author(s):  
Geoffrey M. Bowers ◽  
Eric D. Walter ◽  
Sarah D. Burton ◽  
Kaitlynn C. Schwarz ◽  
David W. Hoyt ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
Pore Size ◽  
Mas Nmr ◽  
13C Mas Nmr

Optimized Spectral Editing of 13C MAS NMR Spectra of Rigid Solids Using Cross-Polarization Methods

1994 ◽  
Vol 107 (1) ◽  
pp. 67-78 ◽  
Author(s):  
R. Sangill ◽  
N. Rastrupandersen ◽  
H. Bildsoe ◽  
H.J. Jakobsen ◽  
N.C. Nielsen
Keyword(s):  
Nmr Spectra ◽  
Mas Nmr ◽  
Cross Polarization ◽  
Spectral Editing ◽  
13C Mas Nmr

Solid-State Heteronuclear-Correlation NMR Studies of Multicomponent Phosphate Glasses

1998 ◽  
Vol 547 ◽  
Author(s):  
S. Prabakar ◽  
J.M. Egan ◽  
R.M. Wenslow ◽  
K.T. Mueller
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Phosphate Glasses ◽  
Mas Nmr ◽  
Quadrupolar Nuclei ◽  
Sodium Ions ◽  
Cross Polarization ◽  
Nmr Studies ◽  
Heteronuclear Correlation ◽  
Aluminophosphate Glasses

AbstractThe correlation between 23Na and 31P nuclei in alkali phosphates has been investigated by cross-polarization MAS NMR spectroscopy. Connectivity between sodium ions with various phosphorus tetrahedra has been demonstrated in a variety of crystalline-and amorphous alkali phosphates. CPMAS NMR experiments were also performed on sodium aluminophosphate glasses from both quadrupolar nuclei (23Na and 27Al) to the phosphorus nuclei to establish connectivity of sodium and phosphorus as well as aluminum and phosphorus nuclei in these systems.

High-resolution J-coupled 13C MAS NMR spectroscopy of lipid membranes

2009 ◽  
Vol 161 (2) ◽  
pp. 77-85 ◽  
Author(s):  
Filip Ciesielski ◽  
David C. Griffin ◽  
Michael Rittig ◽  
Boyan B. Bonev
Keyword(s):  
Nmr Spectroscopy ◽  
High Resolution ◽  
Lipid Membranes ◽  
Mas Nmr ◽  
13C Mas Nmr
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