Preliminary Interlaboratory Trial for ISO/DIS 12010: Determination of Short Chain Polychlorinated Alkanes (SCCP) in Water

2011 ◽  
Vol 39 (6) ◽  
pp. 537-542 ◽  
Author(s):  
Sabine Geiß ◽  
Nicole Lettmann ◽  
Aurélien Rey ◽  
Herbert Lepper ◽  
Birgit Körner ◽  
...  
Keyword(s):  
Short Chain ◽  
Interlaboratory Trial ◽  
Polychlorinated Alkanes

Validation interlaboratory trial for ISO 12010: Water quality—Determination of short-chain polychlorinated alkanes (SCCP) in water

2011 ◽  
Vol 17 (1) ◽  
pp. 15-25 ◽  
Author(s):  
Sabine Geiß ◽  
Max Schneider ◽  
Gerhild Donnevert ◽  
Jürgen W. Einax ◽  
Nicole Lettmann ◽  
...  
Keyword(s):  
Water Quality ◽  
Short Chain ◽  
Interlaboratory Trial ◽  
Polychlorinated Alkanes

scholarly journals Distillation Cleanup Preceded GC Determination of Short-Chain Monocarboxylic Acids in Aqueous and Solid Samples of Wastewater Origin

2012 ◽  
Vol 19 (3) ◽  
pp. 423-431
Author(s):  
Anna Banel ◽  
Anna Jakimska ◽  
Marta Wasielewska ◽  
Bogdan Zygmunt
Keyword(s):  
Biological Treatment ◽  
Organic Molecules ◽  
Enrichment Factors ◽  
Aerobic Biodegradation ◽  
Short Chain ◽  
Aqueous Sample ◽  
Operational Parameters ◽  
Solid Samples ◽  
Monocarboxylic Acids

Distillation Cleanup Preceded GC Determination of Short-Chain Monocarboxylic Acids in Aqueous and Solid Samples of Wastewater OriginShort-chain monocarboxylic acids (SCMAs) (C2-C5) formed in the process of aerobic biodegradation of larger organic molecules should often be monitored to optimize wastewater biological treatment and study the processes of converting organic waste matter into methane, etc. Gas chromatography (GC) seems a method of choice for such a task. Majority of samples require clean up before they can be injected into GC system. In this work a special refluxing apparatus is applied to concentrate and clean up the troublesome environment samples before injection into GC. To optimize separation of SCMAs in aqueous sample a special arrangement of two capillary columns, of very different polarity was used. The operational parameters of sample preparation were optimized and enrichment factors determined. The procedure developed was applied to determine SCMAs in troublesome aqueous and solid samples of wastewater treatment origin.

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