ChemInform Abstract: Structural Characterization of Magnesium-Based Compounds Mg9Si5and Mg4Si3Al (Superconductor) Synthesized under High Pressure and High Temperature Conditions.
In this study, diamond crystals co-doped with boron and nitrogen were synthesized via a temperature gradient method at 5.3–5.8 GPa and 1300–1550 °C by adding B and N dopants to a system of carbon and an Fe-based solvent catalyst.
Correction for ‘Synthesis and characterization of boron and nitrogen co-doped diamond crystals under high pressure and high temperature conditions’ by Meihua Hu et al., CrystEngComm, 2017, 19, 4571–4575.
In this study, {111}-oriented diamond crystals with different nitrogen concentrations were successfully synthesized in a series of experiments at 5.8 GPa pressure and 1380–1400 °C temperature.
By high-pressure/high-temperature multianvil synthesis a new high-pressure (HP) phase of Co3TeO6 was obtained. The compound crystallizes in the acentric trigonal crystal system of the Ni3TeO6-type structure with space group R3...
AbstractThe non-centrosymmetric scandium borate ScB6O9(OH)3 was obtained through a high-pressure/high-temperature experiment at 6 GPa and 1473 K. Single-crystal X-ray diffraction revealed that the structure is isotypic to InB6O9(OH)3 containing borate triple layers separated by scandium layers. The compound crystallizes in the space group Fdd2 with the lattice parameters a = 38.935(4), b = 4.4136(4), and c = 7.6342(6) Å. Powder X-ray diffraction and vibrational spectroscopy were used to further characterize the compound and verify the proposed structure solution.