ChemInform Abstract: Hantzsch Reaction: Synthesis and Characterization of Some New 1,4-Dihydropyridine Derivatives as Potent Antimicrobial and Antioxidant Agents.

ChemInform ◽  
2012 ◽  
Vol 43 (12) ◽  
pp. no-no
Author(s):  
A. M. Vijesh ◽  
Arun M. Isloor ◽  
S. K. Peethambar ◽  
K. N. Shivananda ◽  
T. Arulmoli ◽  
...  
2011 ◽  
Vol 282-283 ◽  
pp. 267-270 ◽  
Author(s):  
Guo Qing Zhong ◽  
Mei Gu ◽  
Yan Zhang

Bioinorganic complexes of nicotinic acid with trivalent antimony and bismuth are synthesized by solid-liquid reaction at room temperature. The formula of the complexes is Sb(C5H4NCOOH)2Cl3•H2O and Bi(C5H4NCOOH)2Cl3•H2O respectively. The crystal structure of the complex of nicotinic acid and Sb(III) belongs to triclinic system and that of nicotinic acid and Bi(III) belongs to monoclinic system. Thermal analysis can indicate the complex formation between antimony or bismuth ion and nicotinic acid.


2006 ◽  
Vol 181 (10) ◽  
pp. 2435-2444 ◽  
Author(s):  
Shahram Ghodsi ◽  
Eskandar Alipour ◽  
Mohsen Amini ◽  
Ramin Miri ◽  
Karim Masoud Tagi-Ganji ◽  
...  

2014 ◽  
Vol 33 (2) ◽  
pp. 189 ◽  
Author(s):  
Mustafa Er ◽  
Ayşe Şahin ◽  
Hakan Tahtacı

<p>Thiosemicarbazone derivatives <strong>3a–e</strong> were synthesized by the reaction of various aldehydes<strong> 1a–e</strong> with 4-methyl thiosemicarbazide <strong>2</strong> in 78% to 90% yield. Then, the thiazole moieties of the target materials <strong>5a–e</strong> were obtained in high yields (71–93%) using the Hantzsch reaction utilizing thiosemicarbazone derivatives <strong>3a–e</strong> with ethyl-2-chloroacetoacetic ester. The substituted nitrile derivatives <strong>7a–e</strong> were obtained in moderate to high yield (58–84%) from the reaction of compounds <strong>5a–e</strong> with chloroacetonitrile by the nucleophilic aliphatic substitution reaction in the presence of anhydrous potassium carbonate. Finally, substituted 2-amino-1,3,4-thiadiazole compounds <strong>9a–e</strong> were obtained in moderate to good yields (51–62%) from the reaction of thiosemicarbazide with substituted nitrile derivatives <strong>7a–e</strong>. As a result, compounds that all share a high disposition for biological activities were obtained. The structures of the newly synthesized compounds were confirmed by IR, <sup>1</sup>H NMR, <sup>13</sup>C NMR, elemental analysis, and mass spectrometric techniques.</p>


Author(s):  
Diqiang Liu ◽  
Aijun Zhang ◽  
Jiangang Jia ◽  
Junyan Zhang ◽  
Junhu Meng

Polyhedron ◽  
2016 ◽  
Vol 120 ◽  
pp. 196-204 ◽  
Author(s):  
Neelima Mishra ◽  
Kavita Poonia ◽  
Nutan Sharma ◽  
Sarvesh K. Soni ◽  
Dinesh Kumar

2008 ◽  
Vol 45 (6) ◽  
pp. 1597-1602 ◽  
Author(s):  
Milind Rode ◽  
R. C. Gupta ◽  
B. K. Karale ◽  
S. S. Rindhe

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