Asymmetric Synthesis of (S)-2-Amino-3-(1-naphthyl)propanoic Acid via Chiral Nickel Complex. Crystal Structure, Circular Dichroism,1H and13C NMR Spectra of the Complex.

ChemInform ◽  
2006 ◽  
Vol 37 (12) ◽  
Author(s):  
Alexander Popkov ◽  
Ivana Cisarova ◽  
Jana Sopkova ◽  
Josef Jirman ◽  
Antonin Lycka ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Asymmetric Synthesis ◽  
Nmr Spectra ◽  
Nickel Complex ◽  
Propanoic Acid ◽  
1H And13c Nmr Spectra ◽  
1H And13c Nmr ◽  
Complex Crystal Structure ◽  
Circular Dichroïsm ◽  
Complex Crystal

Asymmetric Synthesis of (S)-2-Amino-3-(1-naphthyl)propanoic Acid via Chiral Nickel Complex. Crystal Structure, Circular Dichroism, 1H and 13C NMR Spectra of the Complex

2005 ◽  
Vol 70 (9) ◽  
pp. 1397-1410 ◽  
Author(s):  
Alexander Popkov ◽  
Ivana Císařová ◽  
Jana Sopková ◽  
Josef Jirman ◽  
Antonín Lyčka ◽  
...  
Keyword(s):  
Circular Dichroism ◽  
Asymmetric Synthesis ◽  
1H And 13C Nmr ◽  
X Ray ◽  
Complex Crystal Structure ◽  
Cotton Effects ◽  
Circular Dichroïsm ◽  
Complex Crystal ◽  
C Nmr

The recently published environmentally friendly preparation of a glycine synthon 2 from regeneratable chiral auxiliary BPB ((S)-N-(2-benzoylphenyl)-N'-benzylprolinamide) was used for preparative asymmetric synthesis of the non-coded amino acid 3-(1-naphthyl)alanine (1). Full assignment of 1H and 13C NMR of both intermediate complex 3 and 1 and X-ray structure determination of complex 3 were made. Cotton effects observed in circular dichroism spectrum of complex 3 are consistent with published empirical rules.

Synthesis,1H- and13C-NMR spectra, crystal structure and ring openings of 1-methyl-6,9-epoxy-9-aryl-5,6,9,10-tetrahydro-1H-imidazo [3,2-e] [2H-1,5] oxazocinium methanesulfonate

1997 ◽  
Vol 34 (5) ◽  
pp. 1607-1620 ◽  
Author(s):  
Subhash P. Upadhyaya ◽  
Frank S. Davis ◽  
Jae Jeong Lee ◽  
Kyaw Zaw ◽  
Ludwig Bauer ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Nmr Spectra ◽  
1H And13c Nmr Spectra ◽  
1H And13c Nmr

1H and13C NMR spectra of fifteen substituted isoquinolines

1991 ◽  
Vol 29 (5) ◽  
pp. 513-517 ◽  
Author(s):  
Janis T. Nelson ◽  
Roman Davis
Keyword(s):  
Nmr Spectra ◽  
1H And13c Nmr Spectra ◽  
1H And13c Nmr

A Novel Example of Metal-Mediated Aromatic Thiolation in a Ruthenium Complex. Crystal Structure of RuII(SC6H4NNC6H4N)2†

1996 ◽  
Vol 35 (10) ◽  
pp. 3050-3052 ◽  
Author(s):  
Bidyut Kumar Santra ◽  
Ganesh A. Thakur ◽  
Prasanta Ghosh ◽  
Amitava Pramanik ◽  
Goutam Kumar Lahiri
Keyword(s):  
Crystal Structure ◽  
Ruthenium Complex ◽  
Complex Crystal Structure ◽  
Complex Crystal
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