ChemInform Abstract: Synthesis of AlPO4-5 Aluminum Phosphate Molecular Sieve Crystals for Membrane Applications by Microwave Heating.

ChemInform ◽  
2010 ◽  
Vol 26 (46) ◽  
pp. no-no
Author(s):  
I. GIRNUS ◽  
M.-M. POHL ◽  
J. RICHTER-MENDAU ◽  
M. SCHNEIDER ◽  
M. NOACK ◽  
...  
Keyword(s):  
Microwave Heating ◽  
Molecular Sieve ◽  
Aluminum Phosphate

Molecular Sieve Thin Films via Laser Ablation

1994 ◽  
Vol 351 ◽  
Author(s):  
Kenneth J. Balkus ◽  
Scott J. Riley ◽  
Bruce E. Gnade
Keyword(s):  
Thin Films ◽  
Laser Ablation ◽  
Molecular Sieves ◽  
Molecular Sieve ◽  
Film Formation ◽  
Aluminum Phosphate ◽  
Effective Technique ◽  
Solid Films ◽  
Ft Ir ◽  
Ft Ir Spectroscopy

ABSTRACTLaser ablation has become widely recognized as an effective technique for the preparation of thin solid films. We have employed an excimer laser (KrF, 248 nm) to deposit well dispersed thin films of aluminum phosphate molecular sieves on a titanium nitride substrate. Results for the ablation of AIPO4-5, AIPO4-H3 and AIPO4-H1 molecular sieve targets are presented. The laser power and repetition rate as well as substrate distance and temperature affect the thin film formation. A subsequent hydrothermal post treatment of the ablated films was found to enhance the surface crystallinity. The molecular sieve thin films were characterized by XRD, SEM, XRF, and FT-IR spectroscopy.

Synthesis of AIPO4-5 aluminumphosphate molecular sieve crystals for membrane applications by microwave heating

1995 ◽  
Vol 7 (8) ◽  
pp. 711-714 ◽  
Author(s):  
Irina Girnus ◽  
Marga-Martina Pohl ◽  
Jürgen Richter-Mendau ◽  
Matthias Schneider ◽  
Manfred Noack ◽  
...  
Keyword(s):  
Microwave Heating ◽  
Molecular Sieve

Novel Aluminum Phosphate-5 Crystal Morphologies Synthesized by Microwave Heating of a Water-in-Oil Microemulsion

Langmuir ◽  
2004 ◽  
Vol 20 (4) ◽  
pp. 1039-1042 ◽  
Author(s):  
J-C. Lin ◽  
J. T. Dipre ◽  
M. Z. Yates
Keyword(s):  
Microwave Heating ◽  
Aluminum Phosphate

scholarly journals Adsorption calorimetric measurements and aluminum-27 DOR NMR studies on the molecular sieve aluminum phosphate-18

1993 ◽  
Vol 97 (46) ◽  
pp. 12042-12046 ◽  
Author(s):  
Jochen Janchen ◽  
Mart P. J. Peeters ◽  
Jan W. de Haan ◽  
Leo J. M. van de Ven ◽  
Jan H. C. van Hooff ◽  
...  
Keyword(s):  
Molecular Sieve ◽  
Aluminum Phosphate ◽  
Nmr Studies ◽  
Calorimetric Measurements

Preparation and x-ray powder structure solution of a novel aluminum phosphate molecular sieve, (AlPO4)3.cntdot.(CH3)4NOH

1986 ◽  
Vol 90 (23) ◽  
pp. 6122-6125 ◽  
Author(s):  
Philip R. Rudolf ◽  
Carlos Saldarriaga-Molina ◽  
Abraham Clearfield
Keyword(s):  
Molecular Sieve ◽  
Aluminum Phosphate ◽  
X Ray ◽  
Structure Solution

Molecular Sieve Based Chemical Sensors

1994 ◽  
Vol 351 ◽  
Author(s):  
Laura J. Sottile ◽  
Kenneth J. Balkus ◽  
Scott J. Riley ◽  
Bruce E. Gnade
Keyword(s):  
Thin Films ◽  
Laser Ablation ◽  
Titanium Nitride ◽  
Hydrothermal Treatment ◽  
Chemical Sensors ◽  
Molecular Sieves ◽  
Molecular Sieve ◽  
Aluminum Phosphate ◽  
Shape Selectivity ◽  
Target Molecules

ABSTRACTBy virtue of their shape selectivity and stability, molecular sieves are ideal components for discriminating chemical sensors. In this paper we report the preparation of capacitance type sensors based on aluminum phosphate molecular sieves. Thin films of the molecular sieves AlPO4-5, A1PO 4-H3 and AlPO4-H1, which cover a range of pore dimensions, were deposited on titanium nitride coated silicon wafers by laser ablation. A subsequent hydrothermal treatment followed by a Pd/Au coating and the application of standard photoresist/masking techniques were used to generate the capacitors. The molecular sieves exhibit significant changes in capacitance upon exposure to target molecules, including CO2, CO, N2, H2O and toluene.

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