ChemInform Abstract: Radical Pair Formation in Phenyl Ring Containing Molecules: Crystal Structure of Ph3P+CH2SCH3Cl-and ESR Study of the X-Irradiated Single Crystal

1986 ◽  
Vol 17 (33) ◽  
Author(s):  
M. GEOFFROY ◽  
M. V. V. S. REDDY ◽  
G. BERNARDINELLI
Author(s):  
Michel Geoffroy ◽  
Michel Wermeille ◽  
Paule Castan ◽  
Diane Deguenon ◽  
Gérald Bernardinelli

2014 ◽  
Vol 926-930 ◽  
pp. 300-303
Author(s):  
Huan Mei Guo ◽  
Yun Chen Zhang ◽  
Yu Feng Li

3-(4-Fluorophenyl)-1,5-bis (pyridyl)-1,5-pentanedione has been synthesized and the crystal structure has been determined by means of single-crystal X-ray diffraction. In the moleculer structure,the phenyl ring and the two pyridine rings are almost perpendicular , and two pyridine rings are closed to coplane.


2014 ◽  
Vol 926-930 ◽  
pp. 262-265
Author(s):  
Huan Mei Guo ◽  
Yun Chen Zhang ◽  
Yu Feng Li

1N-Acetyl-3-phenyl-5-(3,4,5-trimethoxyl-phenyl)-2-pyrazoline has been synthesized and the crystal structure has been determined by means of single-crystal X-ray diffraction. The pyrazolinyl ring and the phenyl rings at 3 positions of the pyrazoline are almost coplane , with their dihedral angle to be 6.63(2) o. Phenyl ring at 5 positions and pyrazolinyl ring are almost perpendicular, the dihedral angle is 78.03(3) o.


Author(s):  
Michel Geoffroy ◽  
Théo Berclaz ◽  
Alice Celalyan-Berthier ◽  
Natarajan Rajalakshmi ◽  
Malledi V.V.S. Reddy

Author(s):  
Süheyla Özbey ◽  
F. B. Kaynak ◽  
M. Toğrul ◽  
N. Demirel ◽  
H. Hoşgören

AbstractA new type of inclusion complex, S(–)-1 phenyl ethyl ammonium percholorate complex of R-(–)-2-ethyl - N - benzyl - 4, 7, 10, 13 - tetraoxa -1- azacyclopentadecane, has been prepared and studied by NMR, IR and single crystal X-ray diffraction techniques. The compound crystallizes in space group


2020 ◽  
Author(s):  
Keishiro Yamashita ◽  
Kazuki Komatsu ◽  
Hiroyuki Kagi

An crystal-growth technique for single crystal x-ray structure analysis of high-pressure forms of hydrogen-bonded crystals is proposed. We used alcohol mixture (methanol: ethanol = 4:1 in volumetric ratio), which is a widely used pressure transmitting medium, inhibiting the nucleation and growth of unwanted crystals. In this paper, two kinds of single crystals which have not been obtained using a conventional experimental technique were obtained using this technique: ice VI at 1.99 GPa and MgCl<sub>2</sub>·7H<sub>2</sub>O at 2.50 GPa at room temperature. Here we first report the crystal structure of MgCl2·7H2O. This technique simultaneously meets the requirement of hydrostaticity for high-pressure experiments and has feasibility for further in-situ measurements.


1999 ◽  
Vol 84 (4) ◽  
pp. 536-549 ◽  
Author(s):  
Edward S. Grew ◽  
Guenther J. Redhammer ◽  
Georg Amthauer ◽  
Mark A. Cooper ◽  
Frank C. Hawthorne ◽  
...  

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