Coordination Polymers Based on [Cp*Fe(η5-P5)]: Solid-State Structure and MAS NMR Studies

2011 ◽  
Vol 18 (4) ◽  
pp. 1168-1179 ◽  
Author(s):  
Fabian Dielmann ◽  
Andrea Schindler ◽  
Sabine Scheuermayer ◽  
Junfeng Bai ◽  
Roger Merkle ◽  
...  
Keyword(s):  
Solid State ◽  
Coordination Polymers ◽  
Mas Nmr ◽  
State Structure ◽  
Nmr Studies ◽  
Solid State Structure

Solid-state structure by X-ray and 13C CP/MAS NMR of new 6-acetyl-8-bromo-5-O-alkylamino-4,7-dimethylcoumarins

2018 ◽  
Vol 29 (6) ◽  
pp. 1903-1915 ◽  
Author(s):  
Kinga Ostrowska ◽  
Dorota Maciejewska ◽  
Grzegorz Cichowicz ◽  
Łukasz Dobrzycki
Keyword(s):  
Solid State ◽  
Mas Nmr ◽  
State Structure ◽  
Solid State Structure ◽  
X Ray ◽  
Cp Mas Nmr ◽  
13C Cp Mas Nmr

Synthesis, Solid-State Structure and Multinuclear NMR Studies of the New Polyhydrido Iridium Carbonyl Cluster Ir4H4(μ-H)4(CO)4(PPh3)4

2003 ◽  
Vol 2003 (11) ◽  
pp. 2108-2112 ◽  
Author(s):  
Luigi Garlaschelli ◽  
Francesco Greco ◽  
Giulia Peli ◽  
Mario Manassero ◽  
Mirella Sansoni ◽  
...  
Keyword(s):  
Solid State ◽  
Carbonyl Cluster ◽  
State Structure ◽  
Nmr Studies ◽  
Solid State Structure ◽  
Multinuclear Nmr

Solid state structure by X-ray and 13C CP/MAS NMR of new 7-[2-(N,N-diisopropylamino)ethoxy]coumarins

2009 ◽  
Vol 930 (1-3) ◽  
pp. 195-200 ◽  
Author(s):  
Joanna Trykowska ◽  
Elżbieta Hejchman ◽  
Irena Wolska ◽  
Dorota Maciejewska
Keyword(s):  
Solid State ◽  
Mas Nmr ◽  
State Structure ◽  
Solid State Structure ◽  
X Ray ◽  
Cp Mas Nmr ◽  
13C Cp Mas Nmr

Synthesis, solid state structure, and solution behaviour of the lighter lanthanide bis(trimethylsilyl)amido chlorides, [Ln{N(SiMe3)2}2(THF)(µ-Cl)]2 (Ln = Ce, Nd)

2000 ◽  
Vol 78 (4) ◽  
pp. 454-458 ◽  
Author(s):  
David J Berg ◽  
Roland AL Gendron
Keyword(s):  
Crystal Structure ◽  
Solid State ◽  
State Structure ◽  
Nmr Studies ◽  
Centrosymmetric Dimer ◽  
Solid State Structure ◽  
X Ray ◽  
H Nmr ◽  
Redistribution Reactions ◽  
Lanthanide Amide

The synthesis of [Ln{N(SiMe3)2}2(THF)(µ-Cl)]2 (Ln = Ce, 1; Nd, 2) by reaction of sodium bis(trimethylsilyl)amide (2 equiv.) with LnCl3 is reported. The same complexes were also isolated from the ligand redistribution reactions of Ln[N(SiMe3)2]3 and LnCl3 (2:1 ratio) in THF at 80°C. The crystal structure of 2, determined by X-ray diffraction, revealed a centrosymmetric dimer with bridging chlorides and pentacoordinate metal centres. 1H NMR studies show that the solid state structure is not maintained in solution. NMR evidence for the presence of Ln[N(SiMe3)2]3 and two other bis(trimethylsilyl)amide containing species, presumably Ln[N(SiMe3)2]Cl2(THF)x and Ln[N(SiMe3)2]2Cl(THF)y, is presented.Key words: lanthanide, amide, neodymium, cerium, crystal structure, X-ray, nuclear magnetic resonance, redistribution.

Solid state structure by X-ray and 13C CP/MAS NMR of new 5,5′-diethoxy-3,3′-methanediyl-bis-indole

2007 ◽  
Vol 831 (1-3) ◽  
pp. 174-179 ◽  
Author(s):  
Magdalena Rasztawicka ◽  
Irena Wolska ◽  
Dorota Maciejewska
Keyword(s):  
Solid State ◽  
Mas Nmr ◽  
State Structure ◽  
Solid State Structure ◽  
X Ray ◽  
Cp Mas Nmr ◽  
13C Cp Mas Nmr

Solid state structure by X-ray and 13C CP/MAS NMR of new 5-[2-(N,N-dimethylamino)ethoxy]-4,7-dimethylcoumarins

2016 ◽  
Vol 1112 ◽  
pp. 25-32 ◽  
Author(s):  
Kinga Ostrowska ◽  
Dorota Maciejewska ◽  
Łukasz Dobrzycki ◽  
Pawel Socha
Keyword(s):  
Solid State ◽  
Mas Nmr ◽  
State Structure ◽  
Solid State Structure ◽  
X Ray ◽  
Cp Mas Nmr ◽  
13C Cp Mas Nmr
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