Microwave-Assisted Suzuki Coupling Reactions with an Encapsulated Palladium Catalyst for Batch and Continuous-Flow Transformations

2006 ◽  
Vol 12 (16) ◽  
pp. 4407-4416 ◽  
Author(s):  
Ian R. Baxendale ◽  
Charlotte M. Griffiths-Jones ◽  
Steven V. Ley ◽  
Geoffrey K. Tranmer
Keyword(s):  
Palladium Catalyst ◽  
Continuous Flow ◽  
Suzuki Coupling ◽  
Coupling Reactions ◽  
Microwave Assisted

Microwave-Assisted Suzuki Coupling Reactions with an Encapsulated Palladium Catalyst for Batch and Continuous-Flow Transformations.

ChemInform ◽  
2006 ◽  
Vol 37 (40) ◽  
Author(s):  
Ian R. Baxendale ◽  
Charlotte M. Griffiths-Jones ◽  
Steven V. Ley ◽  
Geoffrey K. Tranmer
Keyword(s):  
Palladium Catalyst ◽  
Continuous Flow ◽  
Suzuki Coupling ◽  
Coupling Reactions ◽  
Microwave Assisted

Microwave-assisted, solventless Suzuki coupling reactions on palladium-doped alumina

2000 ◽  
Vol 2 (3) ◽  
pp. 120-122 ◽  
Author(s):  
George W. Kabalka ◽  
Richard M. Pagni ◽  
Lei Wang ◽  
Vasudevan Namboodiri ◽  
C. Maxwell Hair
Keyword(s):  
Suzuki Coupling ◽  
Coupling Reactions ◽  
Microwave Assisted

scholarly journals Microwave-Assisted Synthesis of Pd Nanoparticles and Catalysis Application for Suzuki Coupling Reactions

2017 ◽  
Vol 11 (1) ◽  
pp. 1-8 ◽  
Author(s):  
Jian Zhang ◽  
Xuefeng Bai
Keyword(s):  
Chemical Reduction ◽  
Phenylboronic Acid ◽  
Suzuki Coupling ◽  
Pd Nanoparticles ◽  
Xrd Analysis ◽  
Microwave Assisted Synthesis ◽  
Coupling Reactions ◽  
Microwave Assisted ◽  
Highly Active ◽  
Aryl Bromides

A facile and efficient method was developed for the synthesis of highly active palladium nanoparticles (PdNPs) by microwave-assisted chemical reduction. The PdNPs with different morphology were prepared with or without KBr (capping agent) using ethylene glycol (EG) and citric acid (CA) as reducing agent in the presence of polyvinylpyrrolidone (PVP), respectively. The as-prepared PdNPs were characterized by (UV-Visible Spectrophotometer) UV-Vis, transmission electron microscopy (TEM) and X-ray diffraction (XRD) analysis. The results showed that the PdNPs reduced by EG without KBr (PdNPs-EG) has smaller particle size than other PdNPs. The remarkable catalytic activity of the PdNPs catalysts are obtained using a low amount of PdNPs (0.1 mmol‰) using K2CO3 as base and EtOH/H2O as solvent toward Suzuki coupling reactions of aryl bromides and phenylboronic acid for 15 min.

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